# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Ndzn in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 380.73 _exptl_crystal_F_000 1170.00 _reflns_d_resolution_high 0.8361 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.3751 _cell_length_b 13.7258 _cell_length_c 16.4798 _cell_angle_alpha 103.903 _cell_angle_beta 99.490 _cell_angle_gamma 100.168 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11957.54 12399.89 45.85 o 3 0 0 44465.64 49483.77 213.38 o 4 0 0 9388.65 9535.51 104.10 o 5 0 0 4523.70 4435.72 24.30 o 6 0 0 3912.40 4045.50 13.40 o 7 0 0 4.34 -4.70 10.93 o 8 0 0 448.60 475.51 35.34 o 9 0 0 187.00 181.32 12.18 o 10 0 0 189.97 219.89 18.22 o 11 0 0 2057.82 2170.98 22.05 o 12 0 0 521.32 510.14 19.71 o 13 0 0 278.80 311.67 20.92 o -13 1 0 481.22 455.22 29.21 o -12 1 0 943.44 973.53 24.22 o -11 1 0 0.41 -3.03 14.23 o -10 1 0 1067.49 1094.02 18.25 o -9 1 0 1847.27 1827.32 19.72 o -8 1 0 933.73 954.18 54.74 o -7 1 0 1465.75 1450.43 47.14 o -6 1 0 2390.14 2324.88 53.43 o -5 1 0 11687.32 11796.96 60.08 o -4 1 0 190.32 170.57 7.16 o -3 1 0 18542.23 20575.56 21.53 o -2 1 0 13383.64 14830.00 172.65 o -1 1 0 31712.71 1820.75 937.64 o 0 1 0 616.02 12.44 3.59 o 1 1 0 21011.23 25292.34 128.09 o 2 1 0 4690.04 4795.88 62.51 o 3 1 0 0.41 16.25 6.51 o 4 1 0 2214.36 2137.61 10.01 o 5 1 0 2027.68 1726.21 14.81 o 6 1 0 395.03 407.49 13.62 o 7 1 0 320.14 299.55 10.07 o 8 1 0 638.26 682.27 24.18 o 9 1 0 840.30 910.15 15.32 o 10 1 0 694.96 737.01 14.26 o 11 1 0 3.90 18.43 22.20 o 12 1 0 625.27 587.76 41.82 o -13 2 0 3.70 40.70 16.84 o -12 2 0 50.98 61.73 16.91 o -11 2 0 228.61 267.99 17.79 o -10 2 0 1080.41 1041.16 19.99 o -9 2 0 858.58 843.55 17.50 o -8 2 0 1230.09 1239.15 50.30 o -7 2 0 11763.38 12116.11 266.86 o -6 2 0 3594.01 3321.43 57.93 o -5 2 0 7610.02 7837.69 68.88 o -4 2 0 10073.84 10263.36 103.83 o -3 2 0 3354.40 3063.65 48.34 o -2 2 0 1449.60 1780.57 64.75 o -1 2 0 15848.89 18250.91 244.75 o 0 2 0 2355.27 2224.79 35.29 o 1 2 0 4117.11 3797.52 77.26 o 2 2 0 325.41 283.06 8.71 o 3 2 0 276.50 291.31 11.90 o 4 2 0 10415.44 11181.66 117.81 o 5 2 0 6271.80 6363.30 83.15 o 6 2 0 2638.89 2672.14 32.40 o 7 2 0 6958.85 7248.53 45.64 o 8 2 0 2405.14 2430.32 14.89 o 9 2 0 222.76 262.19 10.73 o 10 2 0 886.72 873.16 29.94 o 11 2 0 245.54 239.53 25.53 o 12 2 0 68.31 