# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' sb200 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 2063.77 _exptl_crystal_F_000 6304.00 _reflns_d_resolution_high 0.7632 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 25.1790 _cell_length_b 13.8220 _cell_length_c 24.1120 _cell_angle_alpha 90.000 _cell_angle_beta 99.580 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 10 0 0 316867.25 279873.00 928.56 o 14 0 0 1774589.63 2000169.38 1252.92 o 16 0 0 22973.44 19275.06 937.06 o 18 0 0 181298.88 184307.42 1844.04 o 20 0 0 44153.79 50211.45 2915.79 o 22 0 0 294765.50 316872.38 2878.93 o 24 0 0 33083.13 35127.21 2919.54 o 26 0 0 74035.05 79729.35 3706.31 o 28 0 0 138498.39 142620.22 4209.62 o 30 0 0 3393.07 3995.76 3371.17 o 32 0 0 3268.44 2882.71 3339.32 o 7 1 0 17578.41 19475.73 812.16 o 9 1 0 82.78 814.81 280.25 o 11 1 0 679.08 1199.28 315.68 o 13 1 0 252201.53 256176.91 1933.80 o 15 1 0 47648.91 49826.75 649.32 o 17 1 0 81652.50 84016.24 1299.35 o 19 1 0 11814.42 15037.91 933.78 o 21 1 0 56241.28 59514.39 1418.33 o 23 1 0 44507.86 50070.86 1382.39 o 25 1 0 7723.35 6850.63 888.03 o 27 1 0 50281.19 53469.05 893.44 o 29 1 0 27192.35 31308.72 1360.11 o 31 1 0 7.72 -244.73 1048.91 o 6 2 0 93368.01 94740.03 1392.65 o 8 2 0 124276.75 137263.70 1190.56 o 10 2 0 40676.66 44179.66 529.17 o 12 2 0 73067.39 80336.95 496.53 o 14 2 0 77257.00 83907.93 582.61 o 16 2 0 235.22 519.03 1016.20 o 18 2 0 23051.82 23715.28 916.60 o 20 2 0 8251.97 9701.75 898.96 o 22 2 0 20674.62 21773.37 851.92 o 24 2 0 6553.44 6283.55 882.42 o 26 2 0 4696.91 5974.45 920.49 o 28 2 0 2480.98 3657.42 878.59 o 30 2 0 1195.68 2393.77 2339.32 o 32 2 0 1493.94 829.14 3040.83 o 1 3 0 891888.19 777356.81 2308.80 o 3 3 0 134953.91 128286.79 1265.60 o 5 3 0 699407.50 675502.06 879.70 o 7 3 0 7520.38 8852.33 378.69 o 9 3 0 65916.58 69816.93 514.09 o 11 3 0 130365.46 137467.63 980.70 o 13 3 0 343926.56 313144.34 1825.81 o 15 3 0 25667.89 26721.71 660.64 o 17 3 0 283892.72 297574.88 1161.34 o 19 3 0 46045.36 46957.59 1286.28 o 21 3 0 119331.59 124813.88 1437.71 o 23 3 0 49622.45 53338.73 1378.94 o 25 3 0 6866.11 7064.02 932.45 o 27 3 0 46631.40 49502.62 1374.78 o 29 3 0 31820.84 32365.87 1326.59 o 31 3 0 1728.12 325.23 916.40 o 0 4 0 4259126.50 3905016.00 2595.87 o 2 4 0 1418302.25 1321749.13 1924.53 o 4 4 0 82034.48 73587.84 650.24 o 6 4 0 331460.06 313171.25 786.67 o 8 4 0 380088.34 331671.09 824.29 o 10 4 0 37903.60 41335.91 653.27 