Acta Cryst. (2005). E61, m1464-m1466  [ doi:10.1107/S1600536805020611 ]

Porous solvent-free ₂-bis(salicylidene)propane-1,3-diaminato-bis{[bis(salicylidene)propane-1,3-diaminato]iron(III)}

M. Bakir, T. P. Dasgupta, S. K. Dutta, N. Ngah and B. M. Yamin

Online 6 July 2005

Key indicators

• Single-crystal X-ray study
• T = 273 K
• Mean (C-C) = 0.004 Å
• R factor = 0.040
• wR factor = 0.102
• Data-to-parameter ratio = 16.3

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT601_ALERT_2_A Structure Contains Solvent Accessible VOIDS of .     352.00 A   3  

Alert level C
PLAT164_ALERT_4_C Nr. of Refined C-H H-Atoms in Heavy-At Struct...          1       
PLAT410_ALERT_2_C Short Intra H...H Contact  H24    ..  H25B    ..       1.99 Ang.  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          7     
            O3  -FE1 -O2  -C17    13.40  0.50   1.555   1.555   1.555   1.555   
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         12     
            O2  -FE1 -O3  -C18    40.50  0.50   1.555   1.555   1.555   1.555   

   1 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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