# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' CI6642 in Pnma C12 H12 Cl2 Cu N3 O S' _shelx_refln_list_code 4 _shelx_F_calc_maximum 449.72 _exptl_crystal_F_000 772.00 _reflns_d_resolution_high 0.7494 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' _cell_length_a 19.3010 _cell_length_b 6.9500 _cell_length_c 11.1730 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1443.45 1720.77 38.94 o 4 0 0 9226.32 10525.86 271.17 o 6 0 0 249.64 217.16 12.71 o 8 0 0 3186.18 3157.67 76.65 o 10 0 0 37.57 22.43 8.25 o 12 0 0 9174.47 8604.63 195.41 o 14 0 0 3448.10 2913.69 105.30 o 16 0 0 691.01 719.32 67.00 o 18 0 0 518.03 605.28 103.16 o 20 0 0 726.79 828.21 66.25 o 22 0 0 257.58 369.68 75.97 o 24 0 0 0.44 0.74 28.28 o 2 1 0 12493.54 13215.11 214.58 o 4 1 0 1801.40 1691.76 30.26 o 6 1 0 20.96 27.35 5.38 o 8 1 0 225.75 186.04 9.96 o 10 1 0 53.20 51.65 7.06 o 12 1 0 5909.63 5808.63 108.91 o 14 1 0 1515.27 1410.77 46.30 o 16 1 0 1475.18 1429.55 49.62 o 18 1 0 1695.71 1573.91 55.73 o 20 1 0 2.80 12.26 18.63 o 22 1 0 238.48 243.08 30.17 o 24 1 0 468.08 422.75 46.21 o 0 2 0 202244.69 149182.48 3065.03 o 2 2 0 1354.19 1519.62 28.80 o 4 2 0 12530.17 13251.10 218.91 o 6 2 0 2440.75 2479.61 45.41 o 8 2 0 4884.82 5022.69 92.06 o 10 2 0 348.36 286.49 14.87 o 12 2 0 4961.26 4830.70 95.51 o 14 2 0 2212.33 2207.57 55.16 o 16 2 0 375.68 379.50 29.71 o 18 2 0 348.55 288.12 28.31 o 20 2 0 655.69 663.23 76.52 o 22 2 0 229.40 205.98 32.85 o 24 2 0 0.00 -3.59 23.13 o 2 3 0 4486.40 4532.27 75.42 o 4 3 0 2226.26 2078.76 40.41 o 6 3 0 419.25 515.06 27.25 o 8 3 0 3.05 -2.08 5.84 o 10 3 0 9.87 -0.75 7.00 o 12 3 0 2587.42 2565.24 60.60 o 14 3 0 617.16 686.51 46.18 o 16 3 0 866.43 790.27 49.64 o 18 3 0 1204.39 1121.44 94.15 o 20 3 0 31.46 8.44 18.39 o 22 3 0 147.95 152.50 32.03 o 0 4 0 44240.27 43537.89 908.69 o 2 4 0 80.82 92.15 9.58 o 4 4 0 2188.38 2191.59 44.79 o 6 4 0 1066.55 1117.61 28.87 o 8 4 0 2086.45 1939.35 75.55 o 10 4 0 99.68 93.72 14.77 o 12 4 0 1708.86 1646.70 64.54 o 14 4 0 879.47 949.57 43.69 o 16 4 0 42.34 16.95 14.08 o 18 4 0 103.06 80.85 23.47 o 20 4 0 411.35 360.03 41.31 o 22 4 0 133.07 164.78 33.07 o 2 5 0 881.07 898.60 28.99 o 4 5 0 512.12 473.15 21.96 o 6 5 0 105.42 118.10 13.61 o 8 5 0 64.47 77.97 12.99 o 10 5 0 87.86 98.99 19.88 o 12 5 0 987.37 953.77 45.47 o 14 5 0 174.96 205.07 24.27 o 16 5 0 206.64 199.25 25.78 o 18 5 0 418.68 496.52 46.12 o 20 5 0 29.74 39.00 25.12 o 0 6 0 9440.89 8977.87 213.27 o 2 6 0 9.40 22.92 16.24 o 4 6 0 69.89 83.00 14.01 o 6 6 0 167.90 172.05 17.65 o 8 6 0 489.56 399.07 29.59 o 10 6 0 0.20 1.72 15.64 o 12 6 0 472.07 463.05 38.05 o 14 6 0 255.30 298.81 34.85 o 16 6 0 1.83 8.30 20.58 o 18 6 0 16.42 30.73 31.14 o 2 7 0 210.18 215.86 39.73 o 4 7 0 127.68 150.75 29.75 o 6 7 0 53.53 53.40 17.90 o 8 7 0 26.54 52.99 27.73 o 10 7 0 44.93 144.19 46.49 o 12 7 0 192.74 207.11 37.13 o 14 7 0 9.12 34.25 27.34 o 16 7 0 42.52 84.55 31.34 o 0 8 0 1282.79 1074.65 117.14 o 2 8 0 22.89 -14.43 33.43 o 4 8 0 14.17 64.22 27.96 o 6 8 0 90.65 80.83 45.73 o 8 8 0 171.08 84.17 42.09 o 10 8 0 