O,O-Bis(2-tert-butyl-4-methoxy­phen­yl) chloro­thio­phospho­nate. Corrigendum.

Odabaşoğlu, M.; Büyükgüngör, O.; Albayrak, C.

doi:10.1107/S1600536805027789

addenda and errata

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 61| Part 10| October 2005| Pages e4-e5

doi:10.1107/S1600536805027789

O,O-Bis(2-tert-butyl-4-methoxyphenyl) chlorothiophosphonate. Corrigendum.

Mustafa Odabaşoğlu,^a ^* Orhan Büyükgüngör ^b and Çiğdem Albayrak ^a

^aDepartment of Chemistry, Ondokuz Mayıs University, TR-55139 Samsun, Turkey, and ^bDepartment of Physics, Ondokuz Mayıs University, TR-55139 Samsun, Turkey
^*Correspondence e-mail: orhanb@omu.edu.tr

(Received 8 August 2005; accepted 5 September 2005; online 17 September 2005)

In the original report by Odabaşoğlu, Büyükgüngör & Albayrak [Acta Cryst. (2005), E61, o2528–o2530], the structure was reported in the incorrect space group Cc. The structure is now reported as disordered in the correct space group C2/c. The P atom lies on a twofold rotation axis.A revised description of the hydrogen bonding is also given.

1. Comment

An ORTEP-3 (Farrugia, 1997 ) view of (I) and a packing diagram are shown in Figs. 1 and 2, respectively. The P atom lies on a twofold rotation axis, eading to disorder of the Cl and S atoms. Compound (I) has no classical hydrogen bonds, but there are two C—H⋯π interactions: H8A⋯Cg1= 3.12 (2) Å and C8—H8A⋯Cg1 = 122.8 (2)° (Cg1 is the centroid of the C1ⁱⁱ–C6ⁱⁱ ring), and H11A⋯Cg2 = 2.71 (2) Å and C11—H11A⋯Cg2 = 142.7 (1)° (Cg2 is the centroid of the C1ⁱⁱⁱ–C6ⁱⁱⁱ ring) [symmetry codes: (ii) x, 1 − y, $[{1\over 2}]$ + z; (iii) $[{1\over 2}]$ − x, $[{1\over 2}]$ − y, − z]. The dihedral angle between the symmetry-related benzene rings is 41.2 (2)°. Selected bond distances and angles are given in Table 1.

Figure 1
A view of (I), with the atom-numbering scheme and 50% probability displacement ellipsoids·[Symmetry code: (i) −x + 1, y, −z + $[{1\over 2}]$ ]

Figure 2
A view of the packing of (I); C—H⋯π interactions are drawn as dashed lines.

2. Experimental

2.1.1. Crystal data

C₂₂H₃₀ClO₄PS
M_r = 456.94
Monoclinic, C 2/c
a = 23.592 (3) Å
b = 8.3111 (6) Å
c = 12.5067 (14) Å
β = 105.740 (9)°
V = 2360.3 (4) Å³
Z = 4
D_x = 1.286 Mg m⁻³
Mo Kα radiation
Cell parameters from 16485 reflections
θ = 1.7–26.7°
μ = 0.34 mm⁻¹
T = 150 K
Prism, colorless
0.64 × 0.59 × 0.55 mm

2.1.2. Data collection

Stoe IPDS-II diffractometer
ω scans
Absorption correction: integration(X-RED32; Stoe & Cie, 2002 )T_min = 0.824, T_max = 0.869
16485 measured reflections
2327 independent reflections
2146 reflections with I > 2σ(I)
R_int = 0.032
θ_max = 26.0°
h = −28 → 28
k = −10 → 10
l = −15 → 15

2.1.3. Refinement

Refinement on F²
R[F² > 2σ(F²)] = 0.028
wR(F²) = 0.073
S = 1.08
2327 reflections
192 parameters
All H-atom parameters refined
w = 1/[σ²(F_o²) + (0.0362P)² + 1.6163P] where P = (F_o² + 2F_c²)/3
(Δ/σ)_max = 0.002
Δρ_max = 0.17 e Å⁻³
Δρ_min = −0.34 e Å⁻³

Table 1
Selected geometric parameters (Å, °)

