# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' a in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 490.84 _exptl_crystal_F_000 1400.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.9620 _cell_length_b 15.4031 _cell_length_c 16.1575 _cell_angle_alpha 73.823 _cell_angle_beta 72.460 _cell_angle_gamma 68.580 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7507.21 6345.09 230.59 o 2 0 0 2985.29 2180.48 84.89 o 3 0 0 20.54 24.72 13.41 o 4 0 0 2514.32 2237.26 94.91 o 5 0 0 3072.79 2910.74 121.78 o 6 0 0 924.49 874.70 54.60 o 7 0 0 1658.50 1825.54 91.86 o 8 0 0 187.13 277.23 56.49 o 9 0 0 1894.91 1749.15 133.40 o 10 0 0 373.53 418.38 67.34 o 11 0 0 166.04 185.36 57.37 o 12 0 0 612.50 647.31 117.22 o 13 0 0 9.63 6.10 50.60 o 14 0 0 4.78 -28.55 51.68 o 15 0 0 37.88 80.31 61.85 o -14 1 0 121.40 228.77 68.94 o -13 1 0 100.16 77.98 160.82 o -12 1 0 57.00 2.33 56.95 o -11 1 0 1616.69 1896.73 150.19 o -10 1 0 566.00 592.63 80.28 o -9 1 0 75.98 61.58 32.79 o -8 1 0 862.14 1002.63 69.83 o -7 1 0 507.62 345.62 41.26 o -6 1 0 1465.30 1425.53 74.75 o -5 1 0 1262.40 1190.52 75.51 o -4 1 0 6583.38 6009.43 230.56 o -3 1 0 7.32 35.31 15.67 o -2 1 0 1199.36 1776.71 72.45 o -1 1 0 9007.19 8894.75 328.72 o 0 1 0 6747.70 5262.54 191.50 o 1 1 0 25111.27 21204.26 936.41 o 2 1 0 858.90 1045.11 87.20 o 4 1 0 488.97 469.04 62.63 o 6 1 0 126.76 166.10 46.02 o 7 1 0 526.05 614.55 45.25 o 8 1 0 2898.26 2481.46 114.29 o 9 1 0 186.01 237.41 57.85 o 10 1 0 1299.27 1255.54 113.16 o 11 1 0 293.76 274.94 63.82 o 12 1 0 119.73 81.69 49.56 o 13 1 0 0.65 -62.65 42.44 o 14 1 0 5.37 66.01 54.17 o 15 1 0 72.05 -24.77 55.21 o -14 2 0 98.81 121.59 63.04 o -13 2 0 207.72 137.27 65.57 o -12 2 0 57.72 81.81 149.12 o -11 2 0 16.40 6.95 41.05 o -10 2 0 1.56 -11.28 40.07 o -9 2 0 1918.18 1971.86 109.65 o -8 2 0 690.91 574.47 56.15 o -7 2 0 231.11 217.31 37.21 o -6 2 0 62.78 16.32 24.53 o -5 2 0 9390.99 9711.72 366.95 o -4 2 0 1599.28 1471.45 77.62 o -3 2 0 40.45 95.98 21.34 o -2 2 0 82070.77 93232.62 3348.59 o -1 2 0 864.50 1372.64 58.62 o 2 2 0 44025.39 42136.07 1822.44 o 3 2 0 29727.09 31221.11 1380.08 o 4 2 0 9823.97 10609.66 482.70 o 5 2 0 229.28 330.53 25.25 o 6 2 0 462.91 421.86 44.05 o 7 2 0 8511.96 7179.64 275.57 o 8 2 0 804.02 849.52 54.12 o 9 2 0 154.70 174.10 52.34 o 10 2 0 1358.43 