0.03 31.00 36.01 o 12 8 0 70.83 145.10 47.71 o 2 9 0 51.93 118.81 47.25 o 4 9 0 25.76 49.08 41.93 o 1 0 1 8206.29 8713.34 129.18 o 2 0 1 9550.49 10281.85 152.35 o 3 0 1 57.63 36.41 6.13 o 4 0 1 10025.18 10693.72 159.93 o 5 0 1 6443.70 6511.20 100.34 o 6 0 1 3822.00 3634.32 59.53 o 7 0 1 2712.79 2817.83 48.71 o 8 0 1 9257.80 10089.91 155.21 o 9 0 1 7831.33 8493.64 133.29 o 10 0 1 6885.84 6803.40 109.56 o 11 0 1 88.26 112.25 8.92 o 12 0 1 273.38 323.11 18.36 o 13 0 1 191.34 191.11 15.86 o 14 0 1 2371.36 2186.58 61.10 o 15 0 1 318.73 315.42 25.41 o 16 0 1 4.55 5.74 12.19 o 17 0 1 1270.59 1183.44 45.87 o 18 0 1 181.00 250.69 25.41 o 19 0 1 116.27 103.12 20.33 o 20 0 1 1.17 7.92 15.62 o 21 0 1 273.80 306.14 32.02 o 22 0 1 316.68 255.36 30.19 o 23 0 1 11.85 9.64 19.66 o 24 0 1 150.72 131.35 26.95 o 25 0 1 95.50 105.44 60.01 o 0 1 1 6418.00 6886.41 114.02 o 1 1 1 4796.29 5481.03 61.77 o 2 1 1 8983.77 9916.25 109.62 o 3 1 1 737.42 764.74 11.25 o 4 1 1 3093.21 3456.70 39.70 o 5 1 1 119.07 146.95 5.21 o 6 1 1 516.27 472.51 10.64 o 7 1 1 450.92 444.04 10.97 o 8 1 1 4787.81 4646.34 57.42 o 9 1 1 1388.98 1189.56 20.37 o 10 1 1 950.71 1110.11 20.16 o 11 1 1 79.43 112.34 7.72 o 12 1 1 2134.49 1964.87 31.22 o 13 1 1 2181.64 2118.37 38.17 o 14 1 1 825.49 839.22 24.13 o 15 1 1 193.05 215.86 15.59 o 16 1 1 46.16 53.27 10.88 o 17 1 1 509.39 520.62 33.29 o 18 1 1 118.59 121.71 14.72 o 19 1 1 19.05 2.53 10.25 o 20 1 1 1013.63 1061.34 36.90 o 21 1 1 1521.91 1393.46 42.04 o 22 1 1 1355.96 1339.03 47.13 o 23 1 1 310.72 294.12 25.94 o 24 1 1 21.58 25.30 16.07 o 25 1 1 184.53 260.04 51.75 o 1 2 1 5804.38 6636.00 75.78 o 2 2 1 5908.74 6148.24 67.92 o 3 2 1 375.49 358.92 8.39 o 4 2 1 8248.79 8398.65 100.44 o 5 2 1 3194.43 3199.34 39.05 o 6 2 1 3945.32 4108.07 49.02 o 7 2 1 2403.88 2322.81 31.14 o 8 2 1 4051.89 3937.89 48.44 o 9 2 1 6537.52 6785.81 78.49 o 10 2 1 3613.39 3229.98 47.16 o 11 2 1 5.25 9.69 5.67 o 12 2 1 182.61 173.74 11.11 o 13 2 1 119.42 123.55 11.53 o 14 2 1 1769.56 1820.12 34.41 o 15 2 1 194.32 185.76 14.07 o 16 2 1 10.46 9.43 9.13 o 17 2 1 868.28 863.27 30.85 o 18 2 1 230.20 234.02 19.48 o 19 2 1 68.20 98.22 15.75 o 20 2 1 5.20 9.67 12.15 o 21 2 1 221.98 250.00 22.39 o 22 2 1 229.21 309.48 34.04 o 23 2 1 7.42 38.89 17.05 o 24 2 1 121.88 133.37 25.03 o 0 3 1 242.63 254.49 14.08 o 1 3 1 5654.08 5940.40 71.07 o 2 3 1 795.96 800.97 14.36 o 3 3 1 3.25 3.16 3.17 o 4 3 1 80.84 76.43 5.40 o 5 3 1 28.14 41.92 4.68 o 6 3 1 1146.61 1119.59 19.82 o 7 3 1 200.67 228.24 13.89 o 8 3 1 3104.28 3076.62 41.04 o 9 3 1 399.35 381.16 12.49 o 10 3 1 883.21 865.31 19.50 o 11 3 1 3.11 -1.59 6.52 o 12 3 1 745.30 791.26 29.99 o 13 3 1 1528.58 1474.08 32.56 o 14 3 1 521.62 651.98 23.77 o 15 3 1 121.90 98.28 11.68 o 16 3 1 41.74 51.40 11.42 o 17 3 1 240.45 186.27 19.77 o 18 3 1 48.27 82.26 15.84 o 19 3 1 22.37 25.24 14.04 o 20 3 1 618.38 621.89 35.41 o 21 3 1 767.53 805.02 41.01 o 22 3 1 779.64 754.58 47.65 o 23 3 1 147.42 189.75 23.47 o 1 4 1 2175.10 2173.24 31.00 o 2 4 1 1872.87 1880.73 29.33 o 3 4 1 467.16 428.65 13.01 o 4 4 1 2621.41 