C1—C2	1.3946 (18)
C1—C6	1.4086 (17)
C1—O1	1.4226 (14)
C2—C3	1.3860 (18)
C3—C4	1.3979 (18)
C4—C5	1.4017 (19)
C5—C6	1.4088 (18)
O1—P1	1.5750 (9)
P1—S1ⁱ	1.9791 (4)
P1—Cl1	1.9791 (4)

C2—C1—C6	123.25 (11)
C2—C1—O1	119.13 (11)
C6—C1—O1	117.58 (11)
C3—C2—C1	119.77 (12)
C2—C3—C4	119.11 (12)
C3—C4—C5	120.39 (11)
C4—C5—C6	121.99 (12)
C1—C6—C5	115.48 (11)
O1—P1—O1ⁱ	97.08 (7)
O1—P1—S1ⁱ	111.27 (4)
O1—P1—Cl1	111.44 (3)
S1ⁱ—P1—Cl1	113.26 (3)
Symmetry code: (i) $[-x+1, y, -z+{\script{1\over 2}}]$ .

All H atoms were refined freely. Atoms S1 and Cl1 were assigned to the same atomic site and refined freely with the same atomic coordinates and with fixed site-occupancy factors of 0.5.

Data collection: X-AREA (Stoe & Cie, 2002); cell refinement: X-AREA; data reduction: X-RED32 (Stoe & Cie, 2002); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997 ); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 for Windows (Farrugia, 1997); software used to prepare material for publication: WinGX (Farrugia, 1999 ).

Supporting information

Crystal structure: contains datablocks global, I. DOI: 10.1107/S1600536805027789/bt6713sup1.cif

Structure factors: contains datablock I. DOI: 10.1107/S1600536805027789/bt6713Isup2.hkl

Comment top

An ORTEP-3 (Farrugia, 1997) view of (I) and a packing diagram are shown in Figs. 1 and 2, respectively. Compound (I) has no classical hydrogen bonds but there are two C—H···π interactions: H8A···Cg1= 3.12 (2) Å and C8—H8A···Cg1 = 122.8 (2)° [Cg1 is the centroid of the C1ⁱ–C6ⁱ ring; and H11A···Cg2 = 2.71 (2) Å and C11—H11A···Cg2 = 142.7 (1)° (Cg2 is the centroid of the C1ⁱⁱ–C6ⁱⁱ ring); symmetry codes: (i) x, 1 − y, 1/2 + z; (ii) 1/2 − x, 1/2 − y, − z]. The dihedral angle between the symmetry-related benzene rings in (I) is 41.2 (2)°. Selected bond distances and angles for (I) are given in Table 1. The benzene ring is planar, with a maximum deviation from the plane defined by the six ring atoms of 0.007 (1) Å (for C3).

Experimental top

Compound (I) was prepared by the method of Odabaşoǧlu et al. (2005), using 2-tert-butyl-4-methoxyphenol and PSCl₃ as starting materials. Crystals of (I) suitable for single-crystal X-ray diffraction were grown by slow evaporation of a solution in n-hexane (yield 77%, m.p. 423 K). Analysis calculated: C 57.83, H 6.57%; found: C 57.36, H 6.38%.

Computing details top

Data collection: X-AREA (Stoe & Cie, 2002); cell refinement: X-AREA; data reduction: X-RED32 (Stoe & Cie, 2002); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 for Windows (Farrugia, 1997); software used to prepare material for publication: WinGX (Farrugia, 1999).

Figures top

	Fig. 1. A view of (I), with the atom-numbering scheme and 50% probability displacement ellipsoids·[Symmetry codes: (i) −x, y, −z + 1/2]
	Fig. 2. A view of the packing of (I); C—H···π interactions are drawn as dashed lines.