43.90 13.37 o -13 3 0 39.49 78.88 20.60 o -12 3 0 64.49 59.66 27.18 o -11 3 0 1078.96 1213.40 31.12 o -10 3 0 342.45 380.66 32.19 o -9 3 0 3863.78 3930.11 267.46 o -8 3 0 10381.56 9967.74 30.30 o -7 3 0 962.06 1095.09 13.14 o -6 3 0 19129.28 19050.06 62.50 o -5 3 0 19716.50 19623.40 198.92 o -4 3 0 1465.05 1749.07 122.10 o -3 3 0 5872.77 6157.07 28.69 o -2 3 0 2146.33 2599.08 151.42 o -1 3 0 15.88 9.30 19.69 o 0 3 0 2235.32 2118.47 12.35 o 1 3 0 15629.05 16922.03 66.67 o 2 3 0 854.05 822.21 9.18 o 3 3 0 12215.46 12467.96 296.65 o 4 3 0 4276.37 4940.03 67.12 o 5 3 0 11632.89 12043.06 81.03 o 6 3 0 7998.67 8207.23 78.19 o 7 3 0 429.73 377.18 20.48 o 8 3 0 5287.39 5304.92 65.11 o 9 3 0 2048.87 2060.68 41.85 o 10 3 0 536.85 540.01 15.43 o 11 3 0 1712.18 1661.18 176.52 o 12 3 0 333.38 277.39 46.79 o -13 4 0 178.74 189.95 21.27 o -12 4 0 36.87 5.43 27.35 o -11 4 0 1099.46 1055.73 74.27 o -10 4 0 1787.91 1631.72 22.48 o -9 4 0 265.58 260.01 20.83 o -8 4 0 3031.52 2861.49 125.16 o -7 4 0 9523.27 9666.56 538.57 o -6 4 0 822.10 764.53 33.48 o -5 4 0 1991.84 1966.48 24.22 o -4 4 0 13323.85 12854.79 119.07 o -3 4 0 285.00 214.88 13.95 o -2 4 0 251.18 215.00 27.62 o -1 4 0 28483.95 32184.89 232.37 o 0 4 0 7590.48 8092.85 110.07 o 1 4 0 8667.08 8670.92 42.93 o 2 4 0 6328.10 7141.69 184.54 o 3 4 0 1154.68 1294.42 16.59 o 4 4 0 8008.96 8649.62 96.37 o 5 4 0 244.81 207.89 10.00 o 6 4 0 4228.31 4462.50 59.93 o 7 4 0 3355.09 3472.36 104.80 o 8 4 0 17.34 49.54 14.31 o 9 4 0 1318.28 1357.93 26.21 o 10 4 0 1634.66 1496.28 81.52 o 11 4 0 58.83 43.25 10.99 o -13 5 0 785.93 742.17 26.74 o -12 5 0 735.83 755.04 24.40 o -11 5 0 127.73 124.02 27.16 o -10 5 0 1540.43 1457.22 69.60 o -9 5 0 1535.84 1441.26 27.04 o -8 5 0 24.96 9.77 47.73 o -7 5 0 1607.86 1460.69 29.19 o -6 5 0 2416.96 2452.14 41.66 o -5 5 0 113.35 83.74 59.09 o -4 5 0 16.73 9.41 17.50 o -3 5 0 957.35 808.26 16.94 o -2 5 0 12319.59 13406.11 31.15 o -1 5 0 5759.28 6501.64 47.74 o 0 5 0 1658.90 1392.65 17.82 o 1 5 0 15197.65 16097.91 51.10 o 2 5 0 6409.42 6480.98 174.01 o 3 5 0 3668.87 3815.62 23.54 o 4 5 0 2651.32 2612.31 59.47 o 5 5 0 2857.90 2871.25 14.45 o 6 5 0 130.86 130.21 23.33 o 7 5 0 1966.02 1966.39 18.16 o 8 5 0 1304.56 1252.78 18.33 o 9 5 0 169.83 190.32 23.10 o 10 5 0 74.91 68.63 25.05 o 11 5 0 166.81 205.05 34.81 o -13 