# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_F_calc_maximum 398.65 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.6195 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 16.5660 _cell_length_b 17.1420 _cell_length_c 8.6720 _cell_angle_alpha 90.000 _cell_angle_beta 98.672 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4448.38 585.38 141.27 o 2 0 0 3871.06 4619.37 29.29 o 3 0 0 2104.08 2010.57 13.26 o 4 0 0 22853.39 23889.12 135.73 o 5 0 0 16249.54 16513.54 98.41 o 6 0 0 31946.58 31548.67 184.42 o 7 0 0 10012.35 9950.73 61.27 o 8 0 0 36728.61 37064.92 244.13 o 9 0 0 31674.57 31786.86 218.01 o 10 0 0 371.43 330.97 19.21 o 11 0 0 44924.61 45552.27 352.10 o 12 0 0 32609.53 30820.37 268.12 o 13 0 0 5280.07 5312.19 63.22 o 14 0 0 9265.55 8746.25 93.74 o 15 0 0 2810.41 2683.16 103.43 o 16 0 0 5586.43 5211.76 88.79 o 17 0 0 39699.62 39786.36 394.74 o 18 0 0 2276.38 2349.93 102.83 o 19 0 0 1620.26 1588.74 102.93 o 20 0 0 1273.52 1249.75 76.95 o 21 0 0 2368.27 2453.80 100.65 o 22 0 0 2843.87 2776.64 105.05 o 23 0 0 1259.72 1415.61 163.90 o 24 0 0 6.80 101.99 131.57 o 25 0 0 64.57 -109.89 215.97 o 26 0 0 1975.28 2056.20 231.84 o 1 1 0 181.78 266.23 28.42 o 2 1 0 6803.78 6344.25 28.12 o 3 1 0 1621.50 1899.85 10.66 o 4 1 0 941.35 976.83 7.10 o 5 1 0 129663.15 124973.52 908.03 o 6 1 0 19637.78 20704.37 89.63 o 7 1 0 14183.97 13442.01 59.25 o 8 1 0 3978.55 4269.86 26.33 o 9 1 0 12471.63 11703.59 62.05 o 10 1 0 1076.06 1092.41 17.37 o 11 1 0 32006.81 30872.30 174.50 o 12 1 0 25.59 44.42 15.47 o 13 1 0 2029.06 1939.84 23.76 o 14 1 0 3561.71 3449.79 51.64 o 15 1 0 256.12 439.09 45.71 o 16 1 0 2282.95 2412.05 47.60 o 17 1 0 2100.78 2065.76 47.95 o 18 1 0 731.43 804.77 43.80 o 19 1 0 2.49 45.15 42.30 o 20 1 0 2469.80 2598.67 56.57 o 21 1 0 276.50 3.23 61.97 o 22 1 0 13881.91 13198.80 133.97 o 23 1 0 1563.77 1570.07 87.52 o 24 1 0 516.37 620.94 79.54 o 25 1 0 150.28 283.67 64.02 o 26 1 0 23.53 -58.97 118.42 o 0 2 0 13990.89 13786.47 159.82 o 1 2 0 690.88 737.38 13.37 o 2 2 0 1259.80 1231.50 6.94 o 3 2 0 10942.83 10509.00 47.92 o 4 2 0 11116.40 11164.45 50.49 o 5 2 0 79.85 186.32 7.87 o 6 2 0 65047.33 65808.98 279.75 o 7 2 0 598.80 534.79 11.73 o 8 2 0 475.92 434.40 14.04 o 9 2 0 3802.00 3780.19 24.63 o 10 2 0 176.36 256.22 18.97 o 11 2 0 39352.01 39474.72 227.00 o 12 2 0 4243.06 4150.81 38.70 o 13 2 0 270.61 306.77 23.42 o 14 2 0 706.06 616.04 