2541.27 37.97 o 5 4 1 1183.03 1133.74 21.34 o 6 4 1 1120.75 1135.40 21.49 o 7 4 1 579.47 591.73 16.17 o 8 4 1 1185.16 1115.48 26.42 o 9 4 1 2479.18 2487.28 41.39 o 10 4 1 1209.80 1215.96 26.43 o 11 4 1 11.86 3.83 6.96 o 12 4 1 198.84 224.79 15.67 o 13 4 1 16.77 2.21 7.70 o 14 4 1 632.32 651.72 26.91 o 15 4 1 33.99 39.59 10.47 o 16 4 1 11.20 26.48 11.15 o 17 4 1 378.99 440.50 28.68 o 18 4 1 171.50 182.72 20.91 o 19 4 1 32.93 28.02 14.98 o 20 4 1 4.68 -0.10 13.59 o 21 4 1 100.49 136.59 21.24 o 22 4 1 105.85 122.60 22.90 o 23 4 1 2.02 16.41 39.20 o 0 5 1 611.26 581.92 22.69 o 1 5 1 945.45 971.23 19.70 o 2 5 1 728.31 707.86 17.31 o 3 5 1 65.18 86.96 8.21 o 4 5 1 86.41 90.88 8.35 o 5 5 1 166.12 178.36 10.70 o 6 5 1 186.55 187.76 11.90 o 7 5 1 316.66 349.19 16.04 o 8 5 1 551.21 565.74 20.20 o 9 5 1 179.15 214.78 16.55 o 10 5 1 208.76 237.67 16.45 o 11 5 1 0.33 12.69 8.89 o 12 5 1 271.59 293.30 20.49 o 13 5 1 495.59 497.25 24.65 o 14 5 1 304.18 308.76 20.59 o 15 5 1 34.20 55.80 12.07 o 16 5 1 26.45 45.55 12.10 o 17 5 1 60.31 72.05 15.02 o 18 5 1 8.65 19.63 14.61 o 19 5 1 25.23 40.13 16.30 o 20 5 1 224.32 206.48 27.30 o 21 5 1 228.90 278.87 74.19 o 1 6 1 681.16 606.80 21.88 o 2 6 1 425.66 442.76 20.13 o 3 6 1 131.30 144.96 12.22 o 4 6 1 436.60 428.49 22.20 o 5 6 1 309.32 319.22 19.71 o 6 6 1 148.98 168.23 14.12 o 7 6 1 47.83 51.52 10.67 o 8 6 1 298.27 309.71 22.18 o 9 6 1 554.33 570.60 29.68 o 10 6 1 324.15 388.57 25.91 o 11 6 1 9.42 42.88 13.06 o 12 6 1 163.72 213.94 23.65 o 13 6 1 0.14 10.71 12.18 o 14 6 1 134.04 145.81 19.43 o 15 6 1 2.56 34.71 14.78 o 16 6 1 3.37 21.85 14.47 o 17 6 1 115.33 141.03 22.69 o 18 6 1 70.61 98.20 24.94 o 19 6 1 18.19 2.13 39.81 o 0 7 1 146.36 189.21 42.77 o 1 7 1 180.04 172.94 22.62 o 2 7 1 152.23 159.27 22.55 o 3 7 1 10.03 12.45 11.06 o 4 7 1 1.99 3.08 11.07 o 5 7 1 41.88 35.47 12.59 o 6 7 1 66.70 82.16 20.45 o 7 7 1 107.54 127.72 18.88 o 8 7 1 91.59 126.19 18.39 o 9 7 1 29.59 30.33 14.19 o 10 7 1 44.70 73.40 16.87 o 11 7 1 0.07 11.33 14.84 o 12 7 1 66.27 79.69 20.49 o 13 7 1 114.00 165.34 22.03 o 14 7 1 101.02 111.47 20.71 o 15 7 1 8.44 10.62 26.09 o 16 7 1 5.69 1.31 21.37 o 1 8 1 179.57 151.95 28.19 o 2 8 1 100.19 99.23 21.46 o 3 8 1 7.04 36.02 17.81 o 4 8 1 82.98 96.66 22.35 o 5 8 1 39.27 22.53 21.02 o 6 8 1 33.45 6.80 20.46 o 7 8 1 0.91 1.43 19.71 o 8 8 1 33.45 36.81 31.95 o 9 8 1 99.63 133.86 27.91 o 10 8 1 36.39 15.38 20.30 o 11 8 1 7.88 14.28 40.11 o 12 8 1 41.14 73.84 40.26 o 0 9 1 11.99 51.31 45.20 o 1 9 1 37.84 69.13 26.81 o 2 9 1 12.68 49.47 40.57 o 3 9 1 0.03 78.40 42.85 o 4 9 1 4.25 62.45 42.85 o 0 0 2 1216.16 1194.20 31.23 o 1 0 2 10006.24 10622.36 158.96 o 2 0 2 1413.73 1350.97 24.87 o 3 0 2 1735.90 1733.98 31.35 o 4 0 2 72.77 63.84 6.02 o 5 0 2 11886.65 11961.58 180.53 o 6 0 2 577.85 504.42 14.50 o 7 0 2 13226.52 13247.45 246.32 o 8 0 2 565.46 553.62 15.91 o 9 0 2 1437.16 1237.39 38.02 o 10 0 2 624.95 783.89 20.65 o 11 0 2 818.64 915.33 25.33 o 12 0 2 288.23 270.71 17.79 o 13 0 2 7629.44 7303.38 223.61 o 14 0 2 1540.99 1513.25 42.07 o 15 0 2 195.26 225.74 