6 0 153.97 203.25 67.17 o -12 6 0 1297.84 1171.59 67.31 o -11 6 0 2209.24 2197.52 157.72 o -10 6 0 92.76 123.28 29.72 o -9 6 0 2426.46 2389.09 26.89 o -8 6 0 2708.88 2702.21 26.29 o -7 6 0 189.39 188.23 52.36 o -6 6 0 175.06 117.35 27.24 o -5 6 0 31.10 2.71 17.83 o -4 6 0 52.88 52.25 30.05 o -3 6 0 1082.69 1290.89 55.29 o -2 6 0 3642.52 3463.10 22.26 o -1 6 0 6623.02 6769.31 153.29 o 0 6 0 15770.02 16341.11 132.32 o 1 6 0 211.19 152.44 12.77 o 2 6 0 14086.21 14670.28 393.38 o 3 6 0 10585.36 10811.88 106.15 o 4 6 0 413.99 487.34 12.24 o 5 6 0 4481.76 4584.65 38.88 o 6 6 0 3762.29 3956.35 31.34 o 7 6 0 293.48 325.93 22.32 o 8 6 0 543.87 534.81 24.29 o 9 6 0 32.08 -4.08 15.68 o 10 6 0 1.50 19.73 10.77 o -13 7 0 337.48 355.00 80.30 o -12 7 0 1027.11 1023.48 26.29 o -11 7 0 2.76 16.58 20.53 o -10 7 0 951.11 917.45 38.04 o -9 7 0 276.03 319.17 25.50 o -8 7 0 24.39 4.37 22.96 o -7 7 0 640.84 641.54 41.04 o -6 7 0 261.65 174.55 38.45 o -5 7 0 364.90 439.59 20.58 o -4 7 0 0.83 25.05 19.41 o -3 7 0 701.78 709.96 69.07 o -2 7 0 6667.07 6880.08 86.66 o -1 7 0 3789.10 4168.61 29.48 o 0 7 0 1227.16 1149.21 18.37 o 1 7 0 8657.03 8874.70 52.97 o 2 7 0 1976.57 1743.44 52.51 o 3 7 0 181.71 209.95 13.82 o 4 7 0 4816.45 4799.88 30.68 o 5 7 0 2742.25 2826.66 80.00 o 6 7 0 19.94 12.10 13.78 o 7 7 0 916.23 860.19 44.96 o 8 7 0 64.34 108.10 18.48 o 9 7 0 75.35 141.75 47.18 o 10 7 0 2.83 51.51 99.44 o -12 8 0 42.16 25.33 28.33 o -11 8 0 147.09 125.66 22.92 o -10 8 0 626.00 680.63 42.86 o -9 8 0 204.36 265.21 38.00 o -8 8 0 2111.48 2125.95 44.22 o -7 8 0 3944.02 3843.13 39.44 o -6 8 0 317.35 379.93 37.94 o -5 8 0 2833.03 2860.53 28.94 o -4 8 0 4380.66 4325.42 30.14 o -3 8 0 457.42 463.95 22.78 o -2 8 0 2250.08 2322.24 65.11 o -1 8 0 1993.92 2085.48 23.65 o 0 8 0 3175.83 2959.60 27.55 o 1 8 0 975.10 961.07 35.99 o 2 8 0 1032.27 984.82 26.05 o 3 8 0 1433.34 1405.59 20.60 o 4 8 0 38.01 40.64 23.48 o 5 8 0 230.60 249.97 14.94 o 6 8 0 1474.81 1523.42 102.90 o 7 8 0 738.71 720.92 28.84 o 8 8 0 25.41 22.37 15.94 o 9 8 0 327.60 330.46 20.95 o -12 9 0 4.77 9.22 27.82 o -10 9 0 46.80 77.01 42.31 o -9 9 0 800.47 725.75 42.87 o -8 9 0 1085.90 1190.35 43.92 o -7 9 0 338.29 383.41 41.82 o -6 9 0 7120.71 7200.61 60.86 o -5 9 0 4994.79 5041.44 53.34 o -4 9 0 1174.72 1153.19 71.68 o -3 9 0 11511.65 12464.92 