# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' bv6019 in Cc' _shelx_refln_list_code 4 _shelx_F_calc_maximum 322.60 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.8018 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' _cell_length_a 10.4862 _cell_length_b 15.1938 _cell_length_c 17.4233 _cell_angle_alpha 90.000 _cell_angle_beta 99.010 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -12 0 0 1239.81 1330.82 37.64 o -10 0 0 1265.37 1336.57 31.53 o -8 0 0 9223.34 8497.81 87.65 o -6 0 0 20424.45 20152.84 110.76 o -4 0 0 13164.71 12126.67 67.65 o -2 0 0 1267.08 1032.96 15.35 o 2 0 0 1029.39 942.64 14.60 o 4 0 0 13653.04 12687.23 69.14 o 6 0 0 20239.26 20155.14 109.95 o 8 0 0 9568.87 8956.75 90.18 o 10 0 0 1264.20 1270.72 30.63 o 12 0 0 1203.94 1285.23 36.25 o -11 1 0 442.24 490.31 15.93 o -9 1 0 420.19 429.16 12.40 o -7 1 0 3458.65 3418.35 52.43 o -5 1 0 10038.21 9890.08 70.12 o -3 1 0 12485.68 12174.70 58.96 o -1 1 0 41701.34 38364.96 235.15 o 1 1 0 40852.12 37709.38 233.22 o 3 1 0 12722.19 12264.78 59.03 o 5 1 0 10526.59 10262.79 71.36 o 7 1 0 3349.20 3270.28 51.16 o 9 1 0 380.93 374.88 12.15 o 11 1 0 484.15 531.84 17.76 o -12 2 0 62.41 52.81 13.08 o -10 2 0 717.99 713.16 21.16 o -8 2 0 1136.18 1037.69 25.07 o -6 2 0 910.87 883.82 26.31 o -4 2 0 27893.11 27328.59 104.11 o -2 2 0 2883.09 2773.78 25.84 o 0 2 0 466.92 530.09 10.10 o 2 2 0 2689.66 2540.66 24.81 o 4 2 0 28807.77 27974.96 105.41 o 6 2 0 892.67 803.74 17.92 o 8 2 0 1097.25 1049.24 24.56 o 10 2 0 733.57 745.75 20.54 o 12 2 0 40.97 10.81 30.03 o -11 3 0 234.08 248.72 13.98 o -9 3 0 589.11 602.91 15.27 o -7 3 0 1587.78 1539.09 37.82 o -5 3 0 5007.18 4984.31 52.67 o -3 3 0 4504.07 4442.22 39.63 o -1 3 0 14661.16 15822.24 57.22 o 1 3 0 16231.79 17589.76 60.31 o 3 3 0 5640.97 5595.36 44.14 o 5 3 0 4703.06 4661.80 50.70 o 7 3 0 1467.73 1441.44 37.54 o 9 3 0 709.25 710.18 18.53 o 11 3 0 175.10 166.28 13.03 o -12 4 0 115.48 106.98 15.40 o -10 4 0 638.24 639.97 20.86 o -8 4 0 3259.57 3173.59 56.39 o -6 4 0 4263.16 4129.96 54.27 o -4 4 0 2362.67 2492.50 35.61 o -2 4 0 720.12 718.39 17.65 o 0 4 0 58679.05 66216.05 466.61 o 2 4 0 877.80 888.96 19.07 o 4 4 0 2238.50 2255.91 34.09 o 6 4 0 4361.41 4197.98 54.91 o 8 4 0 3294.89 3214.54 57.45 o 10 4 0 610.39 