# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' la-l3-fe in P 1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 181.30 _exptl_crystal_F_000 582.00 _reflns_d_resolution_high 0.7704 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' _cell_length_a 10.8815 _cell_length_b 11.0081 _cell_length_c 11.7412 _cell_angle_alpha 69.229 _cell_angle_beta 77.892 _cell_angle_gamma 68.091 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -4 -7 -15 145.75 122.17 24.19 o -3 -7 -15 336.34 369.85 25.47 o -5 -6 -15 298.84 293.50 31.20 o -4 -6 -15 11.93 -0.08 22.85 o -3 -6 -15 363.67 371.54 24.99 o -2 -6 -15 521.62 560.41 26.54 o -5 -5 -15 509.86 505.09 36.10 o -4 -5 -15 118.42 81.90 23.59 o -3 -5 -15 129.69 159.42 47.25 o -2 -5 -15 618.92 688.79 27.48 o -1 -5 -15 238.46 297.17 24.87 o -4 -4 -15 206.23 207.75 29.30 o -3 -4 -15 21.32 18.85 23.56 o -1 -4 -15 354.65 435.39 26.79 o -3 -3 -15 67.25 21.14 16.22 o -2 -3 -15 103.11 118.78 24.94 o -7 -9 -14 285.11 238.11 14.71 o -6 -9 -14 315.44 317.05 85.14 o -5 -9 -14 79.46 118.18 22.04 o -4 -9 -14 32.64 59.05 21.79 o -3 -9 -14 238.18 350.59 23.16 o -2 -9 -14 198.00 259.75 23.24 o -7 -8 -14 93.36 70.05 17.69 o -6 -8 -14 680.39 642.07 81.10 o -5 -8 -14 178.59 179.89 45.24 o -4 -8 -14 22.94 40.13 20.82 o -3 -8 -14 283.22 261.31 22.98 o -2 -8 -14 324.52 332.31 23.76 o -1 -8 -14 78.34 136.10 21.81 o 0 -8 -14 115.58 112.15 22.90 o -8 -7 -14 541.61 538.34 44.08 o -7 -7 -14 16.45 57.01 14.32 o -6 -7 -14 369.55 374.65 53.73 o -5 -7 -14 518.55 526.65 23.42 o -4 -7 -14 47.98 32.01 20.91 o -3 -7 -14 252.96 269.40 22.04 o -2 -7 -14 674.75 665.41 24.38 o -1 -7 -14 338.59 436.63 46.15 o 0 -7 -14 12.55 -14.57 21.54 o 1 -7 -14 212.34 250.69 22.89 o -8 -6 -14 431.02 470.28 41.53 o -7 -6 -14 280.83 287.49 19.68 o -6 -6 -14 70.09 65.46 14.24 o -5 -6 -14 456.98 460.88 86.22 o -4 -6 -14 323.76 423.68 21.98 o -3 -6 -14 22.07 -1.06 20.44 o -2 -6 -14 507.09 536.23 23.59 o -1 -6 -14 696.86 689.37 24.55 o 0 -6 -14 125.63 124.74 22.45 o 1 -6 -14 137.90 113.57 22.98 o -7 -5 -14 215.56 259.90 27.58 o -6 -5 -14 20.89 64.58 13.99 o -5 -5 -14 264.84 237.05 14.65 o -4 -5 -14 581.10 648.32 23.56 o -3 -5 -14 143.20 93.89 21.75 o -2 -5 -14 177.50 181.63 21.56 o -1 -5 -14 733.35 795.06 24.96 o 0 -5 -14 186.10 245.79 22.82 o 2 -5 -14 425.95 479.89 25.95 o -7 -4 -14 317.89 380.54 