# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' TRIS(THIOUREA) COPPER(II) PERCHLORATE' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1072.57 _exptl_crystal_F_000 4112.00 _reflns_d_resolution_high 0.8415 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' _cell_length_a 17.2290 _cell_length_b 15.3630 _cell_length_c 27.6390 _cell_angle_alpha 90.000 _cell_angle_beta 93.302 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -32 219.37 14.27 349.85 o 2 0 -32 642.40 86.85 361.08 o 4 0 -32 3653.82 3797.31 265.73 o 1 1 -32 1757.92 926.99 271.65 o 3 1 -32 363.49 484.31 260.54 o 5 1 -32 475.74 94.28 277.41 o 0 2 -32 1431.25 1312.84 254.19 o 2 2 -32 739.88 1.21 407.25 o 4 2 -32 808.70 3.04 402.99 o 1 3 -32 6989.25 4062.74 372.93 o 3 3 -32 10133.44 10602.05 338.31 o 2 4 -32 17475.24 16163.79 467.68 o 1 1 -31 817.55 709.91 439.59 o 3 1 -31 156.91 250.29 249.68 o 5 1 -31 1218.01 266.81 306.57 o 0 2 -31 809.03 164.60 364.43 o 2 2 -31 767.37 47.68 385.68 o 4 2 -31 96.71 0.30 397.53 o 6 2 -31 225.41 0.30 366.85 o 1 3 -31 1093.99 2.43 521.13 o 3 3 -31 1783.48 1132.45 268.76 o 5 3 -31 606.15 65.29 370.20 o 0 4 -31 592.52 5.47 410.28 o 2 4 -31 2384.23 1562.17 283.34 o 4 4 -31 55.02 250.24 344.08 o 6 4 -31 724.10 4.25 401.48 o 1 5 -31 1281.72 1402.43 256.31 o 3 5 -31 2999.75 3343.60 268.16 o 0 0 -30 81.92 385.99 308.85 o 2 0 -30 506.89 590.98 221.08 o 4 0 -30 9213.98 10299.57 317.66 o 6 0 -30 5621.59 6061.00 277.57 o 8 0 -30 476.23 190.11 366.85 o 1 1 -30 587.74 459.16 188.56 o 3 1 -30 998.54 853.25 189.23 o 5 1 -30 7994.35 7238.44 504.12 o 7 1 -30 1324.75 1588.23 392.67 o 9 1 -30 1910.43 1640.18 852.91 o 0 2 -30 1068.65 287.29 372.32 o 2 2 -30 124.97 0.61 364.43 o 4 2 -30 3922.33 3097.31 258.13 o 6 2 -30 186.00 2.43 340.74 o 8 2 -30 47.63 333.75 345.90 o 1 3 -30 6562.54 6095.93 294.88 o 3 3 -30 1595.96 1427.33 235.66 o 5 3 -30 3504.70 2776.92 259.96 o 7 3 -30 445.86 510.80 355.31 o 0 4 -30 6059.00 5014.19 278.79 o 2 4 -30 9130.34 9176.23 310.98 o 4 4 -30 671.45 227.46 363.51 o 6 4 -30 6968.34 7349.25 306.12 o 8 4 -30 1234.40 1255.75 245.68 o 1 5 -30 5880.75 5979.01 287.59 o 3 5 -30 437.21 93.23 374.75 o 5 5 -30 5152.32 4588.72 277.57 o 7 5 -30 523.70 500.48 385.99 o 0 6 -30 942.01 629.85 241.13 o 2 6 -30 1691.51 2504.82 259.05 o 4 6 -30 2204.69 2848.59 262.99 o 1 7 -30 93.16 13.97 368.68 o 3 7 -30 1804.06 1503.86 263.30 o 1 1 -29 431.27 593.81 419.09 o 3 1 -29 246.70 79.62 256.41 o 5 1 -29 23.67 0.74 273.13 o 7 1 -29 930.57 437.92 346.81 o 9 1 -29 1193.29 774.63 542.99 o 0 2 -29 4.20 1.21 333.15 o 2 2 -29 90.42 2.13 336.18 o 4 2 -29 354.97 3.04 403.60 o 6 2 -29 172.19 277.27 335.27 o 10 2 -29 27.41 0.61 350.15 o 1 3 -29 381.29 0.30 369.28 o 3 3 -29 30.65 2.13 327.68 o 5 3 -29 98.69 256.62 326.77 o 7 3 -29 1410.89 1913.23 227.77 o 9 3 -29 365.84 616.79 234.45 o 0 4 -29 18.09 6.98 345.90 o 2 4 -29 1665.71 1239.05 235.05 o 4 4 -29 4.25 25.21 351.67 o 6 4 -29 583.69 705.77 232.93 o 8 4 -29 150.70 452.80 347.12 o 1 5 -29 1461.32 1243.60 236.57 o 3 5 -29 525.27 492.89 346.20 o 5 5 -29 129.35 3.04 353.19 o 7 5 -29 1246.44 1126.38 232.02 o 0 6 -29 1625.47 1472.28 235.66 o 2 6 -29 2128.58 2091.80 