591.52 19.97 o 12 4 0 113.70 136.30 13.42 o -11 5 0 1277.13 1348.82 36.66 o -9 5 0 1728.00 1767.33 47.98 o -7 5 0 1028.91 984.35 22.89 o -5 5 0 7277.89 7039.75 66.65 o -3 5 0 23979.26 25458.77 105.15 o -1 5 0 3108.06 3658.69 35.96 o 1 5 0 3227.95 3793.93 36.41 o 3 5 0 23494.71 24527.84 103.11 o 5 5 0 7149.39 6768.22 65.01 o 7 5 0 1148.87 1135.56 24.27 o 9 5 0 1620.29 1543.05 45.87 o 11 5 0 1229.50 1230.89 34.70 o -12 6 0 158.33 145.91 11.98 o -10 6 0 1991.91 2142.51 57.76 o -8 6 0 2805.76 2834.34 56.74 o -6 6 0 834.63 787.74 20.28 o -4 6 0 22645.89 22815.49 114.04 o -2 6 0 13809.20 13897.00 78.14 o 0 6 0 11010.82 11741.90 67.63 o 2 6 0 13656.88 13538.40 77.10 o 4 6 0 22660.55 22483.93 113.82 o 6 6 0 948.29 906.22 21.58 o 8 6 0 2841.71 2738.10 55.85 o 10 6 0 2113.54 2136.59 58.63 o 12 6 0 149.93 183.30 16.17 o -11 7 0 350.89 344.29 15.90 o -9 7 0 1073.75 1095.05 30.46 o -7 7 0 1709.15 1689.41 43.08 o -5 7 0 1121.07 1027.60 22.08 o -3 7 0 3227.70 3399.99 45.58 o -1 7 0 2360.70 2423.34 35.41 o 1 7 0 2345.04 2327.14 34.90 o 3 7 0 3534.04 3680.80 47.60 o 5 7 0 1071.93 986.71 21.50 o 7 7 0 1737.70 1716.41 43.59 o 9 7 0 1156.63 1165.98 30.63 o 11 7 0 357.04 388.11 15.88 o -10 8 0 10.62 -2.49 11.88 o -8 8 0 1123.30 1073.42 28.26 o -6 8 0 2415.68 2377.99 48.12 o -4 8 0 3951.54 3802.42 53.80 o -2 8 0 3542.94 3494.12 46.78 o 0 8 0 15104.07 17336.42 97.31 o 2 8 0 3404.94 3324.21 45.75 o 4 8 0 3896.00 3794.38 53.10 o 6 8 0 2556.43 2546.29 49.83 o 8 8 0 1164.85 1068.82 28.68 o 10 8 0 4.34 3.70 25.23 o -11 9 0 113.69 131.37 16.07 o -9 9 0 398.08 429.85 14.89 o -7 9 0 296.00 288.08 10.53 o -5 9 0 915.66 989.83 23.27 o -3 9 0 1471.32 1617.79 36.46 o -1 9 0 1150.28 1274.31 31.27 o 1 9 0 1041.95 1142.26 30.39 o 3 9 0 1254.87 1342.63 33.80 o 5 9 0 946.85 1005.33 24.03 o 7 9 0 287.53 287.47 10.47 o 9 9 0 423.49 412.36 14.64 o 11 9 0 103.56 125.33 15.89 o -10 10 0 5.65 -20.28 27.00 o -8 10 0 801.41 831.52 28.09 o -6 10 0 784.07 808.50 24.33 o -4 10 0 705.92 646.81 20.11 o -2 10 0 105.82 122.98 7.17 o 0 10 0 420.80 420.45 13.03 o 2 10 0 62.20 73.01 6.76 o 4 10 0 703.31 656.82 20.74 o 6 10 0 627.67 631.68 18.20 o 8 10 0 783.61 734.55 22.29 o 10 10 0 7.48 12.20 28.47 o -9 11 0 287.56 319.80 15.06 o -7 11 0 1813.84 1870.82 53.71 o -5 11 0 