# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' VICKI VR06 SOTON DATA' _shelx_refln_list_code 4 _shelx_F_calc_maximum 161.25 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.7691 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 4.7790 _cell_length_b 11.9257 _cell_length_c 14.6703 _cell_angle_alpha 90.000 _cell_angle_beta 96.817 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5468.70 5314.53 142.79 o 4 0 0 3962.24 4149.30 106.38 o 6 0 0 796.40 826.30 80.49 o 1 1 0 1072.83 1085.76 18.37 o 2 1 0 17.50 30.07 2.08 o 3 1 0 1433.70 1637.63 31.89 o 4 1 0 547.93 608.26 12.21 o 5 1 0 225.80 236.47 10.36 o 6 1 0 30.76 18.71 8.56 o 0 2 0 359.99 357.68 10.87 o 1 2 0 21964.94 20052.34 794.22 o 2 2 0 171.95 193.80 5.28 o 3 2 0 5796.93 5876.00 97.93 o 4 2 0 997.57 1042.58 20.66 o 5 2 0 1652.58 1738.99 46.78 o 6 2 0 32.59 10.73 8.69 o 1 3 0 1030.53 1061.65 21.85 o 2 3 0 686.90 710.23 11.35 o 3 3 0 97.12 118.62 4.89 o 4 3 0 1023.84 1044.26 23.70 o 5 3 0 220.69 201.30 11.51 o 6 3 0 184.19 190.18 15.45 o 0 4 0 10117.67 10564.12 253.20 o 1 4 0 2094.08 2100.11 42.54 o 2 4 0 4772.74 4705.70 94.68 o 3 4 0 469.44 456.86 9.09 o 4 4 0 3102.98 3061.43 56.11 o 5 4 0 40.99 31.11 12.94 o 1 5 0 163.22 156.97 5.36 o 2 5 0 9.20 19.25 2.29 o 3 5 0 508.04 546.26 12.55 o 4 5 0 356.43 466.46 16.05 o 5 5 0 704.41 735.32 32.85 o 0 6 0 1932.68 1941.73 50.54 o 1 6 0 8657.92 8458.04 157.14 o 2 6 0 1487.40 1525.91 27.51 o 3 6 0 1973.01 1972.23 38.36 o 4 6 0 22.23 31.52 3.76 o 5 6 0 416.79 392.61 21.14 o 1 7 0 17.18 21.93 4.17 o 2 7 0 718.86 669.56 13.72 o 3 7 0 125.59 123.29 6.60 o 4 7 0 353.61 353.56 12.95 o 5 7 0 5.85 2.28 7.97 o 0 8 0 4903.73 5132.54 125.56 o 1 8 0 1518.45 1498.57 29.83 o 2 8 0 3300.33 3315.50 71.67 o 3 8 0 1406.18 1357.94 38.12 o 4 8 0 551.24 535.30 25.38 o 5 8 0 325.94 325.20 17.69 o 1 9 0 344.80 337.05 9.31 o 2 9 0 13.31 8.69 2.40 o 3 9 0 511.24 525.88 14.71 o 4 9 0 14.35 86.54 14.20 o 5 9 0 249.35 247.73 36.68 o 0 10 0 1532.35 1591.11 49.49 o 1 10 0 743.12 734.54 26.68 o 2 10 0 2823.82 2662.00 76.34 o 3 10 0 903.62 869.90 32.29 o 4 10 0 771.16 763.54 48.07 o 1 11 0 31.85 33.77 4.65 o 2 11 0 149.75 145.19 7.74 o 3 11 0 34.60 31.38 5.83 o 4 11 0 238.52 194.73 15.80 o 0 12 0 16.02 33.53 6.88 o 1 12 0 2802.57 2901.68 