35.36 o 15 2 0 225.54 277.00 32.57 o 16 2 0 1095.74 1113.28 40.37 o 17 2 0 5064.08 4886.44 52.28 o 18 2 0 9936.10 9593.22 81.39 o 19 2 0 667.07 579.26 58.11 o 20 2 0 1439.51 1463.00 80.70 o 21 2 0 1174.41 1202.47 54.11 o 22 2 0 55.89 79.39 97.63 o 23 2 0 3000.43 2857.13 121.32 o 24 2 0 18.71 107.80 110.18 o 25 2 0 55.60 41.36 101.51 o 26 2 0 694.76 741.27 121.93 o 1 3 0 28371.78 28584.73 179.95 o 2 3 0 10692.49 11290.39 52.86 o 3 3 0 4450.78 4627.54 22.27 o 4 3 0 93706.10 91619.56 735.56 o 5 3 0 4868.40 5494.10 31.46 o 6 3 0 10946.77 11279.33 51.28 o 7 3 0 7068.20 6774.57 34.50 o 8 3 0 29632.46 30714.70 146.34 o 9 3 0 5067.12 5479.84 39.75 o 10 3 0 2057.09 2254.16 26.67 o 11 3 0 10965.06 10872.12 67.77 o 12 3 0 589.72 608.83 18.33 o 13 3 0 41721.04 41131.07 250.47 o 14 3 0 1690.93 1658.59 27.95 o 15 3 0 344.83 346.63 40.81 o 16 3 0 16520.06 16170.86 122.10 o 17 3 0 150.63 228.73 33.09 o 18 3 0 5877.74 5867.75 60.01 o 19 3 0 79.37 123.57 38.12 o 20 3 0 790.10 976.25 75.11 o 21 3 0 1769.70 1842.12 81.30 o 22 3 0 2.10 120.61 50.02 o 23 3 0 1213.94 1268.52 71.85 o 24 3 0 27.66 230.31 94.79 o 25 3 0 2173.88 2219.96 106.59 o 26 3 0 360.37 401.85 138.19 o 0 4 0 8207.75 8270.05 68.44 o 1 4 0 19577.85 21810.37 134.65 o 2 4 0 12682.75 13437.96 67.81 o 3 4 0 2030.52 2377.79 13.92 o 4 4 0 398.38 378.44 17.62 o 5 4 0 254.49 370.17 10.27 o 6 4 0 51.03 137.69 13.92 o 7 4 0 10899.33 11625.98 63.53 o 8 4 0 19570.06 19970.55 109.18 o 9 4 0 33076.52 33872.61 208.96 o 10 4 0 2928.55 2790.57 30.21 o 11 4 0 9.28 -5.11 18.24 o 12 4 0 287.36 310.76 28.21 o 13 4 0 83.82 117.96 23.74 o 14 4 0 1484.20 1446.03 36.91 o 15 4 0 3605.43 3640.41 52.41 o 16 4 0 26.66 58.07 30.28 o 17 4 0 2734.48 2668.44 57.01 o 18 4 0 5522.76 5460.51 59.06 o 19 4 0 7.37 40.07 54.34 o 20 4 0 832.34 864.59 39.72 o 21 4 0 3317.46 3314.76 56.23 o 22 4 0 149.91 211.15 122.30 o 23 4 0 213.72 241.74 118.71 o 24 4 0 760.32 730.18 67.52 o 25 4 0 361.89 494.90 188.79 o 26 4 0 1083.26 679.49 352.18 o 1 5 0 14440.00 15282.03 90.26 o 2 5 0 158918.28 146419.36 1341.16 o 3 5 0 4625.60 4738.27 29.74 o 4 5 0 5429.20 5907.22 33.56 o 5 5 0 25.93 40.00 6.92 o 6 5 0 5322.26 5425.79 34.78 o 7 5 0 39113.06 39330.90 204.81 o 8 5 0 6030.12 5613.66 48.65 o 9 5 0 11037.12 10332.59 71.89 o 10 5 0 33287.81 33313.13 222.43 o 11 5 0 5190.87 4940.29 56.13 o 12 5 0 502.37 517.81 30.26 o 13 5 0 2545.96 2450.62 34.94 o 14 5 0 74.29 