O,O-Bis(2-tert-butyl-4-methoxyphenyl) chlorothiophosphonate top

Crystal data top

C₂₂H₃₀ClO₄PS	F(000) = 968
M_r = 456.94	D_x = 1.286 Mg m⁻³
Monoclinic, C2/c	Mo Kα radiation, λ = 0.71073 Å
Hall symbol: -C 2yc	Cell parameters from 16485 reflections
a = 23.592 (3) Å	θ = 1.7–26.7°
b = 8.3111 (6) Å	µ = 0.34 mm⁻¹
c = 12.5067 (14) Å	T = 150 K
β = 105.740 (9)°	Prism, colorless
V = 2360.3 (4) Å³	0.64 × 0.59 × 0.55 mm
Z = 4

Data collection top

Stoe IPDS-II diffractometer	2146 reflections with I > 2σ(I)
Graphite monochromator	R_int = 0.032
ω scans	θ_max = 26.0°, θ_min = 1.8°
Absorption correction: integration (X-RED32; Stoe & Cie, 2002)	h = −28→28
T_min = 0.824, T_max = 0.869	k = −10→10
16485 measured reflections	l = −15→15
2327 independent reflections

Refinement top

Refinement on F²	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F² > 2σ(F²)] = 0.028	Hydrogen site location: difference Fourier map
wR(F²) = 0.073	All H-atom parameters refined
S = 1.08	w = 1/[σ²(F_o²) + (0.0362P)² + 1.6163P] where P = (F_o² + 2F_c²)/3
2327 reflections	(Δ/σ)_max = 0.002
192 parameters	Δρ_max = 0.17 e Å⁻³
0 restraints	Δρ_min = −0.34 e Å⁻³

Crystal data top

C₂₂H₃₀ClO₄PS	V = 2360.3 (4) Å³
M_r = 456.94	Z = 4
Monoclinic, C2/c	Mo Kα radiation
a = 23.592 (3) Å	µ = 0.34 mm⁻¹
b = 8.3111 (6) Å	T = 150 K
c = 12.5067 (14) Å	0.64 × 0.59 × 0.55 mm
β = 105.740 (9)°

Data collection top

Stoe IPDS-II diffractometer	2327 independent reflections
Absorption correction: integration (X-RED32; Stoe & Cie, 2002)	2146 reflections with I > 2σ(I)
T_min = 0.824, T_max = 0.869	R_int = 0.032
16485 measured reflections

Refinement top

R[F² > 2σ(F²)] = 0.028	0 restraints
wR(F²) = 0.073	All H-atom parameters refined
S = 1.08	Δρ_max = 0.17 e Å⁻³
2327 reflections	Δρ_min = −0.34 e Å⁻³
192 parameters

Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
C1	0.58872 (5)	0.29212 (15)	0.41994 (10)	0.0224 (3)
C2	0.59796 (6)	0.14466 (16)	0.47516 (11)	0.0258 (3)
C3	0.65010 (6)	0.11722 (16)	0.55649 (11)	0.0272 (3)
C4	0.69210 (5)	0.23993 (16)	0.58337 (10)	0.0249 (3)
C5	0.68201 (6)	0.38769 (16)	0.52737 (11)	0.0252 (3)
C6	0.62988 (5)	0.41888 (15)	0.44326 (10)	0.0233 (3)
C7	0.61903 (6)	0.58369 (16)	0.38318 (12)	0.0296 (3)
C8	0.61032 (8)	0.56105 (19)	0.25687 (13)	0.0374 (3)
C9	0.56458 (8)	0.66639 (19)	0.40646 (15)	0.0402 (4)
C10	0.67218 (8)	0.6983 (2)	0.42394 (16)	0.0453 (4)
C11	0.78481 (6)	0.32952 (19)	0.70159 (13)	0.0343 (3)
O1	0.53449 (4)	0.31975 (10)	0.33826 (7)	0.0257 (2)
O2	0.74184 (4)	0.20383 (12)	0.66690 (8)	0.0319 (2)
P1	0.5000	0.19428 (5)	0.2500	0.02610 (13)
Cl1	0.554354 (14)	0.06331 (4)	0.18992 (3)	0.03162 (11)	0.50
S1	0.554354 (14)	0.06331 (4)	0.18992 (3)	0.03162 (11)	0.50
H2	0.5683 (7)	0.0634 (19)	0.4571 (13)	0.032 (4)*
H3	0.6579 (7)	0.014 (2)	0.5947 (13)	0.034 (4)*
H5	0.7120 (7)	0.4671 (19)	0.5482 (13)	0.029 (4)*
H8A	0.6047 (8)	0.668 (3)	0.2193 (16)	0.052 (5)*
H8B	0.5774 (8)	0.495 (2)	0.2241 (15)	0.043 (5)*
H8C	0.6466 (9)	0.512 (2)	0.2429 (17)	0.056 (5)*
H9A	0.5571 (8)	0.772 (2)	0.3671 (15)	0.051 (5)*
H9B	0.5703 (8)	0.686 (2)	0.4892 (18)	0.056 (5)*
H9C	0.5281 (8)	0.601 (2)	0.3804 (15)	0.047 (5)*
H10A	0.7097 (9)	0.650 (2)	0.4105 (16)	0.056 (6)*
H10B	0.6816 (9)	0.720 (2)	0.5075 (19)	0.059 (6)*
H10C	0.6631 (9)	0.798 (2)	0.3852 (17)	0.056 (5)*
H11A	0.8030 (8)	0.360 (2)	0.6410 (15)	0.042 (5)*
H11B	0.8151 (8)	0.282 (2)	0.7644 (15)	0.041 (4)*
H11C	0.7671 (7)	0.427 (2)	0.7281 (14)	0.035 (4)*