86.21 o 2 12 0 404.83 397.56 14.07 o 3 12 0 337.31 370.72 17.77 o 1 13 0 66.69 61.31 4.85 o 2 13 0 1.94 11.69 5.68 o 3 13 0 112.50 116.64 11.33 o 0 14 0 956.14 1117.96 49.03 o 1 14 0 8.22 12.28 5.41 o 2 14 0 857.69 772.67 53.89 o 1 15 0 6.52 3.28 6.62 o -5 0 1 941.70 957.36 31.36 o -3 0 1 7298.17 7552.10 180.12 o -1 0 1 223.82 228.48 5.60 o 1 0 1 12283.66 11812.55 339.89 o 3 0 1 1938.94 1873.93 39.84 o 5 0 1 1628.22 1684.89 62.00 o -6 1 1 381.76 415.36 25.05 o -5 1 1 56.32 82.69 6.40 o -4 1 1 546.23 612.66 14.35 o -3 1 1 555.00 548.56 9.65 o -2 1 1 498.94 476.82 8.60 o -1 1 1 324.39 331.01 5.88 o 1 1 1 889.12 885.93 15.76 o 2 1 1 122.41 109.51 3.85 o 3 1 1 265.23 294.94 6.53 o 4 1 1 96.38 143.85 6.19 o 5 1 1 448.37 410.52 14.62 o 6 1 1 191.91 191.89 18.57 o -6 2 1 454.72 392.45 24.99 o -5 2 1 9.98 18.23 5.64 o -4 2 1 1661.57 1626.12 37.80 o -3 2 1 8.06 8.85 2.87 o -2 2 1 5082.39 4803.17 88.08 o -1 2 1 560.43 517.83 17.85 o 0 2 1 8678.21 8463.67 150.00 o 1 2 1 645.84 663.86 19.14 o 2 2 1 5227.74 4962.16 92.13 o 3 2 1 367.12 393.63 10.63 o 4 2 1 2497.65 2526.73 54.28 o 5 2 1 24.63 29.48 5.70 o 6 2 1 542.64 531.26 30.69 o -6 3 1 175.87 155.33 13.82 o -5 3 1 1121.84 1116.13 42.21 o -4 3 1 686.06 694.07 16.73 o -3 3 1 1634.55 1537.20 28.72 o -2 3 1 155.58 146.27 3.83 o -1 3 1 20.38 29.23 2.12 o 0 3 1 281.33 283.08 5.80 o 1 3 1 200.57 206.92 5.54 o 2 3 1 63.54 71.74 3.39 o 3 3 1 35.58 64.80 9.46 o 4 3 1 30.94 305.40 17.11 o 5 3 1 2.53 0.75 6.57 o -5 4 1 552.68 539.65 22.96 o -4 4 1 420.98 451.98 11.43 o -3 4 1 3373.21 3360.86 63.32 o -2 4 1 2306.50 2163.88 40.95 o -1 4 1 5411.73 5140.36 96.32 o 0 4 1 1430.51 1452.46 25.83 o 1 4 1 10473.30 10384.54 196.00 o 2 4 1 623.62 614.05 10.83 o 3 4 1 2854.23 2916.27 48.59 o 4 4 1 746.09 737.59 18.30 o 5 4 1 822.52 891.55 32.08 o -5 5 1 12.91 13.47 5.98 o -4 5 1 353.46 349.94 10.09 o -3 5 1 831.44 879.68 18.03 o -2 5 1 1964.40 2009.25 36.22 o -1 5 1 507.65 560.55 10.87 o 0 5 1 2436.21 2598.79 44.61 o 1 5 1 723.89 811.49 16.56 o 2 5 1 24.28 18.53 2.66 o 3 5 1 412.93 413.00 9.06 o 4 5 1 18.84 32.28 3.73 o 5 5 1 81.58 81.07 7.58 o -5 6 1 234.84 216.09 14.39 o -4 6 1 1268.17 1239.81 38.02 o -3 6 1 3104.09 3201.91 75.69 o -2 6 1 4730.09 4642.30 84.24 o -1 6 1 3424.70 3444.76 71.52 o 0 6 