91.88 29.69 o 15 5 0 4930.64 5042.61 76.06 o 16 5 0 34.30 63.87 39.37 o 17 5 0 1042.42 1014.55 37.91 o 18 5 0 35.37 96.91 35.90 o 19 5 0 12884.99 12562.88 106.55 o 20 5 0 231.24 184.84 55.14 o 21 5 0 722.49 783.38 66.55 o 22 5 0 36.31 113.03 46.29 o 23 5 0 420.21 500.48 161.97 o 24 5 0 3112.50 3063.82 81.17 o 25 5 0 154.12 81.90 98.56 o 26 5 0 94.97 101.68 115.39 o 0 6 0 4527.09 4850.51 55.29 o 1 6 0 452.09 655.69 13.68 o 2 6 0 80.78 111.08 12.63 o 3 6 0 65776.42 65383.19 328.70 o 4 6 0 998.60 874.85 12.09 o 5 6 0 38290.20 38072.83 201.77 o 6 6 0 225.59 180.33 12.21 o 7 6 0 10392.46 10266.53 60.75 o 8 6 0 706.22 725.14 12.83 o 9 6 0 1533.53 1463.55 19.01 o 10 6 0 2.46 4.22 20.69 o 11 6 0 10806.09 10765.33 89.58 o 12 6 0 24430.51 24348.13 175.63 o 13 6 0 7463.86 7517.81 71.12 o 14 6 0 1406.50 1393.33 41.20 o 15 6 0 2017.90 2204.86 54.22 o 16 6 0 5945.92 5957.62 56.58 o 17 6 0 542.29 551.57 52.88 o 18 6 0 1234.66 1303.89 42.66 o 19 6 0 723.19 820.29 71.92 o 20 6 0 5343.91 5259.45 80.40 o 21 6 0 201.58 72.21 81.72 o 22 6 0 43.32 110.12 59.42 o 23 6 0 98.10 104.15 97.21 o 24 6 0 4817.61 4803.08 92.02 o 25 6 0 291.20 443.96 109.20 o 1 7 0 202.78 262.07 13.07 o 2 7 0 7178.66 6764.06 42.37 o 3 7 0 1054.89 1166.93 13.54 o 4 7 0 12791.25 12724.51 79.45 o 5 7 0 1628.38 1845.64 19.55 o 6 7 0 17676.73 18192.90 116.37 o 7 7 0 2372.73 2051.58 23.71 o 8 7 0 212.31 256.25 23.56 o 9 7 0 20562.15 21017.95 154.86 o 10 7 0 8346.69 8248.23 78.51 o 11 7 0 6687.18 6257.56 70.09 o 12 7 0 142.19 164.41 45.35 o 13 7 0 220.73 255.23 44.28 o 14 7 0 302.66 444.23 37.51 o 15 7 0 34.20 95.24 26.62 o 16 7 0 1147.92 1117.07 42.36 o 17 7 0 2735.24 2641.84 73.00 o 18 7 0 3820.27 3630.95 84.70 o 19 7 0 145.35 94.66 54.89 o 20 7 0 1479.44 1551.57 60.64 o 21 7 0 248.88 394.90 50.27 o 22 7 0 99.13 -69.43 86.83 o 23 7 0 35.41 100.64 94.41 o 24 7 0 968.55 1478.52 89.44 o 25 7 0 1084.47 974.74 95.68 o 0 8 0 1230.18 1296.94 34.98 o 1 8 0 6940.46 7225.56 60.23 o 2 8 0 39862.87 38220.42 223.19 o 3 8 0 2054.73 2297.31 17.22 o 4 8 0 24443.24 24752.83 161.07 o 5 8 0 21807.68 22014.46 134.78 o 6 8 0 33338.56 33910.12 210.79 o 7 8 0 1.27 10.82 12.76 o 8 8 0 11.31 48.59 15.64 o 9 8 0 3835.79 3680.58 29.58 o 10 8 0 3543.19 3671.21 51.16 o 11 8 0 9342.31 9624.86 93.89 o 12 8 0 31.45 113.59 43.46 o 13 8 0 11594.24 11459.30 87.35 o 14 8 0 4575.87 4515.98 45.54 o 15 8 0 19199.40 19554.56 140.79 o 16 8 0 