22.27 o 16 0 2 44.42 70.50 15.94 o 17 0 2 0.84 -6.16 12.33 o 18 0 2 522.98 617.99 37.80 o 19 0 2 819.31 692.69 41.80 o 20 0 2 1.37 2.46 18.57 o 21 0 2 438.34 461.43 37.72 o 22 0 2 206.88 171.24 27.29 o 23 0 2 8.88 -8.60 20.06 o 24 0 2 19.50 81.41 28.22 o 25 0 2 5.13 15.04 57.58 o 1 1 2 2192.04 2429.97 28.55 o 2 1 2 11956.34 12597.15 139.24 o 3 1 2 104.73 66.35 4.59 o 4 1 2 2251.97 2247.38 27.98 o 5 1 2 4463.71 4486.43 51.52 o 6 1 2 10.52 15.31 3.64 o 7 1 2 333.19 350.86 10.31 o 8 1 2 7737.22 8486.71 99.22 o 9 1 2 244.66 212.22 9.31 o 10 1 2 881.20 852.03 18.33 o 11 1 2 3552.21 3617.35 49.21 o 12 1 2 1910.06 1801.45 29.79 o 13 1 2 4177.96 4214.50 60.82 o 14 1 2 297.08 284.00 15.39 o 15 1 2 31.41 24.84 8.57 o 16 1 2 1518.11 1306.50 33.63 o 17 1 2 2077.48 2018.69 44.94 o 18 1 2 138.40 144.60 15.19 o 19 1 2 1095.01 1025.77 35.13 o 20 1 2 82.39 112.98 16.00 o 21 1 2 1.01 -9.08 12.38 o 22 1 2 54.28 36.44 15.22 o 23 1 2 270.42 258.05 25.39 o 24 1 2 126.05 179.65 22.19 o 25 1 2 463.77 448.77 63.26 o 0 2 2 5.57 5.11 6.27 o 1 2 2 21056.45 22103.41 241.15 o 2 2 2 40.88 37.17 3.87 o 3 2 2 82.08 92.48 5.41 o 4 2 2 129.05 162.68 7.08 o 5 2 2 4067.98 4104.45 48.65 o 6 2 2 1046.97 1042.25 17.12 o 7 2 2 6089.24 6097.23 73.53 o 8 2 2 123.05 138.15 9.47 o 9 2 2 349.35 321.11 12.03 o 10 2 2 438.40 530.41 15.53 o 11 2 2 1266.05 1141.17 22.76 o 12 2 2 183.12 190.36 12.72 o 13 2 2 6597.83 6379.58 90.95 o 14 2 2 1049.98 1051.31 30.59 o 15 2 2 170.30 169.31 14.74 o 16 2 2 47.77 21.68 10.74 o 17 2 2 0.28 2.89 9.69 o 18 2 2 335.50 304.11 21.75 o 19 2 2 622.22 646.06 34.69 o 20 2 2 1.06 0.71 12.44 o 21 2 2 314.49 346.19 26.40 o 22 2 2 133.87 149.10 19.96 o 23 2 2 4.52 3.42 15.41 o 24 2 2 9.77 26.58 24.16 o 1 3 2 136.20 178.22 7.32 o 2 3 2 4248.26 4291.55 53.62 o 3 3 2 584.86 515.39 11.92 o 4 3 2 242.57 218.83 7.91 o 5 3 2 1756.53 1732.76 25.29 o 6 3 2 106.35 115.90 6.63 o 7 3 2 491.26 557.43 13.96 o 8 3 2 3032.39 2963.54 39.96 o 9 3 2 619.27 566.00 18.09 o 10 3 2 381.54 411.01 16.07 o 11 3 2 2518.29 2450.05 41.29 o 12 3 2 653.97 601.62 21.59 o 13 3 2 2026.97 1926.09 40.98 o 14 3 2 171.59 160.25 13.25 o 15 3 2 50.82 59.94 11.32 o 16 3 2 897.00 845.82 31.41 o 17 3 2 1013.51 1054.25 46.52 o 18 3 2 70.77 67.53 14.51 o 19 3 2 511.58 520.66 30.20 o 20 3 2 59.93 32.59 14.94 o 21 3 2 3.24 30.98 15.43 o 22 3 2 34.16 37.19 23.66 o 23 3 2 176.73 141.90 24.60 o 0 4 2 25.35 45.92 10.30 o 1 4 2 6643.24 6596.61 77.04 o 2 4 2 85.36 122.32 7.30 o 3 4 2 4.37 -1.35 4.18 o 4 4 2 12.93 21.26 4.66 o 5 4 2 1873.48 1774.34 32.58 o 6 4 2 406.34 431.16 14.67 o 7 4 2 2860.56 2811.53 41.84 o 8 4 2 18.33 23.20 6.27 o 9 4 2 187.05 172.10 11.63 o 10 4 2 97.22 95.95 9.80 o 11 4 2 540.00 507.55 20.57 o 12 4 2 31.49 39.02 9.20 o 13 4 2 2978.01 2911.95 52.63 o 14 4 2 410.40 409.44 21.80 o 15 4 2 64.47 68.25 11.33 o 16 4 2 42.77 40.68 12.70 o 17 4 2 0.00 16.21 11.43 o 18 4 2 89.90 102.64 17.50 o 19 4 2 323.77 336.67 26.82 o 20 4 2 1.23 -11.93 14.82 o 21 4 2 148.21 151.15 23.28 o 22 4 2 29.59 128.06 39.96 o 1 5 2 2.94 4.52 6.27 o 2 5 2 663.18 659.54 27.22 