1 1562.81 1447.16 22.76 o 1 6 1 710.02 660.35 18.93 o 2 6 1 3128.80 2967.94 60.01 o 3 6 1 3421.40 3429.10 60.76 o 4 6 1 872.66 841.33 21.88 o 5 6 1 66.20 51.68 9.22 o -5 7 1 740.12 744.37 41.66 o -4 7 1 51.26 170.59 14.96 o -3 7 1 71.90 66.49 4.25 o -2 7 1 202.24 181.41 5.46 o -1 7 1 3045.56 3050.30 72.72 o 0 7 1 111.74 117.01 4.98 o 1 7 1 20.55 15.72 2.65 o 2 7 1 25.38 27.85 4.05 o 3 7 1 4.26 52.28 14.00 o 4 7 1 524.18 548.99 18.64 o 5 7 1 35.60 22.13 7.84 o -5 8 1 485.67 455.14 34.30 o -4 8 1 505.14 537.09 28.03 o -3 8 1 486.82 467.53 14.94 o -2 8 1 3386.90 3318.98 57.27 o -1 8 1 1627.09 1585.44 33.08 o 0 8 1 1847.99 1899.14 31.15 o 1 8 1 1082.00 1038.50 24.06 o 2 8 1 4051.05 3937.65 92.23 o 3 8 1 762.64 766.52 17.17 o 4 8 1 711.67 739.43 21.49 o 5 8 1 538.48 494.72 49.27 o -5 9 1 78.37 68.77 9.74 o -4 9 1 761.64 752.21 32.29 o -3 9 1 1.84 4.99 2.92 o -2 9 1 83.31 85.58 4.88 o -1 9 1 177.45 177.23 6.99 o 0 9 1 6.28 10.12 2.62 o 1 9 1 141.88 142.96 8.43 o 2 9 1 13.79 13.90 3.40 o 3 9 1 98.68 90.62 4.85 o 4 9 1 1.24 10.09 6.08 o -4 10 1 150.22 153.59 10.81 o -3 10 1 877.09 944.03 23.91 o -2 10 1 244.28 227.18 9.46 o -1 10 1 3844.30 3817.66 74.87 o 0 10 1 1146.74 1157.15 24.53 o 1 10 1 1231.91 1258.68 32.42 o 2 10 1 533.00 497.70 14.87 o 3 10 1 1628.53 1638.80 53.99 o 4 10 1 273.09 253.33 17.22 o -4 11 1 1.59 39.49 13.29 o -3 11 1 251.81 257.01 11.78 o -2 11 1 35.84 38.98 4.09 o -1 11 1 175.62 167.07 6.80 o 0 11 1 69.39 71.67 4.95 o 1 11 1 3.27 2.10 4.45 o 2 11 1 3.58 -4.50 4.50 o 3 11 1 3.22 14.45 8.06 o 4 11 1 118.18 117.73 12.24 o -3 12 1 147.96 138.86 14.77 o -2 12 1 1361.16 1300.34 45.42 o -1 12 1 706.42 709.92 27.83 o 0 12 1 1635.14 1706.11 55.81 o 1 12 1 63.48 71.63 5.25 o 2 12 1 1471.11 1465.23 42.35 o 3 12 1 152.09 141.57 17.32 o -3 13 1 107.35 85.48 8.94 o -2 13 1 165.29 140.50 11.70 o -1 13 1 3.26 8.26 3.82 o 0 13 1 259.68 255.42 11.51 o 1 13 1 1.63 8.43 4.19 o 2 13 1 53.21 59.61 8.19 o 3 13 1 0.51 -3.85 10.40 o -2 14 1 106.11 106.48 19.26 o -1 14 1 1363.21 1382.28 86.52 o 0 14 1 26.42 31.49 7.03 o 1 14 1 1355.75 1485.63 50.40 o 2 14 1 10.00 8.81 6.39 o -1 15 1 53.64 46.91 7.79 o 0 15 1 0.71 -5.67 5.67 o 1 15 1 62.99 43.44 9.90 o -6 0 2 174.13 145.85 16.15 o -4 0 2 2631.10 2565.64 68.76 o -2 0 2 2820.16 