6521.96 6324.07 65.15 o 17 8 0 134.46 172.05 70.30 o 18 8 0 25.10 -29.72 61.86 o 19 8 0 1.32 127.74 103.16 o 20 8 0 693.73 815.44 62.29 o 21 8 0 6.33 236.53 101.92 o 22 8 0 1284.34 1378.50 107.92 o 23 8 0 1223.04 1408.23 116.91 o 24 8 0 514.63 643.37 141.64 o 25 8 0 413.40 295.51 146.96 o 1 9 0 4909.49 4849.69 37.06 o 2 9 0 12723.55 13383.54 88.68 o 3 9 0 9324.85 10003.63 66.19 o 4 9 0 3579.55 3316.24 28.42 o 5 9 0 4898.26 4872.05 35.25 o 6 9 0 303.63 301.31 19.48 o 7 9 0 52380.04 51807.66 412.13 o 8 9 0 693.10 637.32 26.90 o 9 9 0 12446.78 11873.41 105.87 o 10 9 0 6584.23 6337.09 71.80 o 11 9 0 3600.01 3627.98 34.91 o 12 9 0 2182.96 2186.01 36.08 o 13 9 0 4232.79 4305.90 59.58 o 14 9 0 841.55 912.64 46.70 o 15 9 0 2117.42 2075.84 38.30 o 16 9 0 4190.01 4153.41 47.44 o 17 9 0 570.02 692.40 50.77 o 18 9 0 1658.31 1657.27 46.75 o 19 9 0 7613.83 7510.31 79.68 o 20 9 0 6177.17 6294.90 147.38 o 21 9 0 279.17 316.88 87.81 o 22 9 0 125.90 292.40 87.63 o 23 9 0 41.86 -114.15 103.86 o 24 9 0 3430.91 3665.31 166.87 o 0 10 0 5081.48 5700.59 71.56 o 1 10 0 1061.89 1170.16 21.39 o 2 10 0 37719.52 38035.59 267.27 o 3 10 0 828.70 799.92 20.11 o 4 10 0 8634.92 8332.39 56.40 o 5 10 0 2780.35 2944.32 34.86 o 6 10 0 1059.35 971.68 24.49 o 7 10 0 150.46 155.37 24.76 o 8 10 0 9203.89 9145.76 80.45 o 9 10 0 9169.91 9379.16 81.27 o 10 10 0 192.98 249.44 37.80 o 11 10 0 19.63 120.84 38.53 o 12 10 0 2643.43 2437.63 44.60 o 13 10 0 1372.40 1514.01 41.54 o 14 10 0 8210.30 8266.26 77.90 o 15 10 0 5924.66 6031.91 65.48 o 16 10 0 1490.30 1533.72 52.18 o 17 10 0 486.51 616.55 88.11 o 18 10 0 520.12 603.27 60.89 o 19 10 0 2824.99 2722.82 56.24 o 20 10 0 22.88 152.26 98.62 o 21 10 0 98.56 84.25 63.43 o 22 10 0 149.32 128.18 71.87 o 23 10 0 24.14 110.71 79.62 o 24 10 0 36.95 384.50 181.73 o 1 11 0 9784.18 9925.13 79.83 o 2 11 0 2510.99 2599.64 31.96 o 3 11 0 26971.51 26896.86 159.93 o 4 11 0 5428.85 5625.02 47.87 o 5 11 0 4171.74 4484.99 54.00 o 6 11 0 217.80 279.64 26.41 o 7 11 0 11.41 65.29 23.34 o 8 11 0 658.44 594.87 22.52 o 9 11 0 8713.21 8560.17 92.32 o 10 11 0 87.94 53.77 27.88 o 11 11 0 2560.41 2709.56 43.03 o 12 11 0 1314.51 1466.12 61.70 o 13 11 0 4047.23 4050.69 48.67 o 14 11 0 13512.45 13431.57 106.40 o 15 11 0 2555.37 2581.03 59.54 o 16 11 0 6239.76 6470.95 84.81 o 17 11 0 414.67 429.72 63.99 o 18 11 0 29.07 52.39 52.36 o 19 11 0 223.89 115.66 74.76 o 20 11 0 757.84 761.94 