2205.08 2175.98 50.28 o -3 11 0 483.77 497.92 13.18 o -1 11 0 1623.11 1553.46 39.79 o 1 11 0 1384.34 1402.96 36.70 o 3 11 0 435.02 424.97 13.22 o 5 11 0 2059.94 1804.62 47.24 o 7 11 0 1613.36 1645.49 35.63 o 9 11 0 246.35 241.45 14.31 o -8 12 0 1334.41 1436.63 37.29 o -6 12 0 2468.97 2580.51 58.98 o -4 12 0 1293.97 1156.86 28.63 o -2 12 0 451.67 465.61 13.72 o 0 12 0 4372.48 4359.55 64.92 o 2 12 0 455.62 457.19 13.74 o 4 12 0 1215.97 1131.69 27.46 o 6 12 0 2436.98 2267.16 57.58 o 8 12 0 1296.52 1400.31 36.47 o -9 13 0 640.72 718.90 16.12 o -7 13 0 486.17 487.59 16.89 o -5 13 0 1691.87 1685.05 50.34 o -3 13 0 2660.70 2738.06 58.65 o -1 13 0 7.95 -16.04 21.83 o 1 13 0 9.20 -9.20 9.20 o 3 13 0 2660.27 2622.83 57.50 o 5 13 0 1588.73 1574.51 34.13 o 7 13 0 483.66 442.74 16.51 o 9 13 0 622.34 640.55 22.36 o -8 14 0 535.98 603.19 21.46 o -6 14 0 94.49 135.67 12.96 o -4 14 0 1639.13 1503.43 35.13 o -2 14 0 3798.05 3588.62 68.16 o 0 14 0 539.82 487.65 15.47 o 2 14 0 3847.66 3688.03 68.63 o 4 14 0 1482.85 1338.55 33.62 o 6 14 0 81.27 99.15 12.38 o 8 14 0 559.96 589.18 21.30 o -7 15 0 15.94 18.43 14.45 o -5 15 0 75.29 77.73 12.97 o -3 15 0 104.47 87.55 12.55 o -1 15 0 213.21 202.09 12.94 o 1 15 0 261.16 276.40 13.51 o 3 15 0 75.81 53.67 12.03 o 5 15 0 85.79 87.66 12.39 o 7 15 0 27.12 6.61 15.00 o -6 16 0 8.55 -29.60 29.60 o -4 16 0 564.88 638.58 17.82 o -2 16 0 425.48 483.94 16.22 o 0 16 0 0.16 -1.18 23.82 o 2 16 0 430.42 474.20 16.13 o 4 16 0 653.45 683.68 18.09 o 6 16 0 16.07 10.15 14.08 o -5 17 0 286.67 310.74 12.61 o -3 17 0 1009.97 980.12 27.53 o -1 17 0 425.32 436.14 16.02 o 1 17 0 524.39 541.68 17.09 o 3 17 0 952.78 954.75 25.96 o 5 17 0 276.61 246.62 17.51 o -4 18 0 369.15 351.72 15.91 o -2 18 0 824.82 770.64 23.59 o 0 18 0 436.25 473.39 20.00 o 2 18 0 795.61 676.97 22.84 o 4 18 0 400.53 356.87 19.97 o -11 1 1 910.54 910.80 29.96 o -9 1 1 642.65 640.96 18.44 o -7 1 1 4084.22 3729.59 53.89 o -5 1 1 14423.67 13605.90 81.71 o -3 1 1 18755.17 17529.40 69.92 o -1 1 1 29381.82 28425.70 208.70 o 1 1 1 26631.76 25794.27 209.77 o 3 1 1 5356.48 5115.96 39.96 o 5 1 1 10269.39 9990.04 71.58 o 7 1 1 7112.49 6395.70 71.02 o 9 1 1 883.36 979.36 26.60 o 11 1 1 179.11 197.69 13.31 o -12 2 1 1049.97 1159.10 34.74 o -10 2 1 1648.89 1511.42 