2726.17 68.35 o 2 0 2 11458.90 11262.84 267.48 o 4 0 2 4777.34 5093.41 116.44 o 6 0 2 821.51 814.81 93.61 o -6 1 2 242.78 213.03 20.16 o -5 1 2 892.07 948.12 31.30 o -4 1 2 1463.43 1496.76 27.64 o -3 1 2 4426.14 4560.60 79.66 o -2 1 2 5753.61 5975.71 111.07 o -1 1 2 1953.33 1876.03 37.54 o 0 1 2 228.76 246.56 5.40 o 1 1 2 13464.63 13830.00 236.88 o 2 1 2 1085.67 1113.68 21.21 o 3 1 2 12.34 39.51 10.26 o 4 1 2 66.33 199.12 11.55 o 5 1 2 11.08 10.23 4.84 o 6 1 2 27.71 13.26 8.75 o -6 2 2 30.55 21.05 7.73 o -5 2 2 755.85 756.20 30.73 o -4 2 2 5.31 111.41 7.57 o -3 2 2 2791.94 3009.51 58.18 o -2 2 2 2.86 9.98 2.01 o -1 2 2 8268.28 7875.37 147.48 o 0 2 2 6238.60 6481.94 126.50 o 1 2 2 26002.40 26485.83 474.41 o 2 2 2 478.52 546.23 9.33 o 3 2 2 4021.51 3974.36 76.45 o 4 2 2 39.00 59.26 7.01 o 5 2 2 2220.80 2253.99 86.45 o -6 3 2 403.41 453.59 20.56 o -5 3 2 39.91 57.88 7.98 o -4 3 2 940.21 1006.06 19.77 o -3 3 2 371.29 349.96 7.07 o -2 3 2 4187.69 4039.16 77.62 o -1 3 2 597.29 579.95 11.16 o 0 3 2 5166.32 5306.68 104.85 o 1 3 2 339.22 373.72 22.69 o 2 3 2 2538.37 2620.45 41.74 o 3 3 2 132.41 157.41 6.32 o 4 3 2 126.49 127.02 5.96 o 5 3 2 77.34 75.35 11.46 o -5 4 2 104.03 104.47 7.97 o -4 4 2 580.73 587.25 15.17 o -3 4 2 117.75 118.36 5.36 o -2 4 2 5320.19 5273.95 102.56 o -1 4 2 158.75 120.60 18.77 o 0 4 2 11482.35 11985.27 197.39 o 1 4 2 1059.21 1069.75 20.23 o 2 4 2 11178.86 11043.88 215.31 o 3 4 2 583.87 579.20 10.94 o 4 4 2 1442.40 1508.75 35.74 o 5 4 2 385.72 390.44 17.82 o -5 5 2 1263.22 1208.01 63.13 o -4 5 2 87.85 83.46 4.85 o -3 5 2 2078.85 2032.10 34.15 o -2 5 2 533.85 551.90 10.09 o -1 5 2 2073.77 2000.53 37.92 o 0 5 2 1273.87 1357.89 24.31 o 1 5 2 820.57 798.04 14.26 o 2 5 2 34.17 32.01 3.93 o 3 5 2 1.08 36.28 10.63 o 4 5 2 54.33 143.02 10.83 o 5 5 2 4.36 -1.88 6.95 o -5 6 2 345.74 319.37 18.23 o -4 6 2 39.56 99.27 7.97 o -3 6 2 955.62 1008.31 22.51 o -2 6 2 792.30 763.52 13.70 o -1 6 2 3320.61 3237.14 58.13 o 0 6 2 2299.55 2446.94 38.60 o 1 6 2 3447.21 3183.91 62.05 o 2 6 2 673.61 623.99 17.07 o 3 6 2 4437.72 4425.66 84.64 o 4 6 2 2550.52 2475.27 59.46 o 5 6 2 1087.31 1141.70 51.98 o -5 7 2 0.17 4.22 6.52 o -4 7 2 2427.03 2493.96 64.95 o -3 7 2 671.26 664.50 16.35 o -2 7 2 1261.99 1180.92 22.50 o -1 7 2 13.87 