116.52 o 21 11 0 1.28 422.09 143.85 o 22 11 0 7.93 59.06 102.22 o 23 11 0 309.03 306.39 113.53 o 24 11 0 7.44 174.48 103.85 o 0 12 0 4.67 -34.20 59.46 o 1 12 0 3906.36 4024.77 49.87 o 2 12 0 129.05 209.15 31.19 o 3 12 0 69.14 61.87 12.35 o 4 12 0 774.35 757.22 23.89 o 5 12 0 9326.35 9541.72 70.64 o 6 12 0 30564.90 30369.08 229.37 o 7 12 0 1275.37 1316.07 20.22 o 8 12 0 22040.59 22060.68 189.06 o 9 12 0 1411.66 1268.31 41.77 o 10 12 0 756.51 752.24 55.17 o 11 12 0 3074.63 3161.43 62.90 o 12 12 0 859.70 972.53 54.42 o 13 12 0 22.78 -4.75 29.48 o 14 12 0 700.76 795.50 52.61 o 15 12 0 2849.31 2936.27 80.20 o 16 12 0 1201.37 1262.17 75.44 o 17 12 0 247.21 381.40 59.16 o 18 12 0 643.46 768.38 90.67 o 19 12 0 1783.63 1873.60 97.48 o 20 12 0 4403.50 4823.47 114.97 o 21 12 0 1646.28 1959.91 80.48 o 22 12 0 59.59 123.59 128.94 o 23 12 0 2995.32 2617.94 90.69 o 1 13 0 14891.66 15149.14 118.81 o 2 13 0 7013.20 7038.62 53.66 o 3 13 0 10523.16 10174.91 71.97 o 4 13 0 16816.46 16602.06 137.93 o 5 13 0 2341.95 2241.55 38.71 o 6 13 0 1015.84 1075.13 26.60 o 7 13 0 2460.48 2504.77 51.47 o 8 13 0 2048.02 2261.05 36.30 o 9 13 0 36.83 98.95 23.10 o 10 13 0 355.23 320.34 40.27 o 11 13 0 1617.94 1638.19 49.42 o 12 13 0 2755.40 2898.26 45.01 o 13 13 0 1110.93 1165.28 56.01 o 14 13 0 4327.84 4405.23 100.22 o 15 13 0 9165.94 9211.72 81.73 o 16 13 0 1431.51 1505.64 69.47 o 17 13 0 5198.14 5286.45 78.50 o 18 13 0 18.88 -10.99 56.82 o 19 13 0 56.70 137.83 121.17 o 20 13 0 297.30 117.72 71.62 o 21 13 0 679.24 840.43 173.32 o 22 13 0 794.74 932.72 86.48 o 23 13 0 48.18 -82.27 69.65 o 0 14 0 16229.04 17033.80 174.03 o 1 14 0 6659.23 6680.05 64.61 o 2 14 0 558.99 625.48 30.55 o 3 14 0 1612.04 1463.49 34.51 o 4 14 0 56.69 49.53 31.91 o 5 14 0 16835.76 16250.73 134.01 o 6 14 0 11371.74 11267.13 89.18 o 7 14 0 2786.27 2611.73 58.05 o 8 14 0 395.20 399.50 36.18 o 9 14 0 11852.01 11828.14 155.39 o 10 14 0 4986.98 5183.36 67.33 o 11 14 0 332.36 309.82 46.36 o 12 14 0 9048.00 9179.26 85.67 o 13 14 0 480.13 531.47 33.49 o 14 14 0 599.34 671.26 62.04 o 15 14 0 440.13 450.62 61.54 o 16 14 0 168.69 164.42 76.63 o 17 14 0 8333.64 8617.02 95.38 o 18 14 0 2443.57 2510.34 82.62 o 19 14 0 730.21 1056.99 131.49 o 20 14 0 3.56 109.36 100.46 o 21 14 0 62.17 343.36 100.72 o 22 14 0 61.83 184.10 89.30 o 1 15 0 4338.20 4485.09 48.33 o 2 15 0 1486.54 1359.02 30.05 o 3 15 0 602.44 643.22 31.66 o 4 15 0 