34.28 o -8 2 1 2638.95 2566.30 50.09 o -6 2 1 13678.83 12739.98 89.39 o -4 2 1 12086.82 12017.88 69.02 o -2 2 1 10818.21 12389.96 52.33 o 0 2 1 59674.39 65979.17 342.50 o 2 2 1 21217.94 21165.11 70.26 o 4 2 1 2764.17 2378.19 32.41 o 6 2 1 4009.17 4022.72 52.46 o 8 2 1 2480.66 2245.31 47.64 o 10 2 1 63.83 77.82 8.96 o 12 2 1 202.58 175.47 14.28 o -11 3 1 851.12 884.63 30.11 o -9 3 1 1753.25 1744.45 45.68 o -7 3 1 4437.59 4139.04 57.77 o -5 3 1 2907.47 3162.14 42.41 o -3 3 1 12195.80 12814.80 65.78 o -1 3 1 17294.24 18338.95 62.20 o 1 3 1 614.73 924.25 16.18 o 3 3 1 3088.51 2920.34 33.06 o 5 3 1 4179.67 3596.07 45.61 o 7 3 1 2197.74 2127.32 44.08 o 9 3 1 597.94 524.92 15.38 o 11 3 1 1378.18 1351.30 35.42 o -12 4 1 7.46 32.58 13.59 o -10 4 1 726.26 738.82 21.83 o -8 4 1 3063.12 2849.45 53.63 o -6 4 1 1083.14 1074.33 29.90 o -4 4 1 22136.45 22856.53 102.79 o -2 4 1 140.40 208.61 6.23 o 0 4 1 5188.92 5511.19 38.26 o 2 4 1 1352.41 1385.03 22.89 o 4 4 1 8333.21 8118.70 63.18 o 6 4 1 1668.09 1395.15 33.64 o 8 4 1 474.60 405.99 13.15 o 10 4 1 1664.84 1498.63 35.19 o 12 4 1 203.83 232.11 16.39 o -11 5 1 406.37 435.79 16.46 o -9 5 1 747.33 771.51 20.19 o -7 5 1 1525.69 1456.88 38.39 o -5 5 1 581.09 520.49 15.40 o -3 5 1 12566.87 13037.64 75.59 o -1 5 1 27791.28 30537.29 100.62 o 1 5 1 2662.63 2692.73 31.58 o 3 5 1 9949.80 9963.81 66.70 o 5 5 1 4589.28 4352.70 53.57 o 7 5 1 461.52 482.81 12.92 o 9 5 1 720.21 724.35 24.43 o 11 5 1 851.01 877.87 26.01 o -12 6 1 182.15 217.34 12.01 o -10 6 1 589.58 596.98 16.61 o -8 6 1 251.79 248.87 11.53 o -6 6 1 159.40 188.24 7.81 o -4 6 1 2117.40 2405.38 38.52 o -2 6 1 216.61 200.77 5.89 o 0 6 1 1625.91 2004.44 29.59 o 2 6 1 277.41 294.00 8.87 o 4 6 1 1008.40 987.33 27.42 o 6 6 1 40.49 32.58 6.48 o 8 6 1 94.88 112.07 9.46 o 10 6 1 201.83 185.45 13.08 o 12 6 1 70.05 67.78 15.97 o -11 7 1 380.43 425.36 16.57 o -9 7 1 2403.10 2348.17 56.96 o -7 7 1 3053.46 2933.82 55.51 o -5 7 1 3289.60 3116.61 49.31 o -3 7 1 27130.16 28395.98 126.47 o -1 7 1 3448.65 3463.24 42.06 o 1 7 1 2186.48 2393.12 35.48 o 3 7 1 19562.68 19904.41 106.66 o 5 7 1 6653.92 6309.97 69.12 o 7 7 1 783.25 775.90 18.94 o 9 7 1 1418.60 1443.49 33.37 o 11 7 1 401.76 454.53 16.82 o -10 8 1 296.95 307.60 14.47 o -8 8 1 950.28 915.29 26.43 