253.58 o 4 6 -29 1719.58 1739.52 247.20 o 6 6 -29 52.91 5.47 367.46 o 1 7 -29 440.21 505.64 342.86 o 3 7 -29 895.29 83.21 376.27 o 5 7 -29 2207.84 2599.26 255.10 o 0 8 -29 219.97 125.12 359.87 o 2 8 -29 265.38 4.25 365.94 o 4 8 -29 565.96 264.51 395.71 o 0 0 -28 2151.38 1963.65 210.15 o 2 0 -28 715.05 983.65 204.69 o 4 0 -28 3512.94 4758.49 246.29 o 6 0 -28 3130.27 3523.08 245.68 o 8 0 -28 157.93 1.21 330.11 o 10 0 -28 8624.58 7190.42 295.49 o 1 1 -28 3084.21 2609.44 383.71 o 3 1 -28 6193.85 5275.29 181.11 o 5 1 -28 437.49 310.39 276.51 o 7 1 -28 60.93 117.20 230.03 o 9 1 -28 1524.28 902.11 314.32 o 11 1 -28 1743.47 1535.08 183.82 o 0 2 -28 92.46 82.91 309.15 o 2 2 -28 4194.25 3805.21 249.63 o 4 2 -28 1005.07 1150.67 220.48 o 6 2 -28 16.40 147.59 314.01 o 8 2 -28 811.01 518.09 220.48 o 10 2 -28 8.45 479.83 354.10 o 1 3 -28 1003.03 860.04 213.49 o 3 3 -28 1972.79 1873.15 211.67 o 5 3 -28 1648.13 2207.51 225.94 o 7 3 -28 220.83 485.29 216.53 o 9 3 -28 80.29 323.43 351.97 o 11 3 -28 688.76 888.59 245.99 o 0 4 -28 11101.17 11415.32 362.30 o 2 4 -28 1240.63 806.59 222.30 o 4 4 -28 779.57 489.85 220.17 o 6 4 -28 2054.12 1450.72 245.08 o 8 4 -28 25.83 0.61 348.03 o 10 4 -28 1374.17 785.03 371.41 o 1 5 -28 695.09 1028.59 208.63 o 3 5 -28 6829.38 5996.32 271.80 o 5 5 -28 140.61 442.17 218.35 o 7 5 -28 130.13 0.61 343.47 o 9 5 -28 517.64 1075.97 233.54 o 0 6 -28 707.36 946.60 227.16 o 2 6 -28 4498.99 4112.84 262.08 o 4 6 -28 4333.56 5142.96 276.05 o 6 6 -28 20.83 418.79 346.20 o 8 6 -28 689.09 659.61 351.06 o 1 7 -28 55.82 0.61 329.50 o 3 7 -28 3869.03 3194.80 257.53 o 5 7 -28 715.28 670.24 243.56 o 7 7 -28 298.67 12.75 356.83 o 0 8 -28 361.14 904.69 228.68 o 2 8 -28 1009.74 1208.37 239.91 o 4 8 -28 1049.90 1129.72 242.65 o 6 8 -28 3887.19 4102.52 292.15 o 1 9 -28 3454.61 3954.02 281.52 o 3 9 -28 1308.48 1390.28 246.29 o 1 1 -27 531.81 297.41 231.71 o 3 1 -27 191.17 123.60 249.48 o 5 1 -27 2040.26 1965.20 1088.57 o 7 1 -27 108.24 0.30 248.41 o 9 1 -27 89.40 377.18 219.57 o 11 1 -27 1317.96 1135.21 339.07 o 0 2 -27 1583.24 1823.04 208.63 o 2 2 -27 632.45 4.25 418.18 o 4 2 -27 719.64 274.53 327.38 o 6 2 -27 625.51 1.21 335.58 o 8 2 -27 379.47 322.82 319.18 o 10 2 -27 255.84 0.61 325.25 o 12 2 -27 104.49 417.27 235.97 o 1 3 -27 1858.46 1748.94 225.94 o 3 3 -27 1041.04 1250.59 206.81 o 5 3 -27 129.79 4.25 334.97 o 7 3 -27 1033.92 1269.42 218.66 o 9 3 -27 498.40 88.07 347.12 o 11 3 -27 421.22 11.24 349.24 o 0 4 -27 1078.90 45.55 341.35 o 2 4 -27 175.55 345.90 315.23 o 4 4 -27 653.60 511.11 333.15 o 6 4 -27 65.29 10.93 331.02 o 8 4 -27 91.75 6.38 334.36 o 10 4 -27 262.94 182.52 357.74 o 1 5 -27 1808.94 2003.13 224.73 o 3 5 -27 1386.79 1364.17 225.03 o 5 5 -27 141.11 501.39 329.20 o 7 5 -27 95.77 47.68 321.00 o 9 5 -27 49.28 57.40 340.74 o 11 5 -27 375.43 0.61 369.59 o 0 6 -27 201.63 115.40 324.64 o 2 6 -27 714.25 985.47 219.26 o 4 6 -27 613.75 375.36 218.35 o 6 6 -27 13.06 9.11 343.77 o 8 6 -27 53.02 55.57 335.58 o 10 6 -27 259.24 59.52 374.14 o 1 7 -27 102.09 13.67 323.73 o 3 7 -27 3241.36 3575.92 247.51 o 5 7 -27 556.34 359.87 341.65 o 7 7 -27 794.10 1048.03 238.39 o 9 7 -27 259.04 331.02 243.56 o 0 8 -27 33.70 188.29 338.92 o 2 8 -27 38.52 495.92 333.45 o 4 8 -27 88.04 161.87 349.85 o 6 8 -27 2481.93 2682.78 274.23 o 8 8 -27 833.29 769.24 392.06 o 1 9 -27 172.63 10.02 333.45 o 3 9 -27 444.01 339.22 353.19 o 5 9 -27 732.03 1060.48 244.17 o 0 10 -27 2162.88 2484.17 255.71 o 2 10 -27 858.45 803.25 249.02 o 4 10 -27 259.74 103.25 383.56 o 0 0 -26 1388.58 969.07 191.32 o 2 0 -26 5470.17 5879.40 229.28 o 4 0 -26 911.58 812.67 194.36 o 6 0 -26 8781.17 10008.64 305.81 o 8 0 -26 3895.08 4631.24 248.42 o 10 0 -26 959.55 651.11 359.87 o 12 0 -26 1172.46 620.13 379.91 o 1 1 -26 1050.74 1056.95 635.47 o 3 1 -26 2188.61 2569.01 154.73 o 5 1 -26 1959.95 2144.93 1166.92 o 7 1 -26 5806.11 4524.32 734.77 o 9 1 -26 171.95 176.87 228.36 o 11 1 -26 65.75 0.61 241.19 o 13 1 -26 763.91 404.39 269.82 o 0 2 -26 1124.22 18.83 317.05 o 2 2 -26 2716.15 1967.59 210.46 o 4 2 -26 746.69 481.95 313.10 o 6 2 -26 7178.46 6615.23 269.67 o 8 2 -26 533.48 510.20 211.37 o 10 2 -26 575.76 641.69 328.59 o 12 2 -26 93.08 368.37 348.33 o 1 3 -26 9277.54 10115.84 278.79 o 3 3 -26 3798.30 3896.32 225.94 o 5 3 -26 30596.23 29629.61 621.35 o 7 3 -26 2866.01 2971.28 233.54 o 9 3 -26 3268.27 3449.29 247.51 o 11 3 -26 962.63 837.87 236.88 o 0 4 -26 21280.34 21902.27 541.78 o 2 4 -26 337.85 480.43 318.26 o 4 4 -26 20771.41 19413.55 532.67 o 6 4 -26 10404.35 9560.40 297.31 o 8 4 -26 2008.55 1700.04 229.28 o 10 4 -26 1426.18 1283.08 240.82 o 12 4 -26 316.92 152.76 370.80 o 1 5 -26 9623.18 9324.74 276.05 o 3 5 -26 2411.09 2498.74 226.85 o 5 5 -26 8648.26 8704.61 286.07 o 7 5 -26 2858.29 3247.64 240.52 o 9 5 -26 3929.44 3824.95 257.53 o 11 5 -26 35.65 76.83 361.08 o 0 6 -26 208.25 164.60 316.44 o 2 6 -26 678.69 10.93 326.16 o 4 6 -26 1346.46 1225.08 227.46 o 6 6 -26 1043.41 942.95 219.87 o 8 6 -26 1732.93 1527.25 234.45 o 10 6 -26 120.95 4.56 367.46 o 1 7 -26 347.68 226.55 317.66 o 3 7 -26 134.73 190.11 328.59 o 5 7 -26 1423.32 1552.15 236.27 o 7 7 -26 8789.27 7334.37 302.47 o 9 7 -26 440.26 465.86 361.39 o 0 8 -26 1699.53 1995.84 232.93 o 2 8 -26 895.38 134.23 352.58 o 4 8 -26 1710.30 2187.77 235.36 o 6 8 -26 2087.05 2521.22 255.71 o 8 8 -26 6910.64 7087.16 308.24 o 1 9 -26 40.67 2.43 345.90 o 3 9 -26 2700.31 2531.54 255.71 o 5 9 -26 284.86 495.31 355.01 o 7 9 -26 1063.49 1227.20 251.15 o 0 10 -26 495.58 313.10 360.17 o 2 10 -26 998.64 968.46 244.47 o 4 10 -26 1629.70 1705.81 247.20 o 6 10 -26 2717.44 2517.27 276.36 o 1 11 -26 1342.74 1470.76 253.28 o 1 1 -25 2148.14 2407.42 896.64 o 3 1 -25 188.37 139.20 250.71 o 5 1 -25 29.33 1.90 256.64 o 7 1 -25 1668.66 929.43 567.29 o 9 1 -25 814.97 325.50 312.49 o 11 1 -25 118.80 74.17 232.23 o 13 1 -25 597.92 378.53 299.74 o 0 2 -25 4320.83 3217.57 220.78 o 2 2 -25 548.65 2.43 305.21 o 4 2 -25 399.88 128.46 292.45 o 6 2 -25 1219.55 1143.69 209.54 o 8 2 -25 278.57 211.67 293.36 o 10 2 -25 26.33 0.30 325.55 o 1 3 -25 975.35 386.29 306.72 o 3 3 -25 131.74 6.98 308.85 o 5 3 -25 4275.18 3853.50 248.72 o 7 3 -25 255.24 477.70 198.61 o 9 3 -25 1396.97 1066.25 224.12 o 11 3 -25 172.91 79.87 343.47 o 13 3 -25 224.81 0.30 362.91 o 0 4 -25 2519.80 1700.35 239.31 o 2 4 -25 812.77 777.74 197.09 o 4 4 -25 