o 12 4 0 81832.43 85505.26 516.72 o 14 4 0 292513.97 304217.84 1562.76 o 16 4 0 3723.14 3204.99 764.58 o 18 4 0 46797.32 52653.47 874.48 o 20 4 0 51530.69 56695.19 932.64 o 22 4 0 75336.34 76906.80 934.48 o 24 4 0 934.45 764.02 1107.27 o 26 4 0 7823.83 9572.99 880.04 o 28 4 0 39472.34 41137.28 919.42 o 30 4 0 5733.80 4421.60 984.23 o 1 5 0 438320.09 413004.75 964.95 o 3 5 0 145395.92 129127.38 932.30 o 5 5 0 40931.14 35198.92 566.34 o 7 5 0 13124.19 11624.71 404.14 o 9 5 0 17725.14 18101.59 496.62 o 11 5 0 2461.44 2642.61 381.88 o 13 5 0 29808.52 30036.87 474.66 o 15 5 0 8812.52 7354.00 580.34 o 17 5 0 1514.92 701.72 825.09 o 19 5 0 3578.35 2823.29 1014.46 o 21 5 0 2565.88 4086.16 1095.93 o 23 5 0 2522.63 1822.52 1361.31 o 25 5 0 3.61 849.47 1351.76 o 27 5 0 5954.99 5090.12 840.58 o 29 5 0 10792.55 12739.48 893.30 o 31 5 0 3587.22 3570.87 881.22 o 0 6 0 691505.81 640582.38 1168.52 o 2 6 0 142525.28 132483.72 1130.90 o 4 6 0 37541.63 33458.52 560.27 o 6 6 0 281577.94 277399.31 1058.02 o 8 6 0 395773.41 390896.50 1421.53 o 10 6 0 23902.55 22020.78 535.59 o 12 6 0 12323.52 12694.77 451.01 o 14 6 0 40983.98 43271.28 496.71 o 16 6 0 711.13 901.30 750.08 o 18 6 0 7345.96 7986.72 1198.43 o 20 6 0 56431.11 54152.93 963.73 o 22 6 0 46043.81 47423.17 974.36 o 24 6 0 121.66 19.71 2211.58 o 26 6 0 387.14 -56.81 2124.58 o 28 6 0 3525.93 1995.48 2081.53 o 30 6 0 405.75 -189.45 2846.18 o 1 7 0 1009.08 401.36 607.78 o 3 7 0 70512.62 66279.28 819.74 o 5 7 0 64077.69 55498.54 587.35 o 7 7 0 27232.47 25403.52 630.42 o 9 7 0 23901.20 20489.82 630.48 o 11 7 0 97564.48 86007.22 783.30 o 13 7 0 15765.89 15140.90 558.84 o 15 7 0 22103.44 21457.10 651.23 o 17 7 0 65707.96 66948.10 616.62 o 19 7 0 992.32 1409.35 1023.86 o 21 7 0 92663.93 88675.34 919.59 o 23 7 0 6542.97 5192.62 1607.57 o 25 7 0 1497.46 878.87 1991.73 o 27 7 0 2529.05 1959.93 2063.56 o 29 7 0 10713.43 11745.95 926.23 o 0 8 0 131957.58 128465.72 759.36 o 2 8 0 12969.33 10784.11 589.38 o 4 8 0 69606.13 62237.06 626.89 o 6 8 0 3967.37 3206.01 536.99 o 8 8 0 6078.70 4357.14 566.59 o 10 8 0 58081.29 50891.27 629.99 o 12 8 0 35160.84 32256.02 590.57 o 14 8 0 9904.60 7296.43 892.27 o 16 8 0 49564.24 41993.87 2801.63 o 18 8 0 74572.34 65347.79 2281.90 o 20 8 0 14.27 -133.65 1689.20 o 22 8 0 1489.72 194.33 1684.93 o 24 8 0 3219.43 2749.04 1420.86 o 26 8 0 2061.80 2029.13 1684.82 o 28 8 0 618.91 213.27 2252.68 o 1 9 0 150360.94 133697.23 3039.86 o 3 9 0 60108.27 54041.52 