19.93 2.71 o 0 7 2 2301.36 2458.55 37.97 o 1 7 2 16.61 15.55 4.11 o 2 7 2 175.98 167.27 6.54 o 3 7 2 195.63 195.49 6.19 o 4 7 2 3.74 -1.03 4.61 o 5 7 2 19.68 18.63 8.80 o -5 8 2 6.81 4.33 6.93 o -4 8 2 565.32 540.20 19.98 o -3 8 2 206.70 255.85 9.22 o -2 8 2 959.83 911.68 23.01 o -1 8 2 2861.16 2757.47 47.62 o 0 8 2 1324.67 1385.24 22.19 o 1 8 2 1644.80 1562.01 50.81 o 2 8 2 1959.63 1891.55 41.83 o 3 8 2 1256.26 1282.92 30.23 o 4 8 2 942.59 886.26 40.07 o 5 8 2 333.58 261.94 20.65 o -5 9 2 554.12 524.24 43.15 o -4 9 2 1.45 30.41 9.35 o -3 9 2 1290.05 1291.54 33.25 o -2 9 2 1.98 2.33 3.18 o -1 9 2 2450.17 2437.27 44.38 o 0 9 2 69.34 76.01 4.37 o 1 9 2 1595.06 1578.86 32.54 o 2 9 2 17.37 18.50 4.04 o 3 9 2 67.18 78.94 12.16 o 4 9 2 72.89 123.29 14.75 o -4 10 2 177.12 179.02 10.93 o -3 10 2 107.80 99.38 8.39 o -2 10 2 231.30 251.30 9.04 o -1 10 2 1395.54 1408.39 29.56 o 0 10 2 2839.77 2986.44 65.85 o 1 10 2 696.05 749.13 24.07 o 2 10 2 993.16 920.68 28.59 o 3 10 2 402.66 394.08 16.84 o 4 10 2 684.84 671.28 34.32 o -4 11 2 950.71 960.44 48.66 o -3 11 2 594.76 559.35 20.93 o -2 11 2 551.30 535.86 18.50 o -1 11 2 29.83 24.53 5.22 o 0 11 2 1729.81 1747.46 46.80 o 1 11 2 13.85 13.30 4.46 o 2 11 2 43.07 57.23 7.44 o 3 11 2 38.46 38.27 7.86 o 4 11 2 41.35 47.24 7.64 o -3 12 2 224.23 236.89 16.84 o -2 12 2 127.14 114.76 6.52 o -1 12 2 778.85 719.23 25.21 o 0 12 2 273.87 271.35 10.04 o 1 12 2 957.85 989.23 31.66 o 2 12 2 194.59 204.04 10.65 o 3 12 2 1200.72 1181.45 67.49 o -3 13 2 293.17 298.18 16.99 o -2 13 2 116.94 104.93 9.45 o -1 13 2 431.79 452.86 27.15 o 0 13 2 103.51 95.41 6.61 o 1 13 2 3.44 2.00 5.24 o 2 13 2 149.71 134.81 9.17 o 3 13 2 12.44 14.36 9.13 o -2 14 2 417.30 413.83 24.79 o -1 14 2 7.10 -1.63 6.84 o 0 14 2 846.04 1023.19 40.65 o 1 14 2 8.30 10.87 12.89 o 2 14 2 908.57 1026.16 81.22 o -1 15 2 118.60 75.32 8.53 o 0 15 2 104.34 87.59 10.83 o 1 15 2 72.44 60.73 9.76 o -5 0 3 3.58 -0.39 8.27 o -3 0 3 1617.29 1651.84 36.04 o -1 0 3 10756.66 10398.13 297.94 o 1 0 3 16291.13 16521.65 495.76 o 3 0 3 3659.76 3513.28 78.68 o 5 0 3 676.21 701.30 82.81 o -6 1 3 497.51 486.23 29.94 o -5 1 3 1170.42 1179.01 38.10 o -4 1 3 1440.52 1478.19 26.96 o -3 1 3 824.97 734.52 16.60 o -2 1 3 6124.35 6066.80 120.10 o -1 1 3 4463.91 