1328.05 116.77 o 11 2 0 441.40 624.64 109.42 o 12 2 0 1478.77 1580.01 222.62 o 13 2 0 80.53 61.04 50.98 o 14 2 0 36.42 -19.38 50.78 o 15 2 0 21.78 -91.53 95.24 o -14 3 0 183.65 140.61 91.93 o -13 3 0 938.82 943.90 265.04 o -12 3 0 0.59 -43.41 44.67 o -11 3 0 40.40 78.68 49.26 o -10 3 0 20.74 45.39 45.46 o -9 3 0 1549.68 1602.00 98.03 o -8 3 0 197.40 71.96 35.97 o -7 3 0 1695.51 1766.15 95.25 o -6 3 0 1231.07 1286.37 76.28 o -5 3 0 20.49 31.17 24.73 o -4 3 0 7048.85 6629.73 256.28 o -3 3 0 21696.28 26187.52 950.98 o -2 3 0 30.39 11.32 21.34 o -1 3 0 32572.17 33718.59 1216.33 o 0 3 0 427.84 262.45 24.37 o 1 3 0 605.68 434.31 25.39 o 2 3 0 26723.07 25937.72 935.79 o 3 3 0 158970.80 165514.53 7410.92 o 4 3 0 704.06 674.83 51.33 o 5 3 0 5.48 33.19 31.90 o 6 3 0 312.74 400.24 89.33 o 7 3 0 87.97 60.72 35.36 o 8 3 0 2306.97 2444.49 146.84 o 9 3 0 1987.94 1740.95 129.11 o 10 3 0 716.81 887.98 94.76 o 11 3 0 43.02 31.96 42.98 o 12 3 0 126.48 103.37 53.67 o 13 3 0 163.21 237.76 68.04 o 14 3 0 120.33 144.15 80.47 o 15 3 0 174.25 172.31 110.95 o -13 4 0 2.46 20.09 69.48 o -12 4 0 223.89 288.14 123.83 o -11 4 0 386.24 419.90 109.65 o -10 4 0 85.84 98.15 39.39 o -9 4 0 28.17 37.98 35.23 o -8 4 0 13.30 29.47 46.38 o -7 4 0 1191.98 1092.22 76.29 o -6 4 0 117.76 182.70 45.39 o -5 4 0 9.84 50.55 26.01 o -4 4 0 1215.08 1366.73 76.83 o -2 4 0 33947.92 32890.82 1191.84 o -1 4 0 1653.52 1978.68 84.90 o 0 4 0 1615.24 1634.48 71.00 o 1 4 0 119.63 239.60 22.94 o 2 4 0 2644.09 3241.87 127.88 o 3 4 0 92.95 169.80 20.69 o 4 4 0 23475.97 24633.07 894.29 o 5 4 0 6958.24 6409.52 244.32 o 6 4 0 461.97 494.43 72.55 o 7 4 0 89.66 141.24 38.68 o 8 4 0 842.39 1089.84 94.89 o 9 4 0 2079.71 1915.89 131.37 o 10 4 0 1449.83 1331.28 114.63 o 11 4 0 717.74 747.31 91.99 o 12 4 0 26.60 -17.59 71.84 o 13 4 0 601.83 579.10 90.43 o 14 4 0 706.76 682.29 100.89 o 15 4 0 283.73 252.66 75.39 o -13 5 0 242.53 347.87 111.31 o -12 5 0 114.55 106.82 85.55 o -11 5 0 76.20 137.72 69.36 o -10 5 0 522.73 526.28 66.57 o -9 5 0 849.39 807.57 71.72 o -8 5 0 325.76 265.26 46.73 o -7 5 0 8.61 40.78 35.37 o -6 5 0 3724.61 3913.47 253.15 o -5 5 0 3368.11 3214.27 141.33 o -4 5 0 364.58 434.60 41.46 o -3 5 0 1647.16 2193.73 99.83 o -2 5 0 1193.28 1256.54 64.75 o -1 5 0 313.57 433.02 34.46 o 0 5 0 9168.41 9007.29 336.86 o 1 