438.06 o -2 9 0 3013.45 2998.08 38.96 o -1 9 0 1707.20 1556.02 45.72 o 0 9 0 6958.85 6742.10 130.40 o 1 9 0 102.56 91.00 38.81 o 2 9 0 544.13 545.00 17.12 o 3 9 0 19.32 39.96 16.98 o 4 9 0 143.72 159.93 21.58 o 5 9 0 535.41 538.34 25.24 o 6 9 0 889.25 827.11 65.35 o 7 9 0 48.03 52.93 18.57 o 8 9 0 1417.39 1200.36 65.45 o 9 9 0 331.78 245.39 19.47 o -12 10 0 156.64 131.32 31.96 o -11 10 0 507.43 553.52 50.83 o -10 10 0 32.10 40.48 46.78 o -9 10 0 255.28 266.68 46.35 o -8 10 0 774.82 821.14 33.11 o -7 10 0 1332.36 1381.99 46.43 o -5 10 0 2675.86 2683.75 47.29 o -4 10 0 2666.82 2644.84 45.89 o -3 10 0 22.80 15.78 37.77 o -2 10 0 3600.87 3568.09 87.50 o -1 10 0 3934.27 3885.91 110.90 o 0 10 0 87.57 89.12 21.25 o 1 10 0 1142.54 1228.16 37.84 o 2 10 0 89.89 133.09 21.92 o 3 10 0 10.29 6.96 29.19 o 4 10 0 2.47 15.81 25.59 o 5 10 0 24.25 45.06 17.68 o 6 10 0 663.89 685.09 33.97 o 7 10 0 630.94 536.86 70.84 o 8 10 0 25.71 16.68 18.41 o -11 11 0 48.79 -12.22 52.05 o -7 11 0 928.11 911.01 79.68 o -6 11 0 549.11 634.37 45.86 o -4 11 0 297.42 285.44 31.42 o -3 11 0 669.42 678.29 45.14 o -1 11 0 957.59 937.19 27.50 o 0 11 0 475.96 461.45 37.09 o 1 11 0 2794.38 2654.52 26.44 o 2 11 0 1551.76 1656.30 40.45 o 3 11 0 1.70 -28.79 25.10 o 4 11 0 1708.70 1735.23 49.04 o 5 11 0 734.79 732.83 38.52 o 6 11 0 29.92 32.48 18.08 o 7 11 0 308.23 296.45 40.85 o -10 12 0 183.26 273.81 51.10 o -9 12 0 743.34 734.24 54.66 o -8 12 0 1841.46 1748.84 57.75 o -7 12 0 0.14 0.29 49.19 o -5 12 0 694.58 806.03 51.59 o -4 12 0 303.60 199.85 44.31 o -3 12 0 89.09 25.84 46.78 o -2 12 0 154.30 136.26 24.55 o -1 12 0 1036.33 1167.82 29.82 o 0 12 0 2408.45 2385.24 88.04 o 1 12 0 328.64 226.30 44.62 o 2 12 0 627.06 683.13 24.69 o 3 12 0 1708.28 1798.02 49.58 o 4 12 0 0.35 57.24 21.24 o 5 12 0 1503.50 1447.23 57.89 o 6 12 0 572.44 558.95 87.93 o -7 13 0 737.51 812.04 40.73 o -4 13 0 159.40 122.27 53.45 o -2 13 0 147.36 188.23 74.02 o -1 13 0 176.49 194.47 27.03 o 0 13 0 146.49 215.53 25.74 o 1 13 0 772.70 698.58 66.59 o 2 13 0 579.12 605.88 34.81 o 3 13 0 103.23 151.04 37.65 o 4 13 0 653.77 645.70 52.65 o 5 13 0 169.47 218.24 34.03 o -7 14 0 250.55 129.31 58.65 o -5 14 0 639.35 441.91 62.71 o -3 14 0 0.84 -13.98 44.14 o -2 14 0 441.86 420.24 37.83 o -1 14 0 1179.90 1262.89 48.83 o 0 14 0 5.84 13.46 35.18 o 1 14 0 239.99 