18.79 o -6 -4 -14 54.48 45.30 14.71 o -5 -4 -14 105.57 120.73 60.08 o -4 -4 -14 658.71 643.95 74.74 o -3 -4 -14 200.40 185.01 21.99 o -2 -4 -14 102.37 61.10 22.08 o -1 -4 -14 497.04 568.99 23.98 o 0 -4 -14 363.65 445.08 23.50 o 1 -4 -14 0.33 0.16 22.49 o 2 -4 -14 101.47 148.89 23.40 o -7 -3 -14 619.70 592.61 27.18 o -6 -3 -14 243.53 277.36 15.64 o -5 -3 -14 7.12 -12.29 14.83 o -4 -3 -14 482.72 451.54 56.89 o -3 -3 -14 625.32 712.38 24.64 o -2 -3 -14 9.45 16.31 21.65 o -1 -3 -14 174.01 192.78 22.29 o 0 -3 -14 448.27 523.75 24.54 o 1 -3 -14 167.15 211.76 23.89 o 2 -3 -14 41.31 65.16 22.91 o -6 -2 -14 441.77 504.68 35.75 o -5 -2 -14 34.28 15.90 22.50 o -4 -2 -14 199.70 201.75 15.89 o -3 -2 -14 574.65 589.36 22.23 o -2 -2 -14 173.28 175.99 23.81 o -1 -2 -14 6.56 17.25 22.21 o 0 -2 -14 332.82 319.49 24.09 o 1 -2 -14 405.23 411.58 24.84 o 2 -2 -14 25.76 57.76 23.24 o -5 -1 -14 216.31 277.75 16.57 o -4 -1 -14 22.48 47.24 25.52 o -3 -1 -14 414.16 428.27 28.18 o -2 -1 -14 473.62 445.56 40.34 o -1 -1 -14 1.89 -1.59 22.81 o 0 -1 -14 24.78 3.45 23.17 o 1 -1 -14 297.89 254.95 48.21 o 2 -1 -14 120.96 135.14 23.62 o -3 0 -14 285.84 270.92 55.08 o -2 0 -14 324.64 413.48 24.87 o -1 0 -14 152.60 169.46 41.36 o 0 0 -14 245.59 275.66 24.13 o 1 0 -14 142.62 135.30 25.05 o -6 -11 -13 225.52 275.15 45.38 o -5 -11 -13 55.41 106.02 21.33 o -4 -11 -13 75.61 68.68 22.12 o -3 -11 -13 300.16 331.71 23.47 o -8 -10 -13 106.95 106.40 25.16 o -7 -10 -13 195.73 205.73 21.83 o -6 -10 -13 260.24 276.54 22.31 o -5 -10 -13 374.54 361.62 22.50 o -4 -10 -13 3.02 20.35 20.22 o -3 -10 -13 307.57 295.06 22.28 o -2 -10 -13 628.74 604.53 23.77 o -1 -10 -13 89.38 119.83 41.55 o -9 -9 -13 446.86 439.09 15.78 o -8 -9 -13 389.47 361.67 15.05 o -7 -9 -13 24.13 4.53 40.54 o -6 -9 -13 445.28 510.95 21.84 o -5 -9 -13 609.65 608.99 22.36 o -4 -9 -13 223.13 243.23 21.23 o -3 -9 -13 96.08 130.78 20.16 o -2 -9 -13 363.86 432.38 22.09 o -1 -9 -13 299.94 350.98 43.81 o 0 -9 -13 15.22 34.10 20.60 o -9 -8 -13 146.55 154.32 24.94 o -8 -8 -13 592.18 638.56 62.07 o -7 -8 -13 201.61 200.89 14.38 o -6 -8 -13 138.81 137.00 25.23 o -5 -8 -13 873.32 930.33 24.35 o -4 -8 -13 470.11 476.16 22.03 o -3 -8 -13 30.40 17.04 19.33 o -2 -8 -13 325.13 330.53 20.85 o -1 -8 -13 338.14 418.84 41.60 o 0 -8 -13 16.15 20.29 19.18 o 1 -8 -13 127.70 187.87 20.74 