o 3 5 2 614.01 616.57 26.31 o 4 5 2 37.91 37.16 8.02 o 5 5 2 916.47 871.30 35.90 o 6 5 2 10.86 16.84 6.71 o 7 5 2 81.96 95.72 9.83 o 8 5 2 361.06 395.07 20.54 o 9 5 2 179.89 172.69 13.20 o 10 5 2 213.89 216.38 15.57 o 11 5 2 737.21 732.03 30.09 o 12 5 2 162.83 178.99 17.72 o 13 5 2 412.99 399.61 23.99 o 14 5 2 17.27 6.98 11.58 o 15 5 2 88.37 110.18 15.36 o 16 5 2 273.66 267.39 23.66 o 17 5 2 360.07 415.61 28.74 o 18 5 2 35.61 51.93 16.07 o 19 5 2 179.80 158.58 25.58 o 20 5 2 23.68 18.57 19.39 o 0 6 2 24.89 39.58 13.30 o 1 6 2 951.88 938.56 30.57 o 2 6 2 83.67 86.23 11.46 o 3 6 2 24.94 24.70 9.60 o 4 6 2 2.66 5.94 8.41 o 5 6 2 737.20 744.29 25.00 o 6 6 2 75.27 104.61 11.25 o 7 6 2 1090.32 1006.84 33.81 o 8 6 2 5.87 12.73 9.60 o 9 6 2 106.54 105.33 18.43 o 10 6 2 11.87 19.94 11.30 o 11 6 2 67.45 60.13 16.89 o 12 6 2 0.87 14.36 11.92 o 13 6 2 762.01 835.81 44.90 o 14 6 2 114.55 126.46 20.07 o 15 6 2 11.13 35.41 14.42 o 16 6 2 25.00 16.14 14.29 o 17 6 2 0.90 36.11 16.97 o 18 6 2 8.37 5.81 19.61 o 19 6 2 118.56 84.78 52.27 o 1 7 2 3.14 11.11 9.82 o 2 7 2 79.11 63.33 13.54 o 3 7 2 179.31 201.59 19.46 o 4 7 2 0.29 7.32 10.37 o 5 7 2 220.39 239.18 20.00 o 6 7 2 5.38 25.78 13.81 o 7 7 2 27.35 42.84 12.56 o 8 7 2 30.75 11.76 15.38 o 9 7 2 43.38 73.12 16.17 o 10 7 2 49.99 45.93 14.31 o 11 7 2 192.67 182.55 23.71 o 12 7 2 14.88 24.58 14.98 o 13 7 2 74.21 94.32 18.58 o 14 7 2 0.21 -7.61 15.67 o 15 7 2 37.12 41.69 16.88 o 16 7 2 69.11 67.31 23.67 o 0 8 2 0.59 -4.53 20.66 o 1 8 2 214.73 269.08 31.27 o 2 8 2 7.58 29.91 17.28 o 3 8 2 1.71 32.35 17.28 o 4 8 2 0.21 1.69 17.82 o 5 8 2 62.68 82.83 26.61 o 6 8 2 22.65 67.09 23.50 o 7 8 2 147.71 72.46 31.29 o 8 8 2 0.10 6.49 23.47 o 9 8 2 10.03 58.36 22.49 o 10 8 2 4.19 -11.24 25.39 o 11 8 2 7.75 86.30 50.14 o 1 9 2 0.47 21.42 44.97 o 2 9 2 6.83 50.78 31.03 o 3 9 2 30.61 13.00 30.05 o 4 9 2 0.89 20.82 41.17 o 5 9 2 36.06 107.72 55.76 o 1 0 3 5760.68 5817.91 91.66 o 2 0 3 2871.99 3035.11 51.65 o 3 0 3 7516.45 7544.92 117.55 o 4 0 3 3024.65 3006.67 52.30 o 5 0 3 7702.16 7798.61 122.32 o 6 0 3 1170.21 1165.67 25.81 o 7 0 3 154.71 192.65 10.93 o 8 0 3 2096.21 2117.68 41.18 o 9 0 3 8228.08 8060.80 141.85 o 10 0 3 280.68 255.19 13.32 o 11 0 3 6185.90 5623.44 106.65 o 12 0 3 1177.64 1111.18 39.86 o 13 0 3 104.63 115.47 14.01 o 14 0 3 149.09 123.90 15.19 o 15 0 3 3543.37 3320.24 132.87 o 16 0 3 821.25 857.41 40.83 o 17 0 3 134.69 126.92 20.37 o 18 0 3 177.79 184.83 29.60 o 19 0 3 340.55 289.16 35.37 o 20 0 3 628.00 598.85 61.38 o 21 0 3 4.32 42.67 42.86 o 22 0 3 0.96 5.86 20.16 o 23 0 3 252.58 336.58 68.20 o 24 0 3 49.46 71.52 27.71 o 0 1 3 14749.12 15779.18 258.27 o 1 1 3 2894.80 3231.68 38.13 o 2 1 3 561.64 622.97 10.98 o 3 1 3 2601.60 2645.44 32.73 o 4 1 3 676.26 594.87 11.32 o 5 1 3 5.58 15.35 3.44 o 6 1 3 255.97 288.41 9.46 o 7 1 3 11551.40 11846.51 129.11 o 8 1 3 216.50 297.87 10.11 o 9 1 3 1089.81 1172.65 21.33 o 10 1 3 1451.83 1408.43 24.68 o 11 1 3 1.70 6.32 5.20 o 12 1 3 317.84 314.64 14.17 o 13 1 3 416.45 456.79 19.23 o 14 1 3 2581.99 2471.05 44.67 o 15 1 3 5479.10 