292.09 31.04 o 2 14 0 189.60 124.22 55.07 o 3 14 0 22.93 17.45 31.22 o -4 15 0 97.34 179.65 45.90 o -3 15 0 1125.86 1080.81 64.29 o -2 15 0 280.71 410.64 49.72 o -1 15 0 357.89 411.97 32.33 o 0 15 0 1020.32 1007.94 62.58 o 1 15 0 200.55 261.57 35.66 o 2 -16 1 9.83 -19.32 49.70 o 3 -16 1 254.85 248.55 37.87 o 4 -16 1 150.86 194.50 38.48 o -2 -15 1 342.11 341.17 32.50 o -1 -15 1 365.15 297.51 31.92 o 0 -15 1 125.83 175.71 61.90 o 1 -15 1 57.64 29.17 39.35 o 2 -15 1 600.58 629.78 94.43 o 3 -15 1 37.58 29.00 47.58 o 4 -15 1 1090.91 1127.32 48.38 o 5 -15 1 247.01 170.81 52.35 o -3 -14 1 17.58 49.58 31.00 o -2 -14 1 165.71 179.42 26.49 o -1 -14 1 129.06 213.71 52.08 o 0 -14 1 1438.93 1520.45 48.59 o 1 -14 1 422.05 440.03 34.38 o 2 -14 1 483.40 485.12 34.37 o 3 -14 1 1453.77 1591.46 46.06 o 4 -14 1 247.54 309.14 27.48 o 6 -14 1 885.53 913.04 41.74 o -5 -13 1 78.05 47.66 26.74 o -4 -13 1 32.75 6.21 20.99 o -3 -13 1 20.85 -12.07 33.06 o -2 -13 1 225.81 159.98 28.71 o -1 -13 1 543.73 575.54 26.44 o 0 -13 1 78.27 117.05 25.14 o 1 -13 1 1099.72 1170.65 44.06 o 2 -13 1 1352.44 1366.15 49.43 o 3 -13 1 46.43 66.16 28.82 o 4 -13 1 2098.18 2239.19 55.58 o 5 -13 1 1466.04 1238.12 57.95 o 6 -13 1 84.94 37.92 50.59 o 8 -13 1 512.22 449.74 54.94 o -6 -12 1 281.16 264.92 38.61 o -5 -12 1 271.90 243.22 22.71 o -4 -12 1 965.80 947.29 23.77 o -3 -12 1 112.33 104.18 43.52 o -2 -12 1 683.17 709.22 24.14 o -1 -12 1 3833.20 3791.63 72.33 o 0 -12 1 452.28 420.77 24.57 o 1 -12 1 466.74 492.13 24.66 o 2 -12 1 189.81 214.84 28.04 o 3 -12 1 1199.90 1207.43 45.03 o 4 -12 1 1.11 61.75 39.42 o 6 -12 1 596.35 649.76 52.90 o 9 -12 1 899.62 879.43 56.06 o -7 -11 1 9.47 42.61 17.23 o -6 -11 1 1193.51 1116.60 46.45 o -5 -11 1 2342.74 2249.52 141.53 o -4 -11 1 258.50 299.43 33.45 o -3 -11 1 3809.54 3913.47 92.95 o -2 -11 1 1844.20 1711.23 42.32 o -1 -11 1 1126.90 1107.25 37.49 o 0 -11 1 6175.36 5988.23 50.66 o 1 -11 1 611.59 625.76 26.76 o 2 -11 1 697.34 736.08 33.20 o 3 -11 1 624.22 669.09 47.96 o 4 -11 1 80.41 -4.20 76.65 o 5 -11 1 101.06 50.44 42.46 o 6 -11 1 227.90 211.33 43.64 o 7 -11 1 62.75 41.95 46.19 o 8 -11 1 2346.70 2286.22 54.65 o 10 -11 1 134.34 20.94 51.10 o -8 -10 1 149.56 133.88 13.05 o -7 -10 1 419.33 375.52 52.10 o -6 -10 1 79.87 136.25 35.65 o -5 -10 1 418.86 433.11 45.04 o -4 -10 1 1628.19 