2043.62 1587.07 231.11 o 6 4 -25 978.38 6.07 349.24 o 8 4 -25 212.42 174.62 321.00 o 10 4 -25 162.54 462.52 321.00 o 12 4 -25 86.84 358.35 353.49 o 1 5 -25 370.58 837.87 192.54 o 3 5 -25 1795.34 2343.86 214.40 o 5 5 -25 5019.18 5122.61 259.96 o 7 5 -25 689.01 867.94 209.85 o 9 5 -25 576.28 554.23 347.12 o 11 5 -25 367.53 278.48 244.17 o 0 6 -25 1310.71 2088.46 206.81 o 2 6 -25 2047.71 1982.78 214.71 o 4 6 -25 1736.27 1581.91 219.87 o 6 6 -25 1064.20 1372.37 223.51 o 8 6 -25 1463.92 1807.25 231.41 o 10 6 -25 258.36 298.22 352.89 o 12 6 -25 24.14 1.52 364.43 o 1 7 -25 1904.79 1820.61 217.14 o 3 7 -25 2339.26 2881.39 232.02 o 5 7 -25 1244.53 688.76 366.25 o 7 7 -25 5483.75 5561.74 281.82 o 9 7 -25 173.08 462.52 364.12 o 11 7 -25 313.14 258.13 396.31 o 0 8 -25 718.67 643.21 215.01 o 2 8 -25 1791.65 1909.59 225.64 o 4 8 -25 1429.40 1378.74 239.00 o 6 8 -25 2188.57 1941.17 253.58 o 8 8 -25 3006.63 2796.36 281.21 o 10 8 -25 738.15 278.18 401.78 o 1 9 -25 867.73 1236.31 221.08 o 3 9 -25 363.56 275.75 341.65 o 5 9 -25 230.10 332.23 350.76 o 7 9 -25 1492.94 1262.73 252.97 o 9 9 -25 352.78 537.22 382.65 o 0 10 -25 809.26 1188.63 229.89 o 2 10 -25 458.94 493.80 232.32 o 4 10 -25 1448.24 1158.27 243.56 o 6 10 -25 759.16 1052.28 251.15 o 1 11 -25 1333.08 1349.29 244.17 o 3 11 -25 4573.90 5183.34 286.68 o 5 11 -25 7542.90 8096.32 328.89 o 0 0 -24 1240.88 1184.99 179.78 o 2 0 -24 21661.12 19875.16 468.29 o 4 0 -24 164.19 23.08 266.33 o 6 0 -24 31543.88 30002.84 590.98 o 8 0 -24 70658.84 73222.80 880.09 o 10 0 -24 343.63 669.63 321.91 o 12 0 -24 9309.55 8458.01 303.08 o 14 0 -24 3044.17 3347.85 252.36 o 1 1 -24 3464.40 3032.12 400.26 o 3 1 -24 9957.75 9683.44 206.70 o 5 1 -24 9993.64 8413.87 252.36 o 7 1 -24 30643.33 27549.46 714.12 o 9 1 -24 7339.15 7341.50 196.64 o 11 1 -24 157.58 3.64 240.74 o 13 1 -24 6610.81 6768.98 206.25 o 0 2 -24 6073.16 5248.33 236.27 o 2 2 -24 132.81 31.28 274.84 o 4 2 -24 1041.15 636.53 268.16 o 6 2 -24 690.93 994.58 203.17 o 8 2 -24 4176.54 4339.09 235.66 o 10 2 -24 1497.24 1962.43 224.73 o 12 2 -24 71.47 2.73 342.56 o 14 2 -24 472.38 458.27 367.46 o 1 3 -24 12110.56 11495.80 369.28 o 3 3 -24 31578.33 30828.88 580.35 o 5 3 -24 9635.53 9757.79 325.25 o 7 3 -24 5876.17 6320.96 255.71 o 9 3 -24 576.49 891.93 213.49 o 11 3 -24 221.30 26.72 340.74 o 13 3 -24 685.65 305.21 355.31 o 0 4 -24 61641.46 62220.18 781.69 o 2 4 -24 28.13 20.65 291.24 o 4 4 -24 29415.07 28835.47 569.41 o 6 4 -24 18355.07 16982.53 427.59 o 8 4 -24 176.85 452.19 303.69 o 10 4 -24 111.91 393.58 321.00 o 12 4 -24 101.95 2.43 336.49 o 14 4 -24 8888.04 9227.86 335.27 o 1 5 -24 8966.42 9422.83 264.21 o 3 5 -24 4299.36 3669.46 228.07 o 5 5 -24 3489.67 4010.81 232.62 o 7 5 -24 680.47 772.58 213.80 o 9 5 -24 1328.01 1440.39 226.55 o 11 5 -24 687.04 639.26 355.31 o 13 5 -24 128.78 204.99 377.48 o 0 6 -24 5043.91 5892.76 239.91 o 2 6 -24 66.48 14.88 299.44 o 4 6 -24 2543.43 2398.83 222.60 o 6 6 -24 3952.71 4864.78 250.54 o 8 6 -24 1717.36 1591.63 229.28 o 10 6 -24 438.54 699.09 223.51 o 12 6 -24 235.20 303.99 362.91 o 1 7 -24 393.35 489.24 303.38 o 3 7 -24 7753.02 9545.52 300.35 o 5 7 -24 15300.84 15547.91 433.06 o 7 7 -24 