5 0 5626.12 5139.56 197.98 o 2 5 0 2791.86 3086.07 124.81 o 3 5 0 101.29 139.76 24.42 o 4 5 0 4817.26 5026.50 195.79 o 5 5 0 2398.57 2213.16 96.47 o 6 5 0 11858.03 11633.86 433.85 o 7 5 0 1149.31 980.77 114.74 o 8 5 0 1100.52 1163.57 97.65 o 9 5 0 1545.80 1742.39 129.41 o 10 5 0 2195.07 2102.34 145.22 o 11 5 0 18.82 48.82 43.11 o 12 5 0 13.23 12.34 46.31 o 13 5 0 11.06 33.27 71.96 o 14 5 0 344.24 328.18 80.96 o 15 5 0 101.02 81.63 62.14 o -12 6 0 0.06 -10.87 70.42 o -11 6 0 629.81 776.32 134.94 o -10 6 0 1170.44 1073.12 86.32 o -9 6 0 645.93 569.56 62.39 o -8 6 0 8.36 -10.70 30.76 o -7 6 0 1080.97 1111.81 97.96 o -6 6 0 684.99 704.72 73.08 o -5 6 0 625.05 680.61 94.29 o -4 6 0 6117.95 6309.22 251.46 o -3 6 0 17.29 -3.49 20.27 o -2 6 0 300.96 222.57 49.29 o -1 6 0 10626.88 10647.89 400.01 o 0 6 0 3266.78 3614.90 147.14 o 1 6 0 1115.73 925.86 51.49 o 2 6 0 116.43 204.52 26.84 o 3 6 0 111.47 168.38 30.89 o 4 6 0 76.48 135.96 23.81 o 5 6 0 11458.49 10846.82 505.64 o 6 6 0 31920.82 31382.65 1142.50 o 7 6 0 28.10 59.27 21.65 o 8 6 0 28.01 94.99 86.38 o 9 6 0 54.90 0.79 36.55 o 10 6 0 34.89 19.04 40.60 o 11 6 0 1354.36 1295.91 183.15 o 12 6 0 790.45 722.09 106.82 o 13 6 0 292.50 310.48 75.26 o 14 6 0 18.35 61.23 61.68 o 15 6 0 184.64 236.00 74.90 o -10 7 0 100.96 129.10 51.56 o -9 7 0 282.75 271.87 50.49 o -8 7 0 458.43 477.25 56.76 o -7 7 0 48.09 39.79 33.34 o -6 7 0 183.96 271.84 43.19 o -5 7 0 2312.85 2294.92 114.57 o -4 7 0 300.51 163.78 58.60 o -3 7 0 2832.32 2864.70 128.66 o -2 7 0 24.05 -2.67 21.24 o -1 7 0 0.52 8.52 19.61 o 0 7 0 10.37 30.79 23.88 o 1 7 0 244.68 210.53 28.86 o 2 7 0 277.57 192.22 30.06 o 3 7 0 322.76 370.86 37.22 o 4 7 0 490.98 515.04 43.16 o 6 7 0 302.97 199.04 38.98 o 7 7 0 7827.06 8017.67 310.64 o 8 7 0 3282.04 2833.97 166.98 o 9 7 0 681.04 637.92 78.62 o 10 7 0 32.93 28.24 47.15 o 11 7 0 49.93 43.66 96.77 o 12 7 0 642.81 644.70 148.53 o 13 7 0 737.65 874.06 243.06 o 14 7 0 307.79 239.77 98.78 o 15 7 0 14.94 -39.51 56.62 o -10 8 0 22.94 71.84 83.66 o -9 8 0 845.40 818.62 144.16 o -8 8 0 299.68 323.15 62.44 o -7 8 0 145.09 234.55 42.91 o -6 8 0 35.32 91.76 37.66 o -5 8 0 154.94 186.98 39.73 o -4 8 0 1909.12 1880.28 101.09 o -3 8 0 1967.18 2382.88 114.61 o -2 8 0 109.77 88.11 28.75 o -1 8 0 1155.84 1585.92 83.26 o 0 8 0 239.00 288.96 35.74 o 