4168.96 84.26 o 0 1 3 48.04 49.34 1.28 o 1 1 3 369.68 386.08 6.68 o 2 1 3 1259.09 1217.38 20.72 o 3 1 3 681.98 770.88 20.76 o 4 1 3 4.42 123.03 9.16 o 5 1 3 55.84 43.05 6.99 o -6 2 3 8.91 7.10 7.10 o -5 2 3 368.62 363.09 19.70 o -4 2 3 677.51 689.78 15.12 o -3 2 3 1089.14 1156.62 19.27 o -2 2 3 4534.83 4569.70 77.01 o -1 2 3 35.88 32.40 10.32 o 0 2 3 2697.14 2714.94 55.33 o 1 2 3 1450.30 1437.45 23.40 o 2 2 3 6268.82 6078.60 104.13 o 3 2 3 304.51 305.07 11.67 o 4 2 3 1703.67 1749.16 37.29 o 5 2 3 579.41 535.64 19.52 o -6 3 3 530.16 468.62 26.99 o -5 3 3 1891.29 1960.12 56.00 o -4 3 3 331.15 372.11 9.65 o -3 3 3 2490.20 2505.80 46.71 o -2 3 3 2619.17 2647.18 54.72 o -1 3 3 9566.41 9321.99 268.41 o 0 3 3 171.54 182.67 4.56 o 1 3 3 775.56 723.35 23.46 o 2 3 3 41.23 59.03 2.71 o 3 3 3 67.07 71.67 9.34 o 4 3 3 20.92 139.99 12.95 o 5 3 3 20.02 42.91 7.89 o -5 4 3 20.39 24.75 5.05 o -4 4 3 2.58 158.83 11.83 o -3 4 3 2143.30 2201.05 41.55 o -2 4 3 1606.60 1680.55 31.70 o -1 4 3 1708.58 1609.43 29.46 o 0 4 3 2856.32 3008.65 50.59 o 1 4 3 242.42 180.33 4.65 o 2 4 3 789.39 748.80 12.64 o 3 4 3 4382.86 4222.29 75.64 o 4 4 3 528.56 509.72 12.72 o 5 4 3 305.36 339.14 15.23 o -5 5 3 135.12 124.77 15.13 o -4 5 3 2873.12 2901.64 57.91 o -3 5 3 167.51 175.28 6.89 o -2 5 3 3753.53 3519.35 78.04 o -1 5 3 1027.82 986.49 17.29 o 0 5 3 3240.49 3397.69 57.56 o 1 5 3 29.17 47.75 8.12 o 2 5 3 598.17 514.49 11.45 o 3 5 3 1.34 2.03 3.05 o 4 5 3 339.25 336.92 10.26 o 5 5 3 79.15 60.65 6.49 o -5 6 3 9.57 10.30 5.96 o -4 6 3 136.54 126.80 8.79 o -3 6 3 106.89 118.01 15.71 o -2 6 3 1139.98 1099.70 20.51 o -1 6 3 2077.54 2038.72 40.38 o 0 6 3 4392.50 4636.04 78.74 o 1 6 3 2603.99 2516.36 43.29 o 2 6 3 2841.03 2820.70 51.98 o 3 6 3 229.58 239.78 10.63 o 4 6 3 419.20 427.82 16.64 o 5 6 3 136.41 133.63 11.33 o -5 7 3 1508.11 1463.74 83.16 o -4 7 3 0.24 19.88 6.69 o -3 7 3 3331.32 3374.84 84.32 o -2 7 3 16.96 19.00 4.61 o -1 7 3 2709.79 2583.03 58.02 o 0 7 3 259.17 263.16 7.73 o 1 7 3 1146.25 1076.34 19.42 o 2 7 3 35.39 42.07 4.92 o 3 7 3 460.15 493.11 18.82 o 4 7 3 2.42 96.81 10.19 o 5 7 3 54.15 52.49 9.34 o -5 8 3 59.91 41.80 11.26 o -4 8 3 218.24 225.69 12.30 o -3 8 3 187.59 210.49 8.85 o -2 8 3 2163.52 2168.25 50.35 o -1 8 3 3301.69 3204.48 51.36 o 0 