13579.63 13809.90 392.97 o 9 7 -24 8765.02 8719.49 317.96 o 11 7 -24 1711.66 2110.63 254.79 o 0 8 -24 5289.12 6053.71 253.58 o 2 8 -24 3513.78 3927.29 239.00 o 4 8 -24 155.60 151.84 330.41 o 6 8 -24 13721.59 14917.15 457.96 o 8 8 -24 26505.94 27451.56 660.82 o 10 8 -24 1120.15 647.77 261.17 o 1 9 -24 3705.30 3605.08 248.42 o 3 9 -24 3198.00 3310.20 247.20 o 5 9 -24 3164.03 2955.79 241.13 o 7 9 -24 7379.09 6664.13 296.70 o 9 9 -24 2363.01 2037.75 266.03 o 0 10 -24 158.75 425.47 337.09 o 2 10 -24 282.06 176.14 347.12 o 4 10 -24 1594.81 1906.86 236.88 o 6 10 -24 285.00 101.74 354.40 o 8 10 -24 1550.94 1503.56 252.67 o 1 11 -24 4877.61 5096.49 282.13 o 3 11 -24 7912.51 8483.22 308.85 o 5 11 -24 1337.74 1102.99 250.85 o 7 11 -24 1042.55 438.53 404.51 o 0 12 -24 10691.38 11455.41 352.28 o 2 12 -24 7.05 313.71 364.12 o 4 12 -24 4809.66 5017.83 291.84 o 1 1 -23 1491.74 858.78 553.17 o 3 1 -23 684.32 287.32 229.27 o 5 1 -23 1399.94 384.06 288.96 o 7 1 -23 276.87 1.04 286.78 o 9 1 -23 3326.24 3146.16 388.26 o 11 1 -23 865.35 801.51 185.88 o 13 1 -23 614.67 399.48 261.87 o 15 1 -23 247.80 196.06 258.60 o 0 2 -23 3358.43 3228.20 202.86 o 2 2 -23 643.18 541.78 174.62 o 4 2 -23 883.45 716.40 179.18 o 6 2 -23 1375.57 1026.46 197.40 o 8 2 -23 636.20 111.15 300.35 o 10 2 -23 153.88 0.30 317.35 o 12 2 -23 89.82 0.61 331.02 o 14 2 -23 476.00 665.38 354.10 o 1 3 -23 6527.13 6766.77 234.14 o 3 3 -23 3600.57 3353.02 207.72 o 5 3 -23 362.33 231.11 273.93 o 7 3 -23 2765.60 2625.99 218.35 o 9 3 -23 1449.96 1618.05 205.60 o 11 3 -23 675.80 554.53 215.01 o 13 3 -23 830.20 1045.60 229.59 o 0 4 -23 5591.07 5226.77 240.22 o 2 4 -23 97.52 165.51 176.14 o 4 4 -23 4557.30 4229.46 225.03 o 6 4 -23 1193.88 989.72 199.52 o 8 4 -23 303.79 314.32 303.99 o 10 4 -23 45.73 321.00 315.23 o 12 4 -23 24.67 518.70 331.02 o 14 4 -23 821.44 576.70 409.67 o 1 5 -23 3439.85 3377.31 218.05 o 3 5 -23 4105.28 4408.03 217.14 o 5 5 -23 2467.90 2861.95 209.85 o 7 5 -23 4767.35 4904.86 244.47 o 9 5 -23 1594.25 1405.77 215.92 o 11 5 -23 800.09 681.48 358.66 o 13 5 -23 380.42 166.42 360.78 o 0 6 -23 6712.87 7402.39 245.38 o 2 6 -23 2887.09 3038.09 212.89 o 4 6 -23 1420.59 1520.26 201.65 o 6 6 -23 3332.88 3745.69 235.05 o 8 6 -23 3147.09 3037.49 230.80 o 10 6 -23 611.48 1030.72 219.26 o 12 6 -23 578.86 582.47 239.61 o 1 7 -23 2339.69 3173.23 217.44 o 3 7 -23 3667.57 4175.71 227.46 o 5 7 -23 7086.83 7023.09 266.64 o 7 7 -23 9543.54 9587.43 299.44 o 9 7 -23 2947.18 2469.59 260.56 o 11 7 -23 973.48 969.68 243.56 o 13 7 -23 639.17 633.49 415.14 o 0 8 -23 4203.83 3991.07 238.70 o 2 8 -23 1436.90 1562.17 211.97 o 4 8 -23 793.24 506.55 338.61 o 6 8 -23 9464.21 10027.47 328.29 o 8 8 -23 10016.41 10913.63 329.20 o 10 8 -23 125.73 544.82 235.66 o 12 8 -23 4171.92 4727.51 307.33 o 1 9 -23 564.16 308.24 321.91 o 3 9 -23 215.55 152.45 330.11 o 5 9 -23 4182.31 4046.94 253.58 o 7 9 -23 2413.10 2149.81 250.54 o 9 9 -23 3125.83 2933.62 273.02 o 11 9 -23 1015.21 1530.28 260.26 o 0 10 -23 1138.87 1480.48 219.87 o 2 10 -23 1052.28 993.97 226.55 o 4 10 -23 141.57 346.81 344.38 o 6 10 -23 255.67 231.71 352.28 o 8 10 -23 122.92 0.30 365.34 o 10 10 -23 273.55 642.00 