o 2 -8 -13 387.67 399.33 22.56 o -9 -7 -13 15.52 29.50 19.11 o -8 -7 -13 651.29 624.36 18.68 o -7 -7 -13 362.53 423.79 21.50 o -6 -7 -13 4.51 13.22 15.49 o -5 -7 -13 427.54 489.50 21.26 o -4 -7 -13 580.94 699.10 41.41 o -3 -7 -13 52.81 100.64 19.21 o -2 -7 -13 311.55 276.76 20.67 o -1 -7 -13 638.09 727.49 22.64 o 0 -7 -13 285.95 340.94 20.61 o 1 -7 -13 21.23 54.19 19.50 o 2 -7 -13 265.69 294.92 21.75 o -9 -6 -13 37.90 21.53 14.82 o -8 -6 -13 529.08 550.95 15.46 o -7 -6 -13 830.54 766.22 38.78 o -6 -6 -13 176.46 186.00 18.92 o -5 -6 -13 227.06 236.89 19.40 o -4 -6 -13 534.20 508.24 20.74 o -3 -6 -13 302.48 311.72 19.63 o -2 -6 -13 10.52 33.81 18.56 o -1 -6 -13 563.98 573.78 21.42 o 0 -6 -13 662.11 677.24 22.92 o 1 -6 -13 207.90 251.97 21.06 o 2 -6 -13 213.62 210.75 21.70 o 3 -6 -13 506.78 542.91 22.78 o -9 -5 -13 122.86 133.84 20.16 o -8 -5 -13 421.89 442.39 15.13 o -7 -5 -13 901.40 928.79 16.29 o -6 -5 -13 343.63 360.71 24.97 o -5 -5 -13 15.33 24.03 20.07 o -4 -5 -13 872.43 989.35 21.96 o -3 -5 -13 726.74 755.60 21.93 o -2 -5 -13 227.34 273.47 19.47 o -1 -5 -13 129.03 157.30 19.43 o 0 -5 -13 587.80 638.45 43.80 o 1 -5 -13 383.86 491.60 21.82 o 2 -5 -13 4.75 20.38 20.53 o 3 -5 -13 440.26 507.52 23.54 o 4 -5 -13 269.80 332.52 22.82 o -9 -4 -13 248.61 255.54 14.69 o -8 -4 -13 70.28 99.06 30.83 o -7 -4 -13 812.25 876.66 26.42 o -6 -4 -13 575.06 626.90 56.09 o -5 -4 -13 98.62 112.13 18.53 o -4 -4 -13 235.81 248.71 20.07 o -3 -4 -13 610.51 671.67 21.74 o -2 -4 -13 522.39 574.31 21.52 o -1 -4 -13 63.31 63.86 19.39 o 0 -4 -13 497.69 597.98 22.91 o 1 -4 -13 321.75 409.46 44.01 o 2 -4 -13 46.27 60.65 20.41 o 3 -4 -13 157.64 144.48 22.66 o 4 -4 -13 469.48 431.13 24.59 o -8 -3 -13 0.41 28.33 24.12 o -7 -3 -13 402.17 426.02 16.96 o -6 -3 -13 707.26 706.81 16.36 o -5 -3 -13 291.80 302.18 14.29 o -4 -3 -13 60.01 65.05 13.13 o -3 -3 -13 1073.16 1239.50 24.75 o -2 -3 -13 232.38 297.07 20.42 o -1 -3 -13 106.89 126.21 19.79 o 0 -3 -13 260.68 300.00 21.38 o 1 -3 -13 542.89 602.27 23.26 o 2 -3 -13 102.47 187.41 42.24 o 3 -3 -13 52.88 19.56 42.96 o 4 -3 -13 400.99 444.52 47.75 o -8 -2 -13 174.66 190.19 14.59 o -7 -2 -13 36.49 31.43 21.08 o -6 -2 -13 623.42 642.18 16.97 o -5 -2 -13 537.52 521.50 34.87 o -4 -2 -13 42.78 40.80 14.15 o -3 -2 -13 595.27 605.49 62.39 o -2 -2 -13 622.72 645.57 22.93 o -1 -2 -13 7.55 19.34 20.36 o 0 -2 -13 7.36 3.08 20.32 o 1 -2 -13 471.59 563.37 22.74 o 2 -2 -13 698.18 672.61 24.35 o 3 -2 -13 3.29 12.53 21.49 o 4 -2 -13 206.96 200.87 23.82 o -7 -1 -13 31.09 45.12 14.38 o -6 -1 -13 229.29 233.07 15.67 o -5 -1 -13 575.41 624.62 60.92 o -4 -1 -13 44.13 64.11 14.29 o -3 -1 -13 190.27 225.77 21.16 o -2 -1 -13 507.66 553.60 22.54 o -1 -1 -13 416.50 448.83 22.33 o 0 -1 -13 1.09 -11.09 20.28 o 1 -1 -13 66.41 62.64 20.94 o 2 -1 -13 497.85 509.96 24.03 o 3 -1 -13 119.60 118.70 21.74 o 4 -1 -13 90.17 125.23 22.12 o -6 0 -13 73.77 65.27 15.33 o -5 0 -13 643.21 650.90 53.35 o -4 0 -13 211.45 206.83 15.05 o -3 0 -13 10.15 16.35 14.34 o -2 0 -13 261.79 306.40 23.73 o -1 0 -13 764.80 819.83 24.50 o 0 0 -13 105.05 89.06 20.39 o 1 0 -13 177.03 230.03 43.17 o 2 0 -13 454.82 461.48 24.56 o 3 0 -13 270.59 341.62 24.63 o 4 0 -13 3.49 16.25 23.01 o -5 1 -13 365.07 360.34 16.50 o -4 1 -13 580.71 603.15 17.15 o -3 1 -13 11.81 19.39 22.04 o -2 1 -13 117.13 117.17 14.56 o -1 1 -13 359.69 332.53 28.13 o 0 1 -13 500.31 469.54 24.02 o 1 1 -13 26.08 69.94 22.42 o 2 1 -13 700.48 812.87 25.77 o 3 1 -13 538.51 594.84 26.35 o -3 2 -13 290.46 307.48 16.78 o -2 2 -13 16.66 41.58 32.06 o -1 2 -13 328.09 312.28 17.18 o 0 2 -13 524.70 563.91 47.72 o 1 2 -13 84.97 58.82 48.43 o 2 2 -13 147.00 163.36 24.78 o -6 -12 -12 300.25 409.82 23.89 o -5 -12 -12 333.29 296.93 22.60 o -4 -12 -12 7.65 21.83 21.48 o -8 -11 -12 345.68 366.94 42.76 o -7 -11 -12 40.60 48.48 20.53 o -6 -11 -12 154.70 146.38 22.10 o -5 -11 -12 459.95 477.32 22.56 o -4 -11 -12 79.93 116.04 20.22 o -3 -11 -12 125.27 117.81 21.40 o -2 -11 -12 415.32 532.05 22.65 o -1 -11 -12 139.95 161.20 20.71 o -9 -10 -12 512.47 632.25 32.84 o -8 -10 -12 961.96 1024.38 64.72 o -7 -10 -12 97.01 125.11 20.59 o -6 -10 -12 151.37 148.76 19.77 o -5 -10 -12 666.53 755.31 23.21 o -4 -10 -12 276.19 300.72 20.24 o -3 -10 -12 9.72 -18.97 18.97 o -2 -10 -12 294.65 265.44 20.94 o -1 -10 -12 430.10 500.11 21.23 o 0 -10 -12 111.96 136.77 19.72 o 1 -10 -12 83.68 43.77 19.00 o -10 -9 -12 243.65 255.04 24.98 o -9 -9 -12 273.39 303.96 47.31 o -8 -9 -12 669.15 668.21 81.64 o -7 -9 -12 330.52 319.17 19.99 o -6 -9 -12 18.15 6.21 18.15 o -5 -9 -12 593.38 641.42 21.26 o -4 -9 -12 878.46 888.25 41.40 o -3 -9 -12 177.31 223.22 19.19 o -2 -9 -12 108.17 136.90 19.18 