1722.71 o 5 9 0 3450.97 3013.49 525.30 o 7 9 0 18173.38 14982.67 906.93 o 9 9 0 3216.20 3058.40 624.21 o 11 9 0 23461.05 25790.72 1330.82 o 13 9 0 5444.23 4095.22 705.49 o 15 9 0 2193.45 1282.97 949.80 o 17 9 0 5865.25 5779.74 946.88 o 19 9 0 27603.72 26934.97 2097.81 o 21 9 0 9339.47 7971.18 1753.37 o 23 9 0 31.49 336.73 2148.52 o 25 9 0 1874.64 2507.23 2305.77 o 27 9 0 351.00 716.46 2302.43 o 0 10 0 20485.02 18639.75 1532.68 o 2 10 0 485.34 449.03 743.82 o 4 10 0 5612.21 5464.05 589.84 o 6 10 0 111767.81 107794.51 2352.05 o 8 10 0 45874.89 43744.06 1032.59 o 10 10 0 74.68 566.48 824.05 o 12 10 0 17092.90 17995.82 927.64 o 14 10 0 21008.13 20844.38 1100.74 o 16 10 0 16696.38 15557.04 1791.17 o 18 10 0 958.48 344.38 2103.56 o 20 10 0 9709.65 8484.72 1633.78 o 22 10 0 7919.45 3767.21 1730.76 o 24 10 0 3286.55 2524.95 1937.76 o 26 10 0 10689.13 11368.31 2840.62 o 1 11 0 480.90 89.01 1179.99 o 3 11 0 44495.21 39290.32 983.81 o 5 11 0 32892.34 30049.56 929.11 o 7 11 0 1616.91 2473.64 628.97 o 9 11 0 10983.75 10181.35 770.00 o 11 11 0 23801.28 26003.60 998.03 o 13 11 0 24779.24 25931.93 997.22 o 15 11 0 23070.43 24126.76 1175.34 o 17 11 0 40078.80 40577.43 1900.80 o 19 11 0 4338.76 3837.13 1778.37 o 21 11 0 9208.53 7410.11 2022.97 o 23 11 0 2195.56 1352.51 2294.44 o 25 11 0 735.20 337.86 2897.89 o 0 12 0 2591.74 2369.54 1362.54 o 2 12 0 2389.80 3082.22 850.25 o 4 12 0 73213.15 75998.87 1775.23 o 6 12 0 61355.30 70971.12 1376.96 o 8 12 0 37594.90 41762.81 1182.72 o 10 12 0 19795.40 19900.88 1001.08 o 12 12 0 17345.33 18310.31 984.35 o 14 12 0 15828.53 16684.55 1140.15 o 16 12 0 35408.96 41401.64 1659.63 o 18 12 0 37762.10 44083.98 3414.23 o 20 12 0 4806.67 4147.75 1987.19 o 22 12 0 2.20 90.29 2862.55 o 24 12 0 65.22 103.38 2913.55 o 1 13 0 11359.58 9157.53 1029.27 o 3 13 0 1240.11 324.23 1780.35 o 5 13 0 661.27 2139.47 764.72 o 7 13 0 3128.81 2937.19 866.09 o 9 13 0 5065.59 5005.24 861.28 o 11 13 0 490.41 230.89 1142.75 o 13 13 0 312.95 189.44 1311.77 o 15 13 0 9.95 650.39 1195.32 o 17 13 0 7850.82 8573.30 1325.69 o 19 13 0 11103.38 11602.51 2114.60 o 21 13 0 3657.48 3359.77 2695.70 o 0 14 0 454.71 906.21 1720.47 o 2 14 0 551.31 705.05 1007.83 o 4 14 0 173.68 290.86 1440.85 o 6 14 0 4209.29 3491.83 882.08 o 8 14 0 126.43 395.94 1177.01 o 10 14 0 1408.39 -290.37 1863.65 o 12 14 0 4838.68 4748.32 982.81 o 14 14 0 10904.98 13466.39 1337.74 o 16 14 0 12042.38 13633.10 1329.70 o 18 14 0 4580.25 4155.44 1917.76 o 20 14 