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Acta Cryst. (2005). E61, m1701-m1704  [ doi:10.1107/S1600536805024220 ]

trans-Chloro[(E)-1,1,1,4,4,4-hexafluorobut-2-en-2-yl]bis(tricyclohexylphosphine)platinum(II)-trans-chloro[(Z)-1,1,1,4,4,4-hexafluorobut-2-en-2yl]bis(tricyclohexylphosphine)platinum(II) (1/1) at 120 K

R. A. Howie and J. L. Wardell

Online 6 August 2005

Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level A
PLAT241_ALERT_2_A Check High      Ueq as Compared to Neighbors for        F4A
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT241_ALERT_2_A Check High      Ueq as Compared to Neighbors for        F5A
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 

Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.64 Ratio 
PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for       C24B
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for       C36B
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for       C36A     


Alert level C
PLAT215_ALERT_3_C Disordered F5A     has ADP max/min Ratio .......       3.20       
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.60 Ratio 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for       C20B
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for       C33B
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for       C35A
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for       C35B
Author Response: ... This problem which also applies to F5A and to a lesser extent to other atoms as well is, as implied in the text of the 'publ section exptl refinement', attibuted to the obvious and comparatively extreme disorder in the 'average' molecule. 
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        F6B     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for       C19A     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for       C19B     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for       C21A     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for       C38A     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C39     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      25.00 Perc. 
PLAT411_ALERT_2_C Short Inter H...H Contact  H11B   ..  H17A    ..       2.10 Ang.  
PLAT412_ALERT_2_C Short Intra XH3 .. XHn     H20D   ..  H30B    ..       1.84 Ang.  


   2 ALERT level A = In general: serious problem
   4 ALERT level B = Potentially serious problem
  15 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  18 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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