Acta Cryst. (2005). E61, m1662-m1664  [ doi:10.1107/S1600536805023639 ]

[1-Acetylacetone (2-hydroxybenzoyl)hydrazonato]pyridinecopper(II)

M.-L. Liu, J.-M. Dou, D.-Q. Wang and D.-C. Li

Online 30 July 2005

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.013 Å
• R factor = 0.067
• wR factor = 0.220
• Data-to-parameter ratio = 13.5

checkCIF/PLATON results

No syntax errors found




Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.10
            Rint given   0.125
PLAT020_ALERT_3_C The value of Rint is greater than 0.10 .........       0.12       
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.98       
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         13       
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety         C8     
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety        C12     

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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