5489.59 82.62 o 16 1 3 9.52 14.30 9.40 o 17 1 3 83.33 96.61 14.68 o 18 1 3 154.93 150.68 16.99 o 19 1 3 348.37 368.05 24.49 o 20 1 3 40.36 27.34 13.01 o 21 1 3 784.26 658.36 33.24 o 22 1 3 139.83 129.84 18.94 o 23 1 3 103.24 88.68 18.42 o 24 1 3 32.01 36.05 19.43 o 1 2 3 3848.19 3853.08 60.80 o 2 2 3 854.63 824.65 14.33 o 3 2 3 4975.32 5247.88 70.55 o 4 2 3 1552.01 1450.55 22.63 o 5 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o 6 0 10 731.61 811.58 54.28 o 7 0 10 196.13 199.44 32.22 o 8 0 10 580.32 722.43 68.08 o 9 0 10 786.03 681.93 66.40 o 10 0 10 16.11 40.91 39.12 o 11 0 10 78.21 53.19 29.93 o 12 0 10 1144.44 1179.03 92.23 o 13 0 10 384.69 404.04 170.40 o 14 0 10 1002.35 868.82 90.33 o 15 0 10 101.29 138.24 37.08 o 16 0 10 2.02 5.24 39.35 o 17 0 10 101.98 89.96 35.25 o 18 0 10 98.82 82.20 44.82 o 1 1 10 132.51 118.72 13.95 o 2 1 10 343.47 382.86 19.99 o 3 1 10 278.98 254.85 17.05 o 4 1 10 6.30 10.65 9.76 o 5 1 10 45.25 50.53 11.32 o 6 1 10 556.87 491.78 23.56 o 7 1 10 16.99 4.83 10.67 o 8 1 10 22.43 17.00 13.11 o 9 1 10 49.62 45.19 15.20 o 10 1 10 275.33 240.86 34.73 o 11 1 10 24.88 20.97 14.19 o 12 1 10 813.88 902.45 42.88 o 13 1 10 233.38 222.23 28.28 o 14 1 10 94.23 126.60 20.94 o 15 1 10 51.72 53.94 17.21 o 16 1 10 220.34 205.63 37.28 o 17 1 10 165.86 247.31 29.17 o 18 1 10 627.28 599.97 68.13 o 0 2 10 2595.23 2456.45 103.61 o 1 2 10 315.47 336.22 21.38 o 2 2 10 204.35 219.90 20.10 o 3 2 10 171.67 184.63 16.66 o 4 2 10 562.31 541.92 30.50 o 5 2 10 164.55 204.72 17.72 o 6 2 10 871.09 847.11 32.98 o 7 2 10 62.05 44.85 12.79 o 8 2 10 652.20 667.38 30.65 o 9 2 10 645.99 615.25 38.19 o 10 2 10 33.02 40.57 13.94 o 11 2 10 45.82 12.64 16.52 o 12 2 10 732.36 731.23 44.20 o 13 2 10 287.42 318.33 28.11 o 14 2 10 621.55 710.42 40.95 o 15 2 10 72.22 58.87 18.58 o 16 2 10 1.69 -14.91 14.91 o 17 2 10 74.31 102.02 25.98 o 18 2 10 112.06 108.57 33.73 o 1 3 10 95.36 85.47 13.87 o 2 3 10 294.30 287.45 20.71 o 3 3 10 240.89 270.64 19.98 o 4 3 10 7.44 32.55 11.25 o 5 3 10 78.12 114.56 16.74 o 6 3 10 343.09 318.36 24.40 o 7 3 10 27.29 13.82 12.91 o 8 3 10 55.82 83.15 15.98 o 9 3 10 28.45 28.08 14.02 o 10 3 10 225.75 214.51 23.24 o 11 3 10 4.17 0.76 17.43 o 12 3 10 412.99 505.40 32.05 o 13 3 10 57.44 62.74 17.35 o 14 3 10 22.74 7.17 16.08 o 15 3 10 71.23 71.20 19.61 o 16 3 10 139.40 140.12 28.86 o 0 4 10 1152.97 1064.97 55.18 o 1 4 10 149.32 217.75 19.41 o 2 4 10 108.68 141.47 16.65 o 3 4 10 29.04 36.06 12.27 o 4 4 10 234.14 199.86 20.04 o 5 4 10 88.47 92.96 16.59 o 6 4 10 530.71 575.13 33.64 o 7 4 10 10.33 12.66 13.70 o 8 4 10 346.32 386.71 28.47 o 9 4 10 251.82 267.28 24.58 o 10 4 10 5.11 -12.79 12.79 o 11 4 10 3.79 29.30 17.65 o 12 4 10 358.63 350.85 31.00 o 13 4 10 127.81 176.70 24.79 o 14 4 10 283.03 280.75 45.05 o 15 4 10 28.84 39.81 50.44 o 1 5 10 27.79 33.37 13.64 o 2 5 10 178.58 135.68 19.91 o 3 5 10 70.06 93.12 18.38 o 4 5 10 8.64 22.64 14.63 o 5 5 10 23.04 9.55 14.73 o 6 5 10 174.45 182.38 22.28 o 7 5 10 1.00 -0.19 15.57 o 8 5 10 47.74 48.11 17.73 o 9 5 10 1.53 25.70 16.70 o 10 5 10 114.72 