0 779.10 463.94 3132.03 o 1 15 0 412.52 192.53 2371.35 o 3 15 0 9651.99 10656.45 1177.20 o 5 15 0 13001.28 12746.71 1209.38 o 7 15 0 3314.60 3977.30 1149.84 o 9 15 0 6962.99 7470.94 1097.49 o 11 15 0 5953.34 7018.77 1102.52 o 13 15 0 9302.37 12735.91 1416.11 o 15 15 0 14333.62 16856.19 1476.57 o 17 15 0 19098.44 20309.12 1621.88 o 0 16 0 183.31 -163.43 1838.34 o 2 16 0 3752.44 6095.71 1256.56 o 4 16 0 9386.94 11837.00 1327.14 o 6 16 0 517.53 359.18 2767.82 o 8 16 0 102.05 -151.41 1791.59 o 10 16 0 5426.56 5274.83 1486.08 o 12 16 0 2551.48 3424.80 1542.43 o 14 16 0 1396.54 1671.39 2125.59 o 1 17 0 1151.85 391.70 2767.35 o 3 17 0 23.40 779.62 2705.57 o 5 17 0 1315.30 3545.81 2260.17 o 7 17 0 4018.20 4314.77 2024.72 o 9 17 0 68.27 1520.16 2805.50 o 11 17 0 895.30 -112.81 2769.26 o 0 18 0 22.91 475.07 4221.59 o 2 18 0 21.24 2280.45 3104.27 o -31 1 1 660.20 1427.22 2430.31 o -29 1 1 9285.07 8817.40 1910.91 o -27 1 1 4802.39 7033.80 1702.24 o -25 1 1 74379.88 75968.23 2950.91 o -23 1 1 8476.35 8491.27 1338.19 o -21 1 1 74701.57 75294.20 2128.49 o -19 1 1 169977.23 176239.50 3281.88 o -17 1 1 18026.09 18881.23 833.78 o -15 1 1 8122.41 8321.73 945.59 o -13 1 1 298660.16 282355.56 682.41 o -11 1 1 655962.25 677753.81 682.80 o -9 1 1 22561.72 22967.46 536.91 o -7 1 1 747563.88 758229.44 1375.78 o 7 1 1 559858.31 570407.44 922.79 o 9 1 1 7294.19 7319.85 533.62 o 11 1 1 206908.92 223946.14 850.23 o 13 1 1 1084.09 1842.50 420.25 o 15 1 1 1980.52 2046.67 488.84 o 17 1 1 52415.86 53894.22 619.97 o 19 1 1 14928.57 15099.59 724.91 o 21 1 1 3559.96 3879.04 900.86 o 23 1 1 4730.67 3573.59 890.40 o 25 1 1 10127.45 9866.18 885.55 o 27 1 1 9472.58 10946.60 895.84 o 29 1 1 8710.95 8458.88 880.35 o 31 1 1 28.65 -218.67 2797.93 o -32 2 1 2.37 -132.47 2905.71 o -30 2 1 11870.95 11833.98 881.07 o -28 2 1 4492.53 5135.97 1676.33 o -26 2 1 34721.57 37434.62 922.45 o -24 2 1 48051.08 52938.49 971.22 o -22 2 1 17854.96 18767.06 896.01 o -20 2 1 174184.08 192375.55 1378.09 o -18 2 1 57610.87 54619.02 980.94 o -16 2 1 23301.48 23540.03 629.53 o -14 2 1 109092.74 114538.98 581.88 o -12 2 1 655690.50 674488.75 1665.13 o -10 2 1 451955.38 427825.91 1058.58 o -8 2 1 17497.57 17385.29 366.06 o 2 2 1 49923.12 46010.20 1004.24 o 4 2 1 204773.11 197721.44 1980.99 o 6 2 1 1196812.75 1073512.13 1798.59 o 8 2 1 330145.13 377957.38 1657.88 o 10 2 1 18707.19 20716.81 342.60 o 12 2 1 5265.48 5741.78 352.64 o 14 2 1 36649.50 39114.36 515.81 o 16 2 1 