15963.36 15754.59 137.68 o 5 15 0 10707.94 10504.23 82.43 o 6 15 0 136.99 172.84 35.44 o 7 15 0 155.36 138.72 34.12 o 8 15 0 129.45 111.92 40.62 o 9 15 0 1043.09 1156.18 61.62 o 10 15 0 2280.92 2387.71 53.57 o 11 15 0 1.47 66.77 48.55 o 12 15 0 12432.85 12649.93 147.62 o 13 15 0 394.56 419.71 57.40 o 14 15 0 569.33 529.49 61.68 o 15 15 0 552.00 581.77 58.95 o 16 15 0 56.65 124.94 57.58 o 17 15 0 1261.45 1389.01 119.41 o 18 15 0 259.19 237.25 62.62 o 19 15 0 1216.23 1432.32 125.58 o 20 15 0 570.53 659.39 126.76 o 21 15 0 1239.92 1357.43 156.64 o 22 15 0 318.54 665.13 149.15 o 0 16 0 68.22 38.20 41.94 o 1 16 0 2359.34 2284.79 50.68 o 2 16 0 2788.78 2868.87 40.48 o 3 16 0 498.17 452.77 34.00 o 4 16 0 2342.09 2422.62 32.46 o 5 16 0 127.06 159.94 46.57 o 6 16 0 967.77 1119.58 41.61 o 7 16 0 6386.51 6145.40 73.47 o 8 16 0 0.04 -11.29 34.06 o 9 16 0 731.97 707.94 41.68 o 10 16 0 10738.50 10645.13 106.15 o 11 16 0 99.64 278.60 88.35 o 12 16 0 527.50 491.77 94.73 o 13 16 0 1301.83 1255.37 88.62 o 14 16 0 2421.29 2672.07 72.33 o 15 16 0 243.16 429.71 75.12 o 16 16 0 1093.64 1191.75 88.51 o 17 16 0 415.27 343.16 85.10 o 18 16 0 43.40 15.41 86.87 o 19 16 0 7.92 58.45 114.62 o 20 16 0 350.02 424.20 150.45 o 21 16 0 1010.94 1083.59 156.15 o 1 17 0 10093.09 10120.92 83.16 o 2 17 0 2623.10 2617.68 39.70 o 3 17 0 7704.44 7619.06 78.10 o 4 17 0 7730.67 7795.33 76.33 o 5 17 0 674.84 648.50 41.45 o 6 17 0 278.45 367.80 42.36 o 7 17 0 106.95 83.02 48.86 o 8 17 0 12329.03 12157.25 111.15 o 9 17 0 3389.62 3456.57 82.31 o 10 17 0 1553.82 1577.57 71.22 o 11 17 0 113.52 64.92 71.43 o 12 17 0 2675.52 2761.75 55.79 o 13 17 0 6092.22 6404.29 94.16 o 14 17 0 487.29 496.02 58.40 o 15 17 0 13.42 -19.64 86.51 o 16 17 0 348.26 486.72 90.05 o 17 17 0 936.51 951.53 183.71 o 18 17 0 582.01 721.31 122.89 o 19 17 0 293.84 299.15 145.02 o 20 17 0 1502.84 1538.91 89.59 o 0 18 0 4133.07 3760.73 73.08 o 1 18 0 1494.76 1378.66 50.29 o 2 18 0 92.85 182.24 43.24 o 3 18 0 1145.07 1033.04 28.79 o 4 18 0 607.44 556.73 52.80 o 5 18 0 921.47 855.37 79.97 o 6 18 0 34.91 10.29 43.78 o 7 18 0 951.02 977.91 52.19 o 8 18 0 272.06 323.51 57.35 o 9 18 0 3109.58 3274.73 50.85 o 10 18 0 906.54 906.41 63.12 o 11 18 0 6.15 38.47 62.56 o 12 18 0 1087.52 1211.12 59.65 o 13 18 0 23.29 -53.59 64.16 o 14 18 0 338.55 177.90 56.18 o 15 18 0 23.31 -40.98 80.98 o 16 18 0 341.56 179.52 78.16 o 17 18 0 651.74 639.12 115.56 