o -1 -9 -12 482.98 549.98 21.60 o 0 -9 -12 294.04 342.67 20.55 o 1 -9 -12 5.50 20.26 18.08 o 2 -9 -12 399.51 357.71 20.70 o -10 -8 -12 198.18 216.05 27.56 o -9 -8 -12 40.16 60.62 16.83 o -8 -8 -12 505.53 520.73 52.69 o -7 -8 -12 475.69 488.56 41.97 o -6 -8 -12 86.56 93.45 14.33 o -5 -8 -12 234.65 222.46 18.30 o -4 -8 -12 1249.05 1211.65 22.53 o -3 -8 -12 779.79 855.52 21.15 o -2 -8 -12 38.10 53.61 17.74 o -1 -8 -12 439.96 446.36 19.52 o 0 -8 -12 599.26 647.45 21.03 o 1 -8 -12 25.48 -5.28 18.73 o 2 -8 -12 291.38 315.22 19.05 o 3 -8 -12 395.71 371.82 21.11 o -10 -7 -12 438.51 522.52 19.31 o -9 -7 -12 2.79 32.84 12.65 o -8 -7 -12 310.39 306.16 19.65 o -7 -7 -12 532.19 520.37 32.10 o -6 -7 -12 376.56 350.54 47.14 o -5 -7 -12 139.65 178.17 16.88 o -4 -7 -12 599.51 621.95 19.19 o -3 -7 -12 851.59 960.91 20.82 o -2 -7 -12 95.92 107.97 17.57 o -1 -7 -12 179.26 208.98 17.87 o 1 -7 -12 423.77 447.01 38.48 o 2 -7 -12 31.87 50.20 35.96 o 3 -7 -12 306.46 320.30 39.12 o 4 -7 -12 276.16 240.01 20.80 o -10 -6 -12 689.59 716.97 15.41 o -9 -6 -12 168.40 191.30 13.11 o -8 -6 -12 104.37 141.71 21.96 o -7 -6 -12 681.60 684.60 76.92 o -6 -6 -12 920.74 931.11 20.19 o -5 -6 -12 29.72 32.35 16.52 o -4 -6 -12 273.67 292.40 18.06 o -3 -6 -12 635.24 665.75 19.33 o -2 -6 -12 388.43 427.58 18.96 o -1 -6 -12 115.75 166.70 17.54 o 0 -6 -12 476.89 589.94 39.09 o 1 -6 -12 1080.04 1219.37 22.83 o 2 -6 -12 95.97 96.11 19.07 o 3 -6 -12 141.56 170.09 18.97 o 4 -6 -12 452.00 470.78 40.65 o -10 -5 -12 487.81 469.73 14.98 o -9 -5 -12 650.23 699.34 16.87 o -8 -5 -12 26.39 33.56 12.43 o -7 -5 -12 376.17 433.26 44.57 o -6 -5 -12 917.54 902.15 65.81 o -5 -5 -12 312.64 281.35 23.19 o -4 -5 -12 138.58 163.22 16.93 o -3 -5 -12 565.47 608.07 36.51 o -2 -5 -12 1024.61 1085.42 21.89 o -1 -5 -12 139.63 205.74 17.79 o 0 -5 -12 401.72 447.11 37.52 o 1 -5 -12 622.52 595.63 21.74 o 2 -5 -12 457.05 510.58 21.26 o 3 -5 -12 11.10 -0.86 19.23 o 4 -5 -12 440.72 458.92 21.48 o 5 -5 -12 269.74 365.47 41.41 o -10 -4 -12 199.13 212.75 13.68 o -9 -4 -12 656.55 653.78 14.46 o -8 -4 -12 339.04 362.53 20.64 o -7 -4 -12 152.95 191.31 12.39 o -6 -4 -12 971.98 1023.33 98.47 o -5 -4 -12 438.51 441.90 12.72 o -4 -4 -12 3.69 21.36 17.04 o -3 -4 -12 117.72 146.76 17.77 o -2 -4 -12 645.99 727.13 20.56 o -1 -4 -12 655.26 729.22 20.81 o 0 -4 -12 22.84 -2.69 36.24 o 1 -4 -12 1099.38 1171.28 24.14 o 2 -4 -12 521.18 563.10 21.85 o 3 -4 -12 15.84 44.71 19.13 o 4 -4 -12 257.81 254.89 20.66 o 5 -4 -12 547.42 635.83 22.60 o -9 -3 -12 426.71 465.04 13.89 o -8 -3 -12 331.51 347.70 16.64 o -7 -3 -12 24.67 45.03 12.34 o -6 -3 -12 708.46 664.73 15.23 o -5 -3 -12 570.29 558.23 68.13 o -4 -3 -12 181.37 195.68 17.42 o -3 -3 -12 221.73 256.72 18.89 o -2 -3 -12 496.93 558.55 20.19 o -1 -3 -12 858.88 1024.73 21.49 o 0 -3 -12 25.60 74.06 17.79 o 1 -3 -12 589.70 619.80 20.96 o 2 -3 -12 954.09 996.26 23.60 o 3 -3 -12 85.39 138.64 19.80 o 4 -3 -12 102.90 124.01 20.07 o 5 -3 -12 676.01 723.36 23.37 o -9 -2 -12 193.22 217.92 30.90 o -8 -2 -12 399.56 418.00 24.02 o -7 -2 -12 53.87 79.22 16.28 o -6 -2 -12 270.21 269.82 13.37 o -5 -2 -12 579.04 618.44 42.68 o -4 -2 -12 219.19 271.55 18.48 o -3 -2 -12 28.42 4.17 18.60 o -2 -2 -12 2226.35 2470.19 46.58 o -1 -2 -12 663.78 731.00 22.08 o 0 -2 -12 94.80 105.64 18.61 o 2 -2 -12 1162.75 1152.03 23.08 o 3 -2 -12 621.42 647.15 21.72 o 4 -2 -12 13.66 29.67 19.25 o 5 -2 -12 334.34 323.44 42.55 o 6 -2 -12 604.87 562.07 23.90 o -8 -1 -12 610.51 635.37 50.51 o -7 -1 -12 314.80 334.63 24.75 o -6 -1 -12 12.79 26.04 13.28 o -5 -1 -12 510.01 537.18 46.13 o -4 -1 -12 459.91 508.43 14.16 o -3 -1 -12 25.29 27.64 16.37 o -2 -1 -12 196.31 213.92 18.91 o -1 -1 -12 1914.38 2007.24 25.16 o 0 -1 -12 457.27 531.30 19.76 o 1 -1 -12 3.70 5.51 17.90 o 2 -1 -12 620.63 545.74 21.45 o 5 -1 -12 234.14 269.13 20.92 o 6 -1 -12 462.58 435.30 23.40 o -8 0 -12 298.59 285.59 20.33 o -7 0 -12 490.12 495.29 15.17 o -6 0 -12 94.80 109.31 25.46 o -5 0 -12 139.51 142.30 13.88 o -4 0 -12 613.57 607.44 14.71 o -3 0 -12 306.41 320.97 13.73 o -2 0 -12 12.65 -2.20 12.61 o -1 0 -12 345.52 412.61 19.53 o 0 0 -12 1415.10 1440.40 24.93 o 1 0 -12 251.87 236.93 19.97 o 2 0 -12 277.20 308.32 21.09 o 3 0 -12 862.71 859.77 24.94 o 4 0 -12 300.76 325.28 22.64 o 5 0 -12 12.88 3.71 22.23 o 6 0 -12 352.93 401.73 24.15 o -7 1 -12 419.29 418.13 15.11 o -6 1 -12 205.80 240.80 14.43 o -5 1 -12 1.99 21.11 28.82 o -4 1 -12 330.83 399.87 28.02 o -3 1 -12 599.02 558.32 43.25 o -2 1 -12 155.07 171.47 21.94 o -1 1 -12 55.40 72.63 13.30 o 0 1 -12 471.91 516.19 21.43 o 1 1 -12 434.10 470.41 43.38 o 2 1 -12 33.77 12.08 21.54 o 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