49541.45 47509.79 655.51 o 18 2 1 156304.17 161270.13 1434.76 o 20 2 1 16066.96 15160.97 861.34 o 22 2 1 866.10 683.35 1313.25 o 24 2 1 23764.42 26043.00 926.81 o 26 2 1 861.43 194.72 1917.40 o 28 2 1 7251.45 5950.29 915.91 o 30 2 1 6303.31 8208.57 923.01 o 32 2 1 3755.43 2813.29 2305.16 o -31 3 1 2180.86 4060.89 919.13 o -29 3 1 18876.61 21262.11 929.24 o -27 3 1 467.67 1263.92 2325.18 o -25 3 1 245.85 1707.19 1224.06 o -23 3 1 18775.87 21638.72 928.53 o -21 3 1 37575.63 38347.93 932.90 o -19 3 1 40490.51 45442.94 827.59 o -17 3 1 97927.33 106692.03 877.46 o -15 3 1 94341.27 96059.80 850.34 o -13 3 1 11247.90 12440.61 506.78 o -11 3 1 31692.59 33607.61 2162.51 o -9 3 1 726.52 743.77 416.97 o -7 3 1 48530.68 45364.03 508.19 o -5 3 1 39520.98 36487.07 631.26 o -3 3 1 257085.58 236404.50 1848.03 o -1 3 1 218575.59 198046.61 1843.42 o 1 3 1 33834.32 31043.95 903.28 o 3 3 1 1931.74 1998.47 403.14 o 5 3 1 54803.38 57130.88 591.40 o 7 3 1 78047.05 78243.61 1191.37 o 9 3 1 1349.80 1600.34 295.81 o 11 3 1 147105.33 160076.77 523.95 o 13 3 1 168619.08 177080.11 800.77 o 15 3 1 13493.57 14470.17 562.60 o 17 3 1 90709.60 93200.96 970.16 o 19 3 1 31047.90 33901.38 926.83 o 21 3 1 1375.46 968.53 1196.65 o 23 3 1 1926.91 666.70 1892.10 o 25 3 1 22499.43 23714.69 888.04 o 27 3 1 21302.18 23114.26 879.53 o 29 3 1 2948.89 1748.71 919.92 o 31 3 1 5406.01 3990.88 2150.54 o -30 4 1 5254.69 5471.48 1996.89 o -28 4 1 776.29 1326.26 2113.98 o -26 4 1 5509.50 5808.51 2104.93 o -24 4 1 50670.24 59820.34 4205.24 o -22 4 1 15515.57 14208.60 883.91 o -20 4 1 2591.38 2314.77 988.04 o -18 4 1 36307.03 38246.94 585.59 o -16 4 1 145250.95 153454.84 591.01 o -14 4 1 63854.68 64173.26 590.64 o -12 4 1 163015.28 170833.30 977.35 o -10 4 1 186655.72 174984.22 660.07 o -8 4 1 77942.89 76178.19 536.56 o -6 4 1 884.33 1825.55 365.80 o -4 4 1 354963.31 327611.59 922.36 o -2 4 1 975816.63 857153.38 1439.39 o 0 4 1 205035.20 203773.95 932.34 o 2 4 1 1148.16 1161.02 554.81 o 4 4 1 43135.21 39541.26 544.66 o 6 4 1 7893.37 7198.14 362.61 o 8 4 1 17967.78 17193.47 1336.77 o 10 4 1 393456.72 356951.31 494.93 o 12 4 1 480072.00 483118.63 1376.72 o 14 4 1 9831.33 9740.71 595.79 o 16 4 1 353.72 127.48 1824.00 o 18 4 1 37682.41 41417.17 3621.33 o 20 4 1 28889.57 34830.84 1876.46 o 22 4 1 15348.60 16491.28 1679.54 o 24 4 1 76161.65 91087.03 5145.60 o 26 4 1 47968.46 56732.89 2663.32 o 28 4 1 0.65 1787.68 1987.36 o 30 4 1 1024.49 1703.85 2259.13 o -31 5 1 2478.72 