142.40 21.13 o 11 5 10 16.94 11.16 19.83 o 12 5 10 125.12 153.00 78.85 o 13 5 10 28.09 194.02 81.74 o 0 6 10 371.55 383.76 43.17 o 1 6 10 50.33 85.89 16.96 o 2 6 10 58.36 59.26 17.93 o 3 6 10 0.40 -10.75 15.09 o 4 6 10 26.78 15.31 16.04 o 5 6 10 20.08 29.45 16.58 o 6 6 10 143.40 197.93 32.46 o 7 6 10 1.81 -23.09 29.34 o 8 6 10 84.46 77.03 51.81 o 1 0 11 33.41 -1.02 18.25 o 2 0 11 285.10 325.92 36.88 o 3 0 11 685.04 716.81 52.68 o 4 0 11 87.73 108.58 26.56 o 5 0 11 1754.13 1831.63 76.64 o 6 0 11 19.54 25.02 21.18 o 7 0 11 1.16 -1.99 23.41 o 8 0 11 112.87 186.37 37.67 o 9 0 11 1141.41 1065.68 123.90 o 10 0 11 313.64 380.80 54.82 o 11 0 11 309.62 250.55 47.09 o 12 0 11 20.69 10.13 30.42 o 13 0 11 75.80 91.25 31.89 o 14 0 11 25.19 37.80 37.45 o 15 0 11 15.10 -24.16 24.16 o 16 0 11 10.72 50.56 33.36 o 17 0 11 180.79 247.20 67.76 o 0 1 11 76.14 71.71 27.61 o 1 1 11 352.22 367.77 34.81 o 2 1 11 108.35 120.38 23.19 o 3 1 11 46.72 67.19 15.90 o 4 1 11 94.23 73.20 14.85 o 5 1 11 25.52 29.14 13.35 o 6 1 11 156.34 195.87 26.63 o 7 1 11 1081.25 1053.37 50.49 o 8 1 11 49.62 76.32 22.70 o 9 1 11 626.62 743.82 50.80 o 10 1 11 22.42 40.62 19.47 o 11 1 11 152.72 159.78 39.19 o 12 1 11 103.80 103.69 25.05 o 13 1 11 205.10 209.75 30.88 o 14 1 11 56.27 74.76 23.19 o 15 1 11 1.79 17.71 26.05 o 16 1 11 157.42 159.25 34.30 o 17 1 11 115.03 55.65 32.90 o 1 2 11 10.98 30.07 11.67 o 2 2 11 274.45 262.55 20.02 o 3 2 11 615.01 587.70 28.69 o 4 2 11 105.02 140.01 16.12 o 5 2 11 1389.64 1337.40 58.03 o 6 2 11 11.53 -1.23 13.04 o 7 2 11 5.18 1.58 12.29 o 8 2 11 91.71 85.88 16.87 o 9 2 11 658.33 689.43 34.61 o 10 2 11 216.45 186.78 22.85 o 11 2 11 197.88 184.93 22.39 o 12 2 11 4.46 32.90 16.28 o 13 2 11 81.34 109.74 20.56 o 14 2 11 41.97 48.39 18.41 o 15 2 11 27.86 56.43 21.23 o 16 2 11 1.09 2.56 26.65 o 0 3 11 49.86 48.13 21.23 o 1 3 11 234.60 248.71 20.42 o 2 3 11 27.40 9.81 11.74 o 3 3 11 7.68 26.68 12.32 o 4 3 11 2.45 4.48 11.59 o 5 3 11 11.63 13.51 12.50 o 6 3 11 235.45 203.58 26.29 o 7 3 11 591.48 569.97 33.17 o 8 3 11 73.74 19.32 14.64 o 9 3 11 361.88 341.36 27.00 o 10 3 11 27.98 15.40 17.14 o 11 3 11 91.06 107.04 20.55 o 12 3 11 60.86 51.59 18.25 o 13 3 11 179.16 162.06 38.51 o 14 3 11 16.30 -8.93 36.38 o 15 3 11 6.60 -41.33 41.33 o 1 4 11 0.42 15.44 12.08 o 2 4 11 161.94 173.69 18.50 o 3 4 11 300.73 322.76 23.44 o 4 4 11 83.14 84.23 18.32 o 5 4 11 494.93 516.62 36.78 o 6 4 11 4.59 -11.67 20.92 o 7 4 11 5.24 26.03 16.41 o 8 4 11 58.37 56.43 17.79 o 9 4 11 242.88 283.04 25.88 o 10 4 11 104.98 99.31 21.08 o 11 4 11 142.78 126.11 21.91 o 12 4 11 0.88 -12.75 22.33 o 13 4 11 22.22 -8.20 54.70 o 0 5 11 79.73 108.68 26.46 o 1 5 11 144.78 89.71 21.52 o 2 5 11 28.73 40.87 16.54 o 3 5 11 0.26 5.80 15.42 o 4 5 11 1.81 5.11 15.30 o 5 5 11 5.23 -1.32 19.12 o 6 5 11 76.89 45.41 17.91 o 7 5 11 201.02 214.13 29.70 o 8 5 11 10.95 24.68 23.25 o 9 5 11 143.65 161.69 48.87 o 10 5 11 1.81 7.75 43.15 o 1 6 11 2.26 -27.20 34.79 o 2 6 11 46.24 95.11 50.75 o 0 0 12 3.79 25.22 39.81 o 1 0 12 2254.32 2157.78 112.20 o 2 0 12 15.15 1.16 20.01 o 3 