Acta Cryst. (2005). E61, m1644-m1645  [ doi:10.1107/S160053680502338X ]

Nonacarbonyl-₃-N,N-diethyldithiocarbamato-³S:S:S'--hydrido-triosmium(3 Os-Os)

I. Garcia-Orozco, C. J. Pastor, B. Souto, E. Delgado, E. Hernández and C. Alvarez-Toledano

Online 27 July 2005

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.009 Å
• R factor = 0.028
• wR factor = 0.067
• Data-to-parameter ratio = 13.6

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......       0.96       
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.84 Ratio 

Alert level C
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) .....         10 Ang.  
PLAT142_ALERT_4_C su on b - Axis Small or Missing (x 100000) .....         10 Ang.  
PLAT143_ALERT_4_C su on c - Axis Small or Missing (x 100000) .....         20 Ang.  
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.67 Ratio 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.33 Ratio 
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Os1    -   C1      ..       5.02 su    
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          9       

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   9 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion

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