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Acta Cryst. (2005). E61, o2027-o2029  [ doi:10.1107/S1600536805017113 ]

Diethyl 2,8-diamino-4,10-bis(3-nitrophenyl)naphtho[1,2-b;6,5-b']dipyran-3,9-dicarboxylate dimethylformamide disolvate

Y.-C. Wang, X.-S. Wang, Z.-S. Zeng and D.-Q. Shi

Abstract: The title compound, C34H28N4O10·2C3H7NO, was synthesized by the reaction of ethyl 2-cyano-3-(3-nitrophenyl)-1-acrylate and 1,5-naphthalenediol in the presence of KF-Al2O3 in refluxing ethanol. The structure is centrosymmetric and the fused pyran ring adopts a boat conformation.

Online 10 June 2005


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