o -6 8 1 85.46 103.36 8.03 o -4 8 1 2380.88 2419.59 43.36 o -2 8 1 1413.63 1467.91 31.26 o 0 8 1 2782.02 2868.18 41.56 o 2 8 1 5896.57 6111.18 60.99 o 4 8 1 4530.28 4857.57 60.46 o 6 8 1 288.96 283.54 9.54 o 8 8 1 1184.46 1188.63 29.95 o 10 8 1 616.11 645.29 22.63 o -11 9 1 150.44 163.27 16.71 o -9 9 1 55.10 45.25 11.38 o -7 9 1 491.85 511.48 17.12 o -5 9 1 2914.51 3046.78 53.74 o -3 9 1 1837.74 1684.43 37.80 o -1 9 1 4586.20 4578.92 55.44 o 1 9 1 9829.66 10075.80 81.20 o 3 9 1 7918.54 8060.73 77.69 o 5 9 1 969.96 940.98 23.46 o 7 9 1 2949.91 2977.97 59.28 o 9 9 1 1029.21 1032.07 31.15 o 11 9 1 40.61 54.47 14.17 o -10 10 1 39.04 49.10 12.35 o -8 10 1 165.51 176.60 12.17 o -6 10 1 942.53 955.51 26.61 o -4 10 1 1004.99 1103.67 24.54 o -2 10 1 1206.05 1136.93 32.54 o 0 10 1 3168.44 3427.38 51.33 o 2 10 1 6793.53 7097.13 75.15 o 4 10 1 1244.68 1276.67 36.65 o 6 10 1 1186.41 1157.70 28.11 o 8 10 1 1557.72 1550.59 35.05 o 10 10 1 83.09 102.78 12.64 o -9 11 1 175.60 163.03 13.80 o -7 11 1 486.78 457.76 12.69 o -5 11 1 635.39 670.45 18.72 o -3 11 1 241.69 227.23 9.13 o -1 11 1 749.63 681.04 19.81 o 1 11 1 1915.61 1888.78 42.55 o 3 11 1 304.31 314.01 9.95 o 5 11 1 114.47 115.51 9.72 o 7 11 1 535.97 557.37 17.46 o 9 11 1 130.50 127.73 13.73 o -10 12 1 35.34 25.42 16.57 o -8 12 1 728.75 733.22 24.60 o -6 12 1 128.93 159.54 10.23 o -4 12 1 498.27 507.71 13.65 o -2 12 1 526.59 486.87 16.00 o 0 12 1 1674.09 1648.70 42.40 o 2 12 1 797.16 696.59 23.13 o 4 12 1 641.11 599.84 17.98 o 6 12 1 218.22 218.72 10.76 o 8 12 1 409.38 419.03 16.07 o -9 13 1 29.20 38.48 15.90 o -7 13 1 389.22 431.36 16.48 o -5 13 1 1922.28 1854.07 51.52 o -3 13 1 302.48 296.93 10.77 o -1 13 1 2579.36 2318.83 53.46 o 1 13 1 2975.50 2766.13 56.50 o 3 13 1 1785.09 1666.69 46.75 o 5 13 1 199.94 184.71 10.52 o 7 13 1 1713.96 1642.60 39.94 o 9 13 1 262.36 283.15 18.19 o -8 14 1 227.99 246.33 18.03 o -6 14 1 379.84 403.82 15.42 o -4 14 1 1304.13 1297.59 32.42 o -2 14 1 610.28 605.12 19.98 o 0 14 1 23.77 22.42 8.80 o 2 14 1 690.39 692.87 20.24 o 4 14 1 808.97 850.53 28.32 o 6 14 1 524.42 499.79 16.56 o 8 14 1 318.98 315.17 18.80 o -7 15 1 505.16 492.00 20.10 o -5 15 1 232.15 206.14 13.90 o -3 15 1 2686.00 2697.32 64.11 o -1 15 1 2196.91 2195.20 56.58 o 1 15 1 219.89 