251.76 o 1 11 -23 3237.53 3657.92 258.13 o 3 11 -23 3636.34 3189.33 257.22 o 5 11 -23 3098.77 3010.76 258.13 o 7 11 -23 540.76 85.94 363.82 o 0 12 -23 13612.34 14232.33 425.16 o 2 12 -23 32.21 529.63 345.90 o 4 12 -23 7017.84 6706.34 305.81 o 6 12 -23 2491.75 2148.29 262.69 o 1 13 -23 803.33 947.81 251.15 o 0 0 -22 25727.58 25750.30 503.51 o 2 0 -22 1787.02 2671.24 185.55 o 4 0 -22 696.75 1017.05 167.03 o 6 0 -22 71328.31 67994.80 774.10 o 8 0 -22 94200.87 93230.35 941.74 o 10 0 -22 107.12 418.79 317.35 o 12 0 -22 20066.54 18678.63 485.60 o 14 0 -22 14311.18 12288.12 362.91 o 1 1 -22 29718.18 28192.97 1168.74 o 3 1 -22 22.57 125.76 137.04 o 5 1 -22 37486.84 35134.05 566.98 o 7 1 -22 16534.18 15713.41 314.12 o 9 1 -22 14467.63 14330.25 285.04 o 11 1 -22 13063.49 12394.28 271.95 o 13 1 -22 8924.32 8950.83 384.62 o 15 1 -22 2423.69 2378.12 382.95 o 0 2 -22 955.08 309.15 248.42 o 2 2 -22 12304.91 13814.76 402.39 o 4 2 -22 10075.69 10769.08 329.81 o 6 2 -22 5147.23 5797.40 227.77 o 8 2 -22 977.56 1015.23 203.77 o 10 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8120.01 296.10 o 1 9 6 9100.00 8216.28 206.20 o 3 9 6 19913.83 18890.90 358.35 o 5 9 6 5333.78 5634.02 173.10 o 7 9 6 18329.72 17758.45 397.83 o 9 9 6 581.96 497.74 160.65 o 11 9 6 4833.29 5123.21 219.87 o 13 9 6 3511.06 3748.12 222.60 o 15 9 6 3670.90 3528.85 248.11 o 17 9 6 303.76 215.01 357.74 o 0 10 6 2910.81 3073.32 155.49 o 2 10 6 1965.85 2150.11 146.07 o 4 10 6 4872.20 4845.34 174.01 o 6 10 6 19913.43 19285.39 433.67 o 8 10 6 347.10 7.90 253.58 o 10 10 6 4152.17 3926.38 217.14 o 12 10 6 7523.81 7852.46 264.21 o 14 10 6 1447.77 1606.51 225.94 o 16 10 6 179.99 4.56 345.60 o 1 11 6 2014.30 2228.16 162.78 o 3 11 6 58.76 13.06 225.03 o 5 11 6 123.17 79.57 221.08 o 7 11 6 2158.17 1949.07 182.21 o 9 11 6 12136.63 11068.82 351.06 o 11 11 6 3769.76 3496.66 225.03 o 13 11 6 800.25 959.65 223.82 o 15 11 6 61.65 59.52 343.17 o 0 12 6 1114.24 1106.03 155.49 o 2 12 6 5711.74 5844.78 204.99 o 4 12 6 252.49 425.77 225.03 o 6 12 6 1296.34 1536.96 182.52 o 8 12 6 841.87 378.09 298.53 o 10 12 6 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7 103.42 191.93 239.31 o 14 4 7 931.18 780.78 186.46 o 16 4 7 671.46 741.00 201.04 o 18 4 7 346.68 305.51 334.66 o 1 5 7 19337.68 23771.78 319.48 o 3 5 7 12175.56 10074.54 235.66 o 5 5 7 3208.10 2763.56 112.67 o 7 5 7 13378.04 13965.39 314.32 o 9 5 7 9985.87 10415.28 272.10 o 11 5 7 609.21 789.59 153.67 o 13 5 7 2992.58 2885.64 196.49 o 15 5 7 1012.18 782.60 212.28 o 17 5 7 280.21 350.15 301.87 o 0 6 7 9710.90 9483.87 179.18 o 2 6 7 10246.66 9380.62 222.30 o 4 6 7 24072.54 23490.87 345.29 o 6 6 7 818.63 1229.63 114.79 o 8 6 7 15344.57 14979.10 362.91 o 10 6 7 960.06 689.68 155.18 o 12 6 7 525.03 537.22 170.37 o 14 6 7 4991.92 5239.22 240.22 o 16 6 7 1114.07 987.29 208.94 o 18 6 7 448.45 514.75 351.37 o 1 7 7 31350.52 28157.94 384.17 o 3 7 7 21687.52 19629.17 337.09 o 5 7 7 14862.30 13134.80 309.76 o 7 7 7 16709.14 17081.23 367.16 o 9 7 7 5443.16 5101.35 177.66 o 11 7 7 18.30 34.01 249.63 o 13 7 7 204.06 455.84 272.71 o 17 7 7 1256.71 1512.37 236.57 o 0 8 7 5927.05 5915.54 206.51 o 2 8 7 45562.18 