1 8 0 2347.78 2418.01 109.93 o 2 8 0 414.77 594.56 71.63 o 3 8 0 6561.17 5721.07 227.67 o 4 8 0 96.42 135.19 40.61 o 5 8 0 302.24 307.40 38.21 o 6 8 0 65.74 165.43 55.77 o 7 8 0 1729.55 1625.22 88.13 o 8 8 0 338.73 402.90 72.79 o 9 8 0 12.60 -28.86 60.14 o 10 8 0 79.27 99.24 48.41 o 11 8 0 147.97 106.09 54.20 o 12 8 0 1058.02 909.36 107.70 o 13 8 0 579.59 607.77 96.19 o 14 8 0 446.64 444.52 89.82 o 15 8 0 38.93 77.05 68.54 o -10 9 0 0.25 -32.61 76.10 o -9 9 0 17.56 -42.54 71.84 o -8 9 0 929.70 1044.08 166.14 o -7 9 0 1157.34 1073.62 167.08 o -6 9 0 0.13 6.55 30.55 o -5 9 0 55.02 79.61 37.29 o -4 9 0 686.73 827.83 68.87 o -3 9 0 210.23 244.72 42.08 o -2 9 0 691.43 610.02 68.31 o -1 9 0 2013.01 1791.16 93.42 o 0 9 0 3.33 31.87 24.87 o 1 9 0 1356.46 1281.85 74.68 o 2 9 0 3067.78 2984.98 133.10 o 3 9 0 1803.64 1910.65 95.42 o 4 9 0 89.33 304.57 39.04 o 5 9 0 54.24 93.33 30.25 o 6 9 0 249.91 343.41 46.52 o 7 9 0 9.31 -37.39 24.93 o 8 9 0 605.79 520.63 70.15 o 9 9 0 3007.70 2730.44 169.84 o 10 9 0 796.13 867.65 98.22 o 11 9 0 7.11 15.31 44.42 o 12 9 0 26.22 23.44 50.33 o 13 9 0 59.46 11.84 117.45 o 14 9 0 58.32 -16.38 49.24 o 15 9 0 274.79 430.54 194.85 o -9 10 0 10.70 25.05 89.57 o -8 10 0 180.26 255.70 111.07 o -7 10 0 7.65 -6.85 82.00 o -6 10 0 1376.60 1292.93 186.93 o -5 10 0 59.59 84.67 46.39 o -4 10 0 566.50 527.95 76.92 o -3 10 0 182.40 140.51 38.88 o -2 10 0 70.09 47.69 31.48 o -1 10 0 197.12 274.11 63.17 o 0 10 0 714.31 758.27 88.98 o 1 10 0 448.42 484.11 49.55 o 2 10 0 172.19 315.59 42.27 o 3 10 0 1370.91 1759.42 95.02 o 4 10 0 2702.01 2459.65 118.28 o 5 10 0 763.10 836.46 65.22 o 6 10 0 969.04 938.70 69.07 o 7 10 0 111.57 132.81 58.37 o 8 10 0 40.22 -6.70 34.06 o 9 10 0 542.42 432.36 81.06 o 10 10 0 4902.69 5180.48 338.30 o 11 10 0 188.82 283.14 68.75 o 12 10 0 5.72 39.35 51.33 o 13 10 0 266.63 224.55 67.08 o 14 10 0 192.63 136.72 64.49 o 15 10 0 0.24 -27.42 76.81 o -8 11 0 0.03 69.95 94.53 o -7 11 0 237.00 252.16 113.67 o -6 11 0 821.57 904.41 171.10 o -5 11 0 486.77 534.80 134.47 o -4 11 0 790.70 778.69 88.03 o -3 11 0 1068.03 979.82 160.46 o -2 11 0 3.86 4.74 41.86 o -1 11 0 2942.50 3109.17 179.33 o 0 11 0 1073.00 1124.75 77.70 o 1 11 0 114.79 176.83 36.34 o 2 11 0 437.13 576.71 57.09 o 3 11 0 2243.22 2219.37 114.06 o 4 11 0 18.15 74.38 33.57 o 5 11 0 