212.64 12.64 o 3 15 1 2844.99 2705.50 62.58 o 5 15 1 1152.39 1035.13 33.38 o 7 15 1 28.30 7.02 29.52 o -6 16 1 142.96 118.27 15.90 o -4 16 1 593.19 598.32 17.84 o -2 16 1 941.28 874.80 24.65 o 0 16 1 300.23 275.49 13.73 o 2 16 1 745.90 725.88 20.10 o 4 16 1 425.34 408.72 15.78 o 6 16 1 115.95 109.65 15.37 o -5 17 1 38.78 12.83 31.91 o -3 17 1 174.54 196.27 14.79 o -1 17 1 304.83 294.93 15.42 o 1 17 1 172.02 198.38 13.89 o 3 17 1 43.58 53.90 12.55 o 5 17 1 0.49 17.28 29.09 o -4 18 1 160.03 162.18 12.41 o -2 18 1 176.22 174.39 17.08 o 0 18 1 25.83 33.66 14.99 o 2 18 1 91.37 92.24 15.98 o -12 0 2 1471.79 1460.95 38.19 o -10 0 2 3667.10 3712.45 69.26 o -8 0 2 1120.63 1100.29 24.43 o -6 0 2 10759.86 9312.07 75.00 o -4 0 2 34496.76 32350.48 109.72 o -2 0 2 18580.85 17836.28 59.16 o 0 0 2 56177.89 49684.53 267.38 o 2 0 2 104073.97 92757.07 527.32 o 4 0 2 2652.69 2664.50 33.99 o 6 0 2 6000.83 6194.75 64.27 o 8 0 2 1659.70 1757.99 44.23 o 10 0 2 1804.58 1812.28 51.93 o 12 0 2 172.16 213.32 16.42 o -13 1 2 227.98 244.04 12.28 o -11 1 2 930.79 891.56 29.96 o -9 1 2 148.67 139.52 9.94 o -7 1 2 1182.25 1051.69 31.10 o -5 1 2 10026.00 9779.71 69.86 o -3 1 2 14884.78 14665.92 65.11 o -1 1 2 25823.14 26636.28 61.67 o 1 1 2 8690.62 9842.53 40.39 o 3 1 2 6348.53 6278.07 45.66 o 5 1 2 4002.35 3357.32 43.31 o 7 1 2 4154.67 3946.00 57.31 o 9 1 2 221.10 227.61 10.24 o 11 1 2 160.32 132.46 13.01 o -12 2 2 64.68 68.46 13.25 o -10 2 2 462.10 441.24 13.78 o -8 2 2 2137.70 2050.56 45.51 o -6 2 2 2653.29 2414.72 40.74 o -4 2 2 17058.89 16428.68 80.98 o -2 2 2 14008.43 14931.37 59.15 o 0 2 2 19034.09 20876.26 58.50 o 2 2 2 6761.80 6277.05 40.98 o 4 2 2 12475.58 11890.46 72.38 o 6 2 2 5595.03 5245.10 60.27 o 8 2 2 198.65 184.47 8.62 o 10 2 2 923.96 984.03 29.83 o 12 2 2 152.11 200.84 14.07 o -11 3 2 814.59 813.60 23.95 o -9 3 2 987.94 1081.41 26.72 o -7 3 2 1811.11 1755.04 39.57 o -5 3 2 2822.39 2846.78 40.17 o -3 3 2 5552.15 5701.98 44.96 o -1 3 2 103940.16 110962.62 577.55 o 1 3 2 1690.66 2026.98 23.60 o 3 3 2 1534.17 1467.41 24.89 o 5 3 2 7134.27 7322.00 65.01 o 7 3 2 3001.00 2897.68 50.79 o 9 3 2 308.49 327.28 10.95 o 11 3 2 301.72 299.65 14.64 o -12 4 2 115.37 135.85 13.46 o -10 4 2 2097.98 2203.66 55.05 o -8 4 2 295.67 292.86 9.52 o -6 4 2 