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
C1	0.0207 (6)	0.0240 (6)	0.0204 (6)	0.0000 (5)	0.0020 (4)	−0.0009 (5)
C2	0.0254 (6)	0.0247 (6)	0.0254 (6)	−0.0045 (5)	0.0037 (5)	0.0004 (5)
C3	0.0293 (7)	0.0261 (7)	0.0243 (6)	−0.0001 (5)	0.0037 (5)	0.0030 (5)
C4	0.0223 (6)	0.0311 (7)	0.0198 (6)	0.0006 (5)	0.0029 (5)	−0.0023 (5)
C5	0.0241 (6)	0.0262 (6)	0.0246 (6)	−0.0044 (5)	0.0053 (5)	−0.0041 (5)
C6	0.0253 (6)	0.0223 (6)	0.0222 (6)	−0.0015 (5)	0.0064 (5)	−0.0023 (5)
C7	0.0315 (7)	0.0212 (6)	0.0333 (7)	−0.0037 (5)	0.0041 (6)	0.0019 (5)
C8	0.0447 (9)	0.0336 (8)	0.0327 (8)	−0.0051 (7)	0.0086 (7)	0.0086 (6)
C9	0.0443 (9)	0.0242 (7)	0.0498 (10)	0.0051 (6)	0.0087 (7)	−0.0019 (7)
C10	0.0439 (9)	0.0279 (8)	0.0556 (11)	−0.0124 (7)	−0.0012 (8)	0.0062 (7)
C11	0.0253 (7)	0.0395 (8)	0.0322 (7)	−0.0019 (6)	−0.0021 (6)	−0.0082 (6)
O1	0.0238 (4)	0.0220 (4)	0.0260 (5)	0.0002 (3)	−0.0022 (4)	−0.0019 (4)
O2	0.0252 (5)	0.0360 (5)	0.0283 (5)	−0.0015 (4)	−0.0033 (4)	0.0005 (4)
P1	0.0288 (2)	0.0192 (2)	0.0242 (2)	0.000	−0.00339 (18)	0.000
Cl1	0.02605 (18)	0.0368 (2)	0.0320 (2)	0.00652 (13)	0.00781 (14)	−0.00242 (13)
S1	0.02605 (18)	0.0368 (2)	0.0320 (2)	0.00652 (13)	0.00781 (14)	−0.00242 (13)

Geometric parameters (Å, º) top

C1—C2	1.3946 (18)	C8—H8C	1.00 (2)
C1—C6	1.4086 (17)	C9—H9A	1.00 (2)
C1—O1	1.4226 (14)	C9—H9B	1.02 (2)
C2—C3	1.3860 (18)	C9—H9C	0.994 (19)
C2—H2	0.955 (16)	C10—H10A	1.03 (2)
C3—C4	1.3979 (18)	C10—H10B	1.02 (2)
C3—H3	0.974 (17)	C10—H10C	0.96 (2)
C4—O2	1.3759 (15)	C11—O2	1.4383 (17)
C4—C5	1.4017 (19)	C11—H11A	0.998 (18)
C5—C6	1.4088 (18)	C11—H11B	0.990 (18)
C5—H5	0.952 (16)	C11—H11C	1.009 (17)
C6—C7	1.5499 (18)	O1—P1	1.5750 (9)
C7—C10	1.5468 (19)	P1—O1ⁱ	1.5750 (9)
C7—C8	1.548 (2)	P1—S1ⁱ	1.9791 (4)
C7—C9	1.552 (2)	P1—Cl1ⁱ	1.9791 (4)
C8—H8A	1.00 (2)	P1—Cl1	1.9791 (4)
C8—H8B	0.948 (19)