o 18 18 0 517.99 912.26 228.23 o 19 18 0 196.88 193.05 75.16 o 20 18 0 0.03 -209.67 199.45 o 1 19 0 2414.37 2395.46 55.90 o 2 19 0 1501.59 1455.65 36.25 o 3 19 0 1090.67 1186.81 52.60 o 4 19 0 4966.31 4779.73 75.86 o 5 19 0 17.53 122.07 47.43 o 6 19 0 195.39 157.34 48.91 o 7 19 0 582.67 481.54 54.66 o 8 19 0 2.13 91.86 45.85 o 9 19 0 149.83 100.98 88.49 o 10 19 0 396.47 578.08 72.15 o 11 19 0 221.22 486.03 97.60 o 12 19 0 3280.69 3352.34 88.20 o 13 19 0 427.81 387.21 89.23 o 14 19 0 1249.21 1195.93 99.87 o 15 19 0 3721.91 3552.90 107.09 o 16 19 0 16.56 -10.56 138.70 o 17 19 0 185.82 -23.55 129.63 o 18 19 0 143.32 168.82 99.94 o 19 19 0 95.38 -57.82 195.83 o 0 20 0 3974.88 3979.07 111.59 o 1 20 0 7493.10 7468.18 71.62 o 2 20 0 554.14 519.68 62.06 o 3 20 0 83.40 53.20 35.96 o 4 20 0 6948.71 6955.12 78.96 o 5 20 0 2157.64 2125.78 52.35 o 6 20 0 236.29 201.02 51.96 o 7 20 0 10557.98 10748.88 115.32 o 8 20 0 1947.71 1983.99 88.11 o 9 20 0 84.76 63.84 60.01 o 10 20 0 12127.72 12128.88 145.18 o 11 20 0 56.42 125.96 80.71 o 12 20 0 1621.10 1471.92 93.95 o 13 20 0 34.93 -46.61 174.34 o 14 20 0 951.71 754.52 148.44 o 15 20 0 374.70 672.94 166.05 o 16 20 0 3051.73 2869.16 112.55 o 17 20 0 413.38 589.23 221.27 o 18 20 0 632.52 415.97 107.50 o 1 21 0 5454.39 5348.58 73.42 o 2 21 0 14.47 245.07 84.16 o 3 21 0 568.20 515.95 78.61 o 4 21 0 781.62 849.74 79.93 o 5 21 0 974.11 969.44 108.54 o 6 21 0 93.89 -23.33 53.33 o 7 21 0 211.57 163.29 89.80 o 8 21 0 396.03 383.85 114.50 o 9 21 0 567.07 621.16 93.21 o 10 21 0 4.15 -64.67 61.47 o 11 21 0 25.31 237.35 74.26 o 12 21 0 2288.42 2297.05 79.62 o 13 21 0 1708.76 1714.91 164.92 o 14 21 0 185.84 450.71 146.96 o 15 21 0 2021.85 2234.83 142.54 o 16 21 0 614.00 790.10 205.60 o 17 21 0 5.17 -63.82 223.80 o 0 22 0 3853.63 3766.03 80.82 o 1 22 0 6462.67 6531.74 89.25 o 2 22 0 1461.53 1522.99 92.62 o 3 22 0 732.53 911.38 78.09 o 4 22 0 2870.63 2784.89 80.17 o 5 22 0 199.65 213.61 48.90 o 6 22 0 298.83 396.72 128.56 o 7 22 0 2376.43 2213.85 83.28 o 8 22 0 3631.22 3485.71 135.76 o 9 22 0 162.26 -57.85 86.10 o 10 22 0 7625.73 7721.10 109.23 o 11 22 0 4010.63 4412.36 120.01 o 12 22 0 531.30 804.58 152.36 o 13 22 0 530.58 335.69 76.06 o 14 22 0 9.55 -27.81 162.64 o 15 22 0 656.09 845.29 94.48 o 16 22 0 104.23 -69.04 141.50 o 1 23 0 208.51 45.10 47.03 o 2 23 0 53.29 88.87 63.91 o 3 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