1750.91 2276.76 o -29 5 1 338.06 952.19 2122.77 o -27 5 1 369.58 374.97 2385.74 o -25 5 1 20538.80 21537.39 3020.19 o -23 5 1 2346.09 1883.56 1218.65 o -21 5 1 14967.75 12893.07 1440.54 o -19 5 1 8850.46 9034.88 898.71 o -17 5 1 7312.27 7895.04 871.90 o -15 5 1 10465.30 11166.64 1125.38 o -13 5 1 135216.67 120534.45 5782.20 o -11 5 1 291293.03 254996.78 5903.71 o -9 5 1 29727.19 27524.16 2135.59 o -7 5 1 14249.12 12523.83 748.84 o -5 5 1 215292.78 188115.02 973.28 o -3 5 1 609142.69 573118.81 1056.97 o -1 5 1 117810.28 109425.09 1124.37 o 1 5 1 3123.84 2714.01 407.07 o 3 5 1 26862.01 25368.84 517.15 o 5 5 1 17676.89 15620.08 1045.80 o 7 5 1 16903.30 16476.95 1195.68 o 9 5 1 180345.28 159139.44 3226.70 o 11 5 1 168808.75 159864.13 690.12 o 13 5 1 1117.34 1747.56 465.32 o 15 5 1 164.35 -10.26 830.38 o 17 5 1 113036.62 103295.77 10743.93 o 19 5 1 83689.09 97183.76 8714.65 o 21 5 1 11207.89 9393.96 1484.44 o 23 5 1 8863.65 8425.62 1365.82 o 25 5 1 244.51 419.00 1776.84 o 27 5 1 6737.67 7951.78 1952.76 o 29 5 1 1712.71 3178.92 2438.89 o 31 5 1 2892.04 1580.04 2265.95 o -30 6 1 6097.83 5569.07 2224.68 o -28 6 1 3494.79 2891.35 1908.37 o -26 6 1 601.12 -234.99 2104.17 o -24 6 1 1077.62 1889.51 1604.51 o -22 6 1 23961.04 29139.73 2024.79 o -20 6 1 7088.05 8545.94 1146.82 o -18 6 1 3919.50 3187.15 644.29 o -16 6 1 55363.84 56953.42 538.88 o -14 6 1 921.71 1232.83 561.21 o -12 6 1 110883.53 107494.50 716.96 o -10 6 1 4394.37 3337.79 440.71 o -8 6 1 11594.19 9523.91 457.52 o -6 6 1 6016.74 5275.58 492.00 o -4 6 1 4233.75 3912.25 604.92 o -2 6 1 136096.94 124043.54 1119.10 o 0 6 1 306455.31 291739.38 1170.35 o 2 6 1 103959.26 95898.82 1062.02 o 4 6 1 226115.89 211032.41 589.64 o 6 6 1 214784.80 204413.91 590.16 o 8 6 1 25429.89 22131.61 1220.56 o 10 6 1 33361.33 31694.53 2237.39 o 12 6 1 328720.13 315679.97 3372.02 o 14 6 1 119328.58 109921.41 2156.29 o 16 6 1 31164.95 34475.89 3412.32 o 18 6 1 65288.02 77320.67 6854.96 o 20 6 1 3727.58 2668.23 1099.68 o 22 6 1 2596.09 507.19 2408.56 o 24 6 1 2972.30 2992.59 1269.01 o 26 6 1 46644.02 56678.54 4603.80 o 28 6 1 6213.61 5382.70 1917.69 o 30 6 1 12552.02 16767.48 2548.29 o -29 7 1 19572.87 25513.82 5213.12 o -27 7 1 390.54 -409.69 2915.35 o -25 7 1 1077.74 1084.55 1733.51 o -23 7 1 61772.38 62216.46 8290.05 o -21 7 1 35725.56 36275.91 4768.90 o -19 7 1 16280.23 14533.96 1214.21 o -17 7 1 167180.77 144610.39 4704.64 o 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