42476.22 498.05 o 4 8 7 16171.82 15986.74 353.80 o 6 8 7 7937.04 7630.16 214.10 o 8 8 7 12749.33 12278.40 309.15 o 10 8 7 3552.01 3758.74 201.65 o 12 8 7 1624.47 1624.73 196.79 o 14 8 7 794.41 880.39 202.56 o 16 8 7 515.88 710.33 221.69 o 1 9 7 9334.94 9423.43 241.13 o 3 9 7 3809.10 3366.68 142.13 o 5 9 7 2196.17 1843.69 139.70 o 7 9 7 10720.99 10346.04 301.26 o 9 9 7 228.02 337.40 241.74 o 11 9 7 3084.73 2819.44 195.57 o 13 9 7 604.58 482.86 314.01 o 15 9 7 312.33 95.66 355.01 o 0 10 7 366.52 290.63 195.88 o 2 10 7 4208.67 4417.75 160.04 o 4 10 7 8056.99 7550.89 235.05 o 6 10 7 1900.35 2129.46 169.76 o 8 10 7 8051.22 7633.20 238.39 o 10 10 7 2252.86 2313.19 200.74 o 12 10 7 2343.83 2394.58 230.50 o 14 10 7 1401.39 1670.89 230.50 o 16 10 7 2688.04 2648.77 260.26 o 1 11 7 1431.08 1443.12 150.93 o 3 11 7 5542.99 5891.55 208.94 o 5 11 7 3806.49 3616.32 192.84 o 7 11 7 10118.39 9139.18 262.39 o 9 11 7 3162.36 3223.34 211.06 o 11 11 7 3897.02 3705.60 236.27 o 13 11 7 1066.34 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5 16 2769.28 2221.48 206.81 o 13 5 16 7822.38 8208.99 283.95 o 15 5 16 24.19 198.31 321.30 o 0 6 16 208.59 3.64 201.65 o 2 6 16 6360.52 6000.87 168.55 o 4 6 16 7948.76 7815.71 247.51 o 6 6 16 4616.07 4380.09 189.20 o 8 6 16 232.88 330.41 254.49 o 10 6 16 41.38 19.44 275.75 o 12 6 16 1715.77 1907.16 221.39 o 14 6 16 8018.16 8545.78 298.53 o 1 7 16 3661.06 3295.92 170.67 o 3 7 16 12508.13 10886.60 314.92 o 5 7 16 13096.41 13077.71 387.81 o 7 7 16 688.51 877.66 173.41 o 9 7 16 14868.65 15177.71 450.07 o 11 7 16 1485.65 1133.06 215.62 o 13 7 16 766.18 215.31 360.78 o 15 7 16 1632.52 1744.99 251.76 o 0 8 16 9952.23 8971.85 295.18 o 2 8 16 2689.37 2593.80 172.80 o 4 8 16 84249.02 81414.47 812.97 o 6 8 16 67.51 7.59 267.25 o 8 8 16 3161.34 2958.83 205.60 o 10 8 16 12978.95 12753.07 360.78 o 12 8 16 310.51 324.34 297.01 o 14 8 16 344.71 633.49 221.08 o 1 9 16 10323.78 9906.60 303.99 o 3 9 16 5744.97 5393.19 201.35 o 5 9 16 4511.53 4173.58 203.17 o 7 9 16 1.01 7.29 269.67 o 9 9 16 12756.86 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894.97 225.03 o 3 15 16 810.06 239.61 354.71 o 5 15 16 4945.47 4763.65 290.33 o 1 1 17 2186.26 2431.59 98.24 o 3 1 17 6279.30 6560.70 3373.97 o 5 1 17 3834.33 4236.62 2196.73 o 7 1 17 1685.34 2834.03 1349.89 o 9 1 17 1473.30 1280.85 126.48 o 11 1 17 433.71 174.81 202.23 o 13 1 17 136.34 2.44 214.85 o 15 1 17 49.05 51.93 338.31 o 0 2 17 2610.30 2403.39 143.64 o 2 2 17 2178.50 1784.47 141.52 o 4 2 17 1561.51 1708.24 140.61 o 6 2 17 1360.14 1265.16 156.70 o 8 2 17 1556.58 1906.86 163.08 o 10 2 17 1245.96 1833.67 184.64 o 12 2 17 2604.59 2569.81 218.66 o 14 2 17 1043.40 1498.40 227.77 o 16 2 17 106.87 363.21 345.90 o 1 3 17 78.64 27.64 191.63 o 3 3 17 5802.46 5920.09 174.32 o 5 3 17 2965.35 3257.05 163.99 o 7 3 17 433.28 345.90 242.04 o 9 3 17 481.85 200.13 281.21 o 11 3 17 1736.95 1891.98 208.33 o 13 3 17 1754.80 1873.45 238.39 o 15 3 17 27.42 242.65 335.88 o 0 4 17 42.97 180.69 200.74 o 2 4 17 646.76 832.10 134.53 o 4 4 17 896.08 975.45 142.73 o 6 4 17 940.80 834.84 157.31 o 8 4 17 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5.47 334.06 