1597.48 59.39 o -3 -10 1 176.47 184.48 17.87 o -2 -10 1 997.13 1060.67 46.17 o -1 -10 1 2492.78 2361.10 32.87 o 0 -10 1 1189.37 1184.38 20.27 o 1 -10 1 144.01 149.48 29.47 o 2 -10 1 421.81 456.60 37.21 o 3 -10 1 182.29 206.06 35.70 o 4 -10 1 717.47 615.41 48.59 o 5 -10 1 143.92 199.15 40.27 o 6 -10 1 613.87 722.35 46.42 o 7 -10 1 1282.52 1188.91 46.06 o 11 -10 1 3.27 61.63 46.48 o -9 -9 1 676.97 752.60 58.83 o -8 -9 1 7.01 10.19 13.84 o -7 -9 1 1456.18 1299.24 61.59 o -6 -9 1 1493.20 1426.88 59.70 o -5 -9 1 113.41 109.80 19.58 o -4 -9 1 184.90 243.55 25.81 o -3 -9 1 245.86 253.27 15.93 o -2 -9 1 33.06 74.32 20.32 o -1 -9 1 708.71 734.22 35.05 o 0 -9 1 59.84 31.60 18.11 o 1 -9 1 5873.35 5922.25 140.98 o 2 -9 1 2803.67 2794.79 111.03 o 3 -9 1 92.64 152.22 46.56 o 4 -9 1 9876.62 10075.87 52.72 o 5 -9 1 3100.32 3123.34 43.37 o 6 -9 1 323.64 310.83 37.06 o 7 -9 1 4861.21 4876.52 58.45 o 8 -9 1 702.56 746.28 30.50 o 9 -9 1 44.88 -44.51 42.02 o 11 -9 1 613.06 538.74 26.74 o 12 -9 1 74.08 89.96 42.86 o -10 -8 1 31.29 168.21 54.53 o -9 -8 1 719.45 602.76 48.43 o -8 -8 1 2360.19 2067.30 79.20 o -7 -8 1 99.34 106.07 43.00 o -6 -8 1 1075.85 947.52 25.07 o -5 -8 1 430.55 508.64 20.54 o -4 -8 1 65.88 79.57 14.70 o -3 -8 1 630.61 700.95 30.14 o -2 -8 1 124.75 172.95 14.11 o -1 -8 1 9.31 -23.89 14.17 o 0 -8 1 3989.53 4103.51 22.41 o 1 -8 1 624.71 721.22 42.26 o 2 -8 1 9945.61 10301.46 501.53 o 3 -8 1 17879.89 18942.77 319.74 o 4 -8 1 2679.97 3020.84 36.88 o 5 -8 1 7852.92 8127.66 37.44 o 6 -8 1 5899.86 5671.47 95.97 o 7 -8 1 7.17 -35.28 35.43 o 8 -8 1 2310.84 2293.81 43.79 o 9 -8 1 1052.88 1109.11 53.30 o 10 -8 1 109.28 133.82 28.01 o 11 -8 1 282.18 296.32 29.95 o 12 -8 1 0.50 26.42 25.84 o -10 -7 1 1027.06 1096.42 49.95 o -9 -7 1 333.41 281.16 60.18 o -8 -7 1 393.08 372.20 31.95 o -7 -7 1 1511.81 1389.39 57.60 o -6 -7 1 1084.51 1023.29 46.37 o -5 -7 1 26.16 29.50 22.21 o -4 -7 1 2200.43 2220.66 41.29 o -3 -7 1 1893.64 1964.50 63.63 o -2 -7 1 681.24 630.33 26.29 o -1 -7 1 576.69 534.89 13.27 o 0 -7 1 6663.68 7340.13 52.51 o 1 -7 1 11562.62 12063.03 158.71 o 2 -7 1 558.92 686.56 20.33 o 3 -7 1 649.09 784.32 25.84 o 4 -7 1 10812.49 10718.85 51.95 o 5 -7 1 2974.00 3226.19 40.04 o 6 -7 1 410.02 360.34 30.73 o 7 -7 1 8184.34 8368.07 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