197.86 194.32 39.92 o 6 11 0 682.99 694.81 63.43 o 7 11 0 109.35 54.33 38.55 o 8 11 0 233.22 253.43 57.11 o 9 11 0 124.73 80.82 47.61 o 10 11 0 729.41 755.33 139.08 o 11 11 0 11.69 -29.99 42.81 o 12 11 0 175.45 72.70 104.22 o 13 11 0 10.40 -77.72 51.82 o 14 11 0 55.76 0.99 56.72 o -7 12 0 2.85 -102.33 84.84 o -6 12 0 9.89 -76.57 84.37 o -5 12 0 465.75 513.29 145.10 o -4 12 0 774.91 703.77 158.57 o -3 12 0 24.88 -67.35 80.11 o -2 12 0 7.91 -16.83 36.11 o -1 12 0 292.04 200.42 65.82 o 0 12 0 4.10 77.36 39.29 o 1 12 0 375.53 500.86 70.38 o 2 12 0 479.81 477.36 73.30 o 3 12 0 393.35 420.19 57.04 o 4 12 0 46.34 23.18 43.00 o 5 12 0 1279.30 1119.28 80.48 o 6 12 0 167.02 169.96 41.43 o 7 12 0 841.36 747.89 99.73 o 8 12 0 88.52 31.19 54.35 o 9 12 0 690.12 688.71 91.92 o 10 12 0 0.78 -43.36 37.70 o 11 12 0 514.35 527.45 86.91 o 12 12 0 1816.56 2021.33 260.90 o 13 12 0 51.02 48.10 63.16 o 14 12 0 68.36 120.89 66.52 o -6 13 0 20.58 79.17 116.74 o -5 13 0 31.77 44.19 107.76 o -4 13 0 126.76 199.93 118.16 o -3 13 0 1138.81 1318.69 204.18 o -2 13 0 29.20 3.54 83.89 o -1 13 0 1.43 26.23 40.55 o 0 13 0 275.94 260.86 58.09 o 1 13 0 1521.46 1724.61 133.02 o 2 13 0 30.70 38.63 44.46 o 3 13 0 290.23 257.70 59.19 o 4 13 0 0.49 14.90 29.82 o 5 13 0 2.13 -10.65 65.68 o 6 13 0 119.49 107.61 37.16 o 7 13 0 462.26 506.66 136.48 o 8 13 0 188.57 245.30 81.06 o 9 13 0 525.88 579.94 83.78 o 10 13 0 10.70 46.66 54.71 o 11 13 0 4.03 1.28 46.07 o 12 13 0 162.54 135.39 97.60 o 13 13 0 441.43 407.65 86.87 o -5 14 0 1.09 214.82 129.74 o -4 14 0 89.45 63.57 110.13 o -3 14 0 342.62 345.27 130.45 o -2 14 0 67.99 75.15 93.82 o -1 14 0 51.16 -0.24 90.51 o 0 14 0 21.86 1.18 41.34 o 1 14 0 212.17 229.02 108.47 o 2 14 0 481.78 459.94 74.78 o 3 14 0 167.15 219.55 59.09 o 4 14 0 57.74 80.12 71.96 o 5 14 0 4.95 -25.94 49.16 o 6 14 0 0.78 -3.76 43.77 o 7 14 0 745.62 631.52 92.64 o 8 14 0 424.72 449.96 95.00 o 9 14 0 465.92 449.62 76.98 o 10 14 0 325.03 421.73 76.01 o 11 14 0 4.19 26.75 50.65 o 12 14 0 19.34 9.76 53.28 o -3 15 0 27.58 15.36 89.80 o -2 15 0 216.25 226.16 109.42 o -1 15 0 439.50 785.30 163.30 o 0 15 0 1.67 -41.36 86.97 o 1 15 0 17.98 21.74 83.66 o 2 15 0 17.98 -28.62 53.88 o 3 15 0 0.11 -49.18 90.63 o 4 15 0 155.35 145.73 54.84 o 5 15 0 328.57 250.54 65.61 o 6 15 0 26.91 -5.44 62.39 o 7 15 0 