C2—C1—C6	123.25 (11)	C7—C9—H9A	109.9 (11)
C2—C1—O1	119.13 (11)	C7—C9—H9B	111.8 (11)
C6—C1—O1	117.58 (11)	H9A—C9—H9B	108.6 (16)
C3—C2—C1	119.77 (12)	C7—C9—H9C	112.5 (11)
C3—C2—H2	120.3 (9)	H9A—C9—H9C	107.2 (15)
C1—C2—H2	119.9 (9)	H9B—C9—H9C	106.6 (15)
C2—C3—C4	119.11 (12)	C7—C10—H10A	111.4 (11)
C2—C3—H3	121.1 (9)	C7—C10—H10B	112.1 (11)
C4—C3—H3	119.8 (9)	H10A—C10—H10B	106.1 (16)
O2—C4—C3	115.24 (12)	C7—C10—H10C	108.5 (12)
O2—C4—C5	124.38 (11)	H10A—C10—H10C	109.9 (16)
C3—C4—C5	120.39 (11)	H10B—C10—H10C	108.8 (16)
C4—C5—C6	121.99 (12)	O2—C11—H11A	111.5 (10)
C4—C5—H5	117.3 (9)	O2—C11—H11B	104.1 (10)
C6—C5—H5	120.7 (9)	H11A—C11—H11B	109.7 (14)
C1—C6—C5	115.48 (11)	O2—C11—H11C	111.3 (9)
C1—C6—C7	123.14 (11)	H11A—C11—H11C	110.4 (14)
C5—C6—C7	121.37 (11)	H11B—C11—H11C	109.7 (13)
C10—C7—C8	106.40 (13)	C1—O1—P1	126.11 (8)
C10—C7—C6	111.83 (11)	C4—O2—C11	117.18 (11)
C8—C7—C6	110.24 (11)	O1—P1—O1ⁱ	97.08 (7)
C10—C7—C9	107.68 (13)	O1—P1—S1ⁱ	111.27 (4)
C8—C7—C9	110.96 (12)	O1ⁱ—P1—S1ⁱ	111.44 (3)
C6—C7—C9	109.67 (12)	O1—P1—Cl1ⁱ	111.27 (4)
C7—C8—H8A	109.7 (11)	O1ⁱ—P1—Cl1ⁱ	111.44 (3)
C7—C8—H8B	112.2 (11)	S1ⁱ—P1—Cl1ⁱ	0.00 (2)
H8A—C8—H8B	108.9 (16)	O1—P1—Cl1	111.44 (3)
C7—C8—H8C	110.0 (12)	O1ⁱ—P1—Cl1	111.27 (4)
H8A—C8—H8C	106.8 (16)	S1ⁱ—P1—Cl1	113.26 (3)
H8B—C8—H8C	109.0 (16)	Cl1ⁱ—P1—Cl1	113.26 (3)

C6—C1—C2—C3	−0.8 (2)	C5—C6—C7—C10	2.35 (18)
O1—C1—C2—C3	−178.73 (11)	C1—C6—C7—C8	−60.70 (16)
C1—C2—C3—C4	1.4 (2)	C5—C6—C7—C8	120.51 (13)
C2—C3—C4—O2	178.39 (11)	C1—C6—C7—C9	61.76 (16)
C2—C3—C4—C5	−1.14 (19)	C5—C6—C7—C9	−117.03 (14)
O2—C4—C5—C6	−179.21 (11)	C2—C1—O1—P1	−40.07 (15)
C3—C4—C5—C6	0.28 (19)	C6—C1—O1—P1	141.89 (10)
C2—C1—C6—C5	−0.05 (18)	C3—C4—O2—C11	−176.65 (12)
O1—C1—C6—C5	177.90 (10)	C5—C4—O2—C11	2.86 (18)
C2—C1—C6—C7	−178.90 (12)	C1—O1—P1—O1ⁱ	−155.66 (11)
O1—C1—C6—C7	−0.95 (18)	C1—O1—P1—S1ⁱ	88.01 (9)
C4—C5—C6—C1	0.31 (18)	C1—O1—P1—Cl1ⁱ	88.01 (9)
C4—C5—C6—C7	179.19 (12)	C1—O1—P1—Cl1	−39.46 (10)
C1—C6—C7—C10	−178.86 (13)

Symmetry code: (i) −x+1, y, −z+1/2.

