Acta Cryst. (2005). E61, m1475-m1477  [ doi:10.1107/S1600536805020982 ]

Di--diphenylphosphido-bis[tricarbonyliron(II)] dichloromethane solvate

M. G. Ballinas-López, I. I. Padilla-Martínez, F. J. Martínez-Martínez, H. Höpfl and E. V. García-Báez

Online 6 July 2005

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.044
• wR factor = 0.132
• Data-to-parameter ratio = 18.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT199_ALERT_1_C Check the Reported _cell_measurement_temperature        293 K     
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.71 Ratio 
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Fe     -   C10     ..       7.17 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Fe     -   C11     ..       6.10 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Fe     -   C12     ..       6.66 su    
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C21    -C22_b         1.37 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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