109.41 40.41 67.59 o 9 15 0 190.43 230.18 94.29 o 10 15 0 23.00 65.83 50.34 o 11 15 0 36.40 83.97 56.61 o 12 15 0 10.66 9.95 59.89 o -1 16 0 30.05 107.05 97.37 o 0 16 0 597.88 1225.34 204.42 o 1 16 0 92.50 26.47 90.98 o 2 16 0 5.78 89.09 97.37 o 3 16 0 25.82 71.19 53.52 o 4 16 0 33.82 -13.04 66.76 o 5 16 0 76.13 115.80 84.13 o 6 16 0 307.57 324.94 100.44 o 7 16 0 56.24 95.00 81.06 o 9 16 0 151.68 337.47 109.18 o 10 16 0 183.66 302.97 111.78 o 1 17 0 0.28 -6.14 92.17 o 2 17 0 6.32 -15.60 91.46 o 3 17 0 54.20 176.77 104.46 o 4 17 0 3.79 -51.28 90.51 o 5 17 0 222.71 311.34 75.57 o 6 17 0 501.94 445.94 112.73 o 7 17 0 6.83 -106.70 71.13 o -7 -17 1 0.03 -6.38 77.28 o -6 -17 1 4.71 24.34 78.93 o -5 -17 1 46.67 59.06 55.65 o -4 -17 1 20.41 -70.01 52.63 o -3 -17 1 192.18 311.70 79.52 o -2 -17 1 81.32 156.21 118.87 o -8 -16 1 0.11 86.02 90.28 o -7 -16 1 282.66 280.52 98.78 o -6 -16 1 254.02 262.79 94.77 o -5 -16 1 18.36 -2.99 57.94 o -4 -16 1 17.82 -0.87 50.82 o -3 -16 1 295.44 362.39 100.67 o -2 -16 1 90.43 108.88 61.50 o -1 -16 1 25.32 -10.16 95.24 o 0 -16 1 172.14 186.93 111.54 o 1 -16 1 1.20 7.33 98.07 o -11 -15 1 57.35 104.22 102.56 o -10 -15 1 148.95 291.15 113.91 o -8 -15 1 411.26 476.43 118.63 o -7 -15 1 827.10 936.79 157.16 o -6 -15 1 40.13 -36.39 57.90 o -5 -15 1 320.90 288.08 69.28 o -4 -15 1 46.49 77.49 74.09 o -3 -15 1 4.19 10.90 46.80 o -2 -15 1 410.81 340.48 73.17 o -1 -15 1 1027.83 1045.02 113.76 o 0 -15 1 29.89 26.54 79.40 o 1 -15 1 177.28 136.36 98.07 o 2 -15 1 3.78 4.49 88.15 o 3 -15 1 105.61 67.35 96.18 o -12 -14 1 142.59 146.25 90.39 o -11 -14 1 147.76 282.00 71.64 o -10 -14 1 85.87 237.27 63.97 o -9 -14 1 107.73 115.25 121.82 o -8 -14 1 3.52 134.70 81.77 o -7 -14 1 304.47 380.72 103.51 o -6 -14 1 695.26 837.77 138.01 o -5 -14 1 289.18 346.40 101.26 o -4 -14 1 28.70 -8.13 43.15 o -3 -14 1 120.71 153.53 55.79 o -2 -14 1 678.55 648.60 86.93 o -1 -14 1 5.18 47.24 53.76 o 0 -14 1 994.37 987.72 107.97 o 1 -14 1 418.38 676.57 87.56 o 2 -14 1 2.72 -8.74 87.20 o 3 -14 1 18.83 -93.58 73.50 o 4 -14 1 315.55 441.93 152.19 o 5 -14 1 28.95 197.80 131.40 o -13 -13 1 1.35 85.12 66.53 o -12 -13 1 2.22 13.45 56.13 o -11 -13 1 47.91 63.12 55.29 o -10 -13 1 402.97 336.25 74.21 o -9 -13 1 497.15 563.56 154.79 o -8 -13 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