o 12 10 18 3719.71 3834.97 274.23 o 1 11 18 3269.01 3401.30 211.37 o 3 11 18 207.42 300.95 182.21 o 5 11 18 2582.71 2599.57 215.01 o 7 11 18 1635.10 1783.26 216.53 o 9 11 18 1543.38 1559.13 230.50 o 11 11 18 1959.65 2319.87 258.74 o 0 12 18 2884.84 2993.45 222.91 o 2 12 18 237.32 453.71 193.15 o 4 12 18 1590.01 1543.34 212.89 o 6 12 18 185.17 0.61 317.96 o 8 12 18 110.72 2.13 328.59 o 1 13 18 46.71 128.46 303.99 o 3 13 18 269.31 448.24 318.26 o 5 13 18 136.34 0.30 326.16 o 7 13 18 1150.46 1181.04 215.31 o 0 14 18 864.88 1141.56 222.60 o 2 14 18 8.34 0.30 329.20 o 4 14 18 263.21 0.61 346.51 o 6 14 18 352.22 373.54 351.37 o 1 15 18 392.53 545.12 354.10 o 1 1 19 9027.49 9199.70 4771.70 o 3 1 19 1342.67 960.78 507.16 o 5 1 19 1888.38 1800.10 550.59 o 7 1 19 887.82 639.87 174.62 o 9 1 19 62.36 42.18 218.02 o 11 1 19 945.73 1288.03 139.12 o 13 1 19 706.42 700.39 178.81 o 15 1 19 525.43 235.07 199.24 o 0 2 19 3589.40 4020.52 169.76 o 2 2 19 2104.94 2558.27 160.35 o 4 2 19 6098.65 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3 11 19 5829.86 5224.65 252.36 o 5 11 19 4584.28 4392.84 244.17 o 7 11 19 1530.21 1227.81 219.87 o 9 11 19 473.45 140.30 349.24 o 0 12 19 7297.77 7152.15 268.76 o 2 12 19 235.94 13.67 298.53 o 4 12 19 2338.46 1923.26 220.78 o 6 12 19 1554.75 1589.81 225.03 o 8 12 19 58.41 197.70 335.27 o 1 13 19 311.68 224.43 331.02 o 3 13 19 173.29 362.00 320.69 o 5 13 19 174.87 3.64 337.40 o 7 13 19 2797.04 2620.22 251.45 o 0 14 19 2964.34 2615.97 250.85 o 2 14 19 767.73 728.55 228.68 o 4 14 19 1242.30 1186.81 232.02 o 0 0 20 20473.43 22072.95 410.59 o 2 0 20 180990.42 176810.42 1068.37 o 4 0 20 33121.21 33282.06 519.00 o 6 0 20 30495.38 29650.87 528.11 o 8 0 20 23474.23 26672.60 541.78 o 10 0 20 4566.29 4190.59 237.48 o 12 0 20 2075.33 2273.10 221.69 o 14 0 20 3029.61 3353.32 256.92 o 1 1 20 26508.40 28226.28 3927.14 o 3 1 20 54264.88 52708.26 3530.22 o 5 1 20 362.87 605.57 374.75 o 7 1 20 21307.82 21924.50 517.18 o 9 1 20 16162.18 15161.39 323.82 o 11 1 20 264.97 349.94 216.86 o 13 1 20 2268.41 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380.86 4.86 301.56 o 4 10 20 13175.88 12450.29 348.94 o 6 10 20 233.05 464.95 305.81 o 8 10 20 685.24 269.37 339.22 o 10 10 20 3631.16 3805.21 268.46 o 1 11 20 1842.26 1469.24 206.20 o 3 11 20 1524.81 1275.49 208.94 o 5 11 20 39.24 245.68 311.89 o 7 11 20 576.21 140.00 337.70 o 9 11 20 287.15 322.82 341.65 o 0 12 20 6753.03 6716.97 267.55 o 2 12 20 793.44 515.36 325.55 o 4 12 20 1215.70 1138.83 225.64 o 6 12 20 3378.29 3426.81 250.85 o 8 12 20 192.48 366.85 349.24 o 1 13 20 585.10 581.87 325.55 o 3 13 20 102.93 2.73 326.16 o 5 13 20 663.53 627.12 345.90 o 0 14 20 408.30 729.15 347.12 o 2 14 20 817.97 276.36 368.98 o 1 1 21 3014.52 2213.34 1161.76 o 3 1 21 5498.14 4358.41 2246.53 o 5 1 21 95.81 55.52 193.32 o 7 1 21 1813.16 1060.48 630.15 o 9 1 21 171.85 0.91 346.20 o 11 1 21 645.23 668.80 146.87 o 13 1 21 58.00 227.17 182.70 o 0 2 21 1939.69 1640.83 164.90 o 2 2 21 2001.43 1886.81 159.74 o 4 2 21 298.04 15.79 247.81 o 6 2 21 79.32 242.95 256.62 o 8 2 21 1886.80 2260.35 193.45 o 10 2 21 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