4310.01 3757.59 51.93 o -4 4 2 3783.26 3948.95 44.07 o -2 4 2 283.71 364.01 10.35 o 0 4 2 15497.40 18337.36 71.03 o 2 4 2 4041.44 4004.11 38.10 o 4 4 2 847.30 772.80 22.84 o 6 4 2 1276.86 1329.72 33.65 o 8 4 2 206.25 218.48 10.23 o 10 4 2 302.63 335.99 13.60 o 12 4 2 42.03 45.67 14.31 o -11 5 2 10.84 7.48 25.75 o -9 5 2 3387.84 3328.87 63.38 o -7 5 2 3313.40 3116.53 53.71 o -5 5 2 1308.87 1342.83 31.25 o -3 5 2 8290.94 8512.00 61.85 o -1 5 2 33569.10 36906.59 112.64 o 1 5 2 1977.67 2229.33 29.76 o 3 5 2 6106.26 6393.25 55.33 o 5 5 2 6471.50 5979.43 63.30 o 7 5 2 2933.44 2857.74 52.85 o 9 5 2 460.00 456.72 13.22 o 11 5 2 707.37 690.32 20.47 o -12 6 2 30.17 -5.69 30.62 o -10 6 2 944.52 975.58 30.63 o -8 6 2 4766.27 4810.50 71.19 o -6 6 2 4426.19 4246.93 58.82 o -4 6 2 7328.67 7295.54 65.40 o -2 6 2 50536.34 54871.57 155.86 o 0 6 2 4216.51 4127.56 41.83 o 2 6 2 1538.87 1396.91 27.14 o 4 6 2 27317.61 26602.94 126.50 o 6 6 2 5712.22 5604.18 68.73 o 8 6 2 887.68 895.23 25.70 o 10 6 2 1306.59 1380.99 35.09 o 12 6 2 299.21 312.19 19.19 o -11 7 2 38.74 74.23 12.51 o -9 7 2 867.21 886.10 27.71 o -7 7 2 1556.27 1448.71 40.87 o -5 7 2 2341.47 2349.94 43.12 o -3 7 2 2313.75 2144.28 37.52 o -1 7 2 8811.00 10314.80 71.63 o 1 7 2 3266.61 3566.91 43.10 o 3 7 2 6312.89 6212.92 61.70 o 5 7 2 1799.31 1923.99 41.32 o 7 7 2 615.69 591.74 18.03 o 9 7 2 1061.42 1034.44 30.34 o 11 7 2 273.91 286.25 17.89 o -10 8 2 108.30 148.95 13.20 o -8 8 2 222.10 215.36 10.13 o -6 8 2 4513.40 4224.35 63.20 o -4 8 2 5011.46 4883.71 60.31 o -2 8 2 2117.81 2336.92 39.22 o 0 8 2 9681.97 10232.36 76.03 o 2 8 2 16748.07 17381.34 103.39 o 4 8 2 1731.86 1506.10 36.22 o 6 8 2 1504.89 1450.69 41.16 o 8 8 2 1956.14 1931.77 51.93 o 10 8 2 537.22 573.86 19.04 o -11 9 2 92.47 111.06 16.00 o -9 9 2 603.01 619.38 18.67 o -7 9 2 204.60 181.05 9.80 o -5 9 2 1112.29 1064.89 24.17 o -3 9 2 37.89 61.50 6.52 o -1 9 2 2934.25 3073.95 46.29 o 1 9 2 203.42 212.22 7.46 o 3 9 2 1112.12 1158.61 34.17 o 5 9 2 98.86 115.12 7.86 o 7 9 2 923.03 913.53 26.95 o 9 9 2 153.15 143.38 13.16 o 11 9 2 45.68 65.86 14.73 o -10 10 2 25.54 22.18 12.27 o -8 10 2 23.47 8.89 25.42 o -6 10 2 733.11 824.22 24.19 o -4 10 2 1190.92 1187.49 35.61 o -2 10 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