Experimental details

Crystal data
Chemical formula	C₂₂H₃₀ClO₄PS
M_r	456.94
Crystal system, space group	Monoclinic, C2/c
Temperature (K)	150
a, b, c (Å)	23.592 (3), 8.3111 (6), 12.5067 (14)
β (°)	105.740 (9)
V (Å³)	2360.3 (4)
Z	4
Radiation type	Mo Kα
µ (mm⁻¹)	0.34
Crystal size (mm)	0.64 × 0.59 × 0.55

Data collection
Diffractometer	Stoe IPDS-II diffractometer
Absorption correction	Integration (X-RED32; Stoe & Cie, 2002)
T_min, T_max	0.824, 0.869
No. of measured, independent and observed [I > 2σ(I)] reflections	16485, 2327, 2146
R_int	0.032
(sin θ/λ)_max (Å⁻¹)	0.617

Refinement
R[F² > 2σ(F²)], wR(F²), S	0.028, 0.073, 1.08
No. of reflections	2327
No. of parameters	192
H-atom treatment	All H-atom parameters refined
Δρ_max, Δρ_min (e Å⁻³)	0.17, −0.34

Computer programs: X-AREA (Stoe & Cie, 2002), X-AREA, X-RED32 (Stoe & Cie, 2002), SHELXS97 (Sheldrick, 1997), SHELXL97 (Sheldrick, 1997), ORTEP-3 for Windows (Farrugia, 1997), WinGX (Farrugia, 1999).

Selected geometric parameters (Å, º) top

C1—C2	1.3946 (18)	C4—C5	1.4017 (19)
C1—C6	1.4086 (17)	C5—C6	1.4088 (18)
C1—O1	1.4226 (14)	O1—P1	1.5750 (9)
C2—C3	1.3860 (18)	P1—S1ⁱ	1.9791 (4)
C3—C4	1.3979 (18)	P1—Cl1	1.9791 (4)

C2—C1—C6	123.25 (11)	C4—C5—C6	121.99 (12)
C2—C1—O1	119.13 (11)	C1—C6—C5	115.48 (11)
C6—C1—O1	117.58 (11)	O1—P1—O1ⁱ	97.08 (7)
C3—C2—C1	119.77 (12)	O1—P1—S1ⁱ	111.27 (4)
C2—C3—C4	119.11 (12)	O1—P1—Cl1	111.44 (3)
C3—C4—C5	120.39 (11)	S1ⁱ—P1—Cl1	113.26 (3)

Symmetry code: (i) −x+1, y, −z+1/2.

References

Farrugia, L. J. (1997). J. Appl. Cryst. 30, 565. CrossRef IUCr Journals Google Scholar
Farrugia, L. J. (1999). J. Appl. Cryst. 32, 837–838. CrossRef CAS IUCr Journals Google Scholar
Sheldrick, G. M. (1997). SHELXS97 and SHELXL97. University of Göttingen, Germany. Google Scholar
Stoe & Cie (2002). X-AREA (Version 1.18) and X-RED32 (Version 1.04). Stoe & Cie, Darmstadt, Germany. Google Scholar

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Volume 61| Part 10| October 2005| Pages e4-e5

doi:10.1107/S1600536805027789

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addenda and errata\(\def\hfill{\hskip 5em}\def\hfil{\hskip 3em}\def\eqno#1{\hfil {#1}}\)

O,O-Bis(2-tert-butyl-4-meth­oxy­phen­yl) chloro­thio­phospho­nate. Corrigendum.

1. Comment

2. Experimental

2.1.1. Crystal data

2.1.2. Data collection

2.1.3. Refinement

Supporting information

References

addenda and errata

O,O-Bis(2-tert-butyl-4-methoxyphenyl) chlorothiophosphonate. Corrigendum.