8 3 702.03 725.99 13.32 o 1 8 3 2114.42 2074.58 43.55 o 2 8 3 1284.47 1191.80 27.27 o 3 8 3 763.95 732.05 23.38 o 4 8 3 999.09 955.48 43.09 o 5 8 3 376.32 363.53 29.82 o -5 9 3 92.70 87.76 13.38 o -4 9 3 1773.09 1780.59 60.51 o -3 9 3 3.01 2.65 2.89 o -2 9 3 1652.05 1669.41 34.83 o -1 9 3 375.37 346.73 8.34 o 0 9 3 3148.39 3387.27 56.86 o 1 9 3 29.08 35.39 4.00 o 2 9 3 210.45 208.10 8.14 o 3 9 3 46.33 34.16 5.09 o 4 9 3 51.07 49.03 6.79 o -4 10 3 546.95 552.58 38.09 o -3 10 3 998.12 928.82 32.45 o -2 10 3 103.67 99.31 4.37 o -1 10 3 1784.68 1783.92 46.33 o 0 10 3 960.83 981.90 23.61 o 1 10 3 2017.90 1960.94 42.06 o 2 10 3 126.38 120.73 6.30 o 3 10 3 1449.39 1385.27 58.81 o 4 10 3 488.16 441.98 18.39 o -4 11 3 35.27 45.03 10.67 o -3 11 3 2139.01 2133.62 98.24 o -2 11 3 151.11 150.86 9.26 o -1 11 3 240.48 247.25 8.41 o 0 11 3 129.87 151.37 6.94 o 1 11 3 1686.28 1672.72 46.29 o 2 11 3 13.37 14.07 4.89 o 3 11 3 96.36 121.58 17.68 o 4 11 3 199.93 207.87 17.36 o -3 12 3 1.87 9.60 6.89 o -2 12 3 644.32 635.51 20.21 o -1 12 3 69.67 64.02 5.29 o 0 12 3 2811.89 3012.88 82.18 o 1 12 3 175.82 172.04 8.21 o 2 12 3 1177.63 1126.32 42.67 o 3 12 3 4.77 -0.13 10.09 o -3 13 3 516.33 474.73 29.85 o -2 13 3 432.02 415.95 25.08 o -1 13 3 249.03 213.88 14.75 o 0 13 3 647.39 677.39 19.41 o 1 13 3 33.87 32.61 4.58 o 2 13 3 182.97 140.56 12.85 o 3 13 3 62.32 56.66 11.94 o -2 14 3 62.11 42.11 7.14 o -1 14 3 745.49 747.27 37.13 o 0 14 3 114.29 125.74 10.10 o 1 14 3 759.12 717.52 36.81 o 2 14 3 2.68 4.88 12.36 o -1 15 3 366.44 300.79 25.61 o 0 15 3 204.03 176.48 15.41 o 1 15 3 153.71 124.58 17.32 o -6 0 4 0.98 1.99 9.06 o -4 0 4 140.15 140.33 9.69 o -2 0 4 1658.60 1574.09 42.63 o 0 0 4 3402.76 3429.74 84.00 o 2 0 4 1627.69 1566.68 38.33 o 4 0 4 2305.95 2340.55 62.39 o -6 1 4 381.82 391.97 24.06 o -5 1 4 1006.92 1032.79 35.04 o -4 1 4 787.31 794.24 18.23 o -3 1 4 3140.55 3052.54 52.24 o -2 1 4 2505.16 2400.37 40.71 o -1 1 4 4662.27 4457.54 65.86 o 0 1 4 16797.34 17048.45 240.31 o 1 1 4 2950.26 2856.76 53.60 o 2 1 4 2324.33 2281.71 36.36 o 3 1 4 1255.43 1285.13 29.15 o 4 1 4 82.82 131.80 6.58 o 5 1 4 126.83 102.19 10.17 o -6 2 4 47.90 20.72 8.17 o -5 2 4 35.78 34.90 5.84 o -4 2 4 4.60 155.10 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