0 12 0.07 40.23 33.96 o 4 0 12 10.26 21.86 20.98 o 5 0 12 1300.06 1309.32 70.20 o 6 0 12 1.53 27.28 36.01 o 7 0 12 359.29 351.99 66.47 o 8 0 12 152.08 192.21 39.57 o 9 0 12 90.95 125.22 37.71 o 10 0 12 169.26 149.33 37.30 o 11 0 12 72.09 73.79 33.43 o 12 0 12 245.02 262.16 46.40 o 13 0 12 226.07 255.49 68.75 o 14 0 12 2.40 -12.16 29.44 o 1 1 12 574.02 537.32 33.75 o 2 1 12 5.77 32.80 15.37 o 3 1 12 575.71 515.20 38.04 o 4 1 12 36.58 52.27 24.01 o 5 1 12 8.26 -5.85 16.18 o 6 1 12 46.49 63.51 22.02 o 7 1 12 0.75 21.00 17.95 o 8 1 12 0.25 -0.76 17.45 o 9 1 12 21.35 38.91 19.82 o 10 1 12 20.80 82.71 22.56 o 11 1 12 536.56 500.50 44.61 o 12 1 12 24.97 65.15 22.21 o 13 1 12 78.52 24.95 21.82 o 14 1 12 5.11 4.97 36.69 o 0 2 12 16.33 92.61 20.94 o 1 2 12 1640.27 1577.22 52.99 o 2 2 12 0.41 12.73 11.87 o 3 2 12 1.98 9.21 12.08 o 4 2 12 0.23 12.63 12.01 o 5 2 12 844.04 801.17 40.89 o 6 2 12 3.62 36.31 18.54 o 7 2 12 226.14 270.52 29.87 o 8 2 12 65.00 99.91 24.71 o 9 2 12 60.48 81.27 22.40 o 10 2 12 100.06 139.08 30.44 o 11 2 12 80.26 87.94 23.90 o 12 2 12 209.04 269.04 41.17 o 13 2 12 222.94 247.28 51.26 o 1 3 12 301.24 311.37 23.93 o 2 3 12 5.14 14.06 12.83 o 3 3 12 309.14 335.19 24.32 o 4 3 12 5.84 25.06 14.04 o 5 3 12 20.46 34.37 20.61 o 6 3 12 13.69 9.79 14.16 o 7 3 12 8.04 -0.20 15.72 o 8 3 12 0.02 -13.14 16.42 o 9 3 12 19.46 26.02 20.40 o 10 3 12 28.77 29.68 17.60 o 11 3 12 313.17 301.72 48.63 o 12 3 12 1.84 -5.16 34.11 o 0 4 12 6.00 52.03 21.70 o 1 4 12 656.41 665.94 34.74 o 2 4 12 0.27 24.97 14.00 o 3 4 12 5.26 12.60 15.93 o 4 4 12 0.40 -7.25 14.39 o 5 4 12 310.20 311.78 26.81 o 6 4 12 1.73 21.27 16.31 o 7 4 12 102.45 147.25 21.85 o 8 4 12 22.74 19.28 28.38 o 9 4 12 48.86 66.37 29.12 o 1 5 12 93.86 110.84 31.14 o 2 5 12 0.09 6.08 40.42 o 3 5 12 89.73 123.22 54.24 o 1 0 13 16.75 13.57 30.01 o 2 0 13 367.05 408.32 57.75 o 3 0 13 514.08 536.06 67.57 o 4 0 13 129.69 175.46 58.65 o 5 0 13 192.40 273.26 88.96 o 6 0 13 3.22 -16.99 23.89 o 7 0 13 7.48 36.91 32.17 o 8 0 13 14.68 41.59 29.78 o 9 0 13 592.75 681.74 95.57 o 10 0 13 125.86 142.68 89.11 o 11 0 13 40.61 136.44 54.39 o 12 0 13 50.02 9.72 52.57 o 0 1 13 354.73 330.66 53.37 o 1 1 13 48.91 69.26 20.00 o 2 1 13 47.41 77.90 21.80 o 3 1 13 326.99 403.95 36.24 o 4 1 13 67.58 48.96 21.10 o 5 1 13 7.95 27.47 22.02 o 6 1 13 106.54 114.90 30.72 o 7 1 13 528.63 557.94 55.73 o 8 1 13 64.17 84.06 29.71 o 9 1 13 3.06 -15.56 26.52 o 10 1 13 27.45 24.21 24.19 o 11 1 13 23.13 51.55 59.79 o 1 2 13 11.24 42.39 18.12 o 2 2 13 272.53 295.13 35.60 o 3 2 13 384.93 389.69 34.61 o 4 2 13 88.79 116.70 28.58 o 5 2 13 136.44 165.37 30.57 o 6 2 13 0.33 10.87 21.00 o 7 2 13 1.47 36.78 25.79 o 8 2 13 33.05 60.21 28.01 o 9 2 13 387.03 464.17 82.96 o 0 3 13 285.92 278.06 33.28 o 1 3 13 47.72 48.61 15.67 o 2 3 13 48.67 66.39 16.35 o 3 3 13 187.73 193.35 25.33 o 4 3 13 32.59 47.97 21.53 o 5 3 13 0.51 23.09 16.02 o 6 3 13 69.78 61.57 18.58 o 7 3 13 202.80 237.78 44.05 o 8 3 13 39.04 167.59 48.32 o 1 4 13 3.92 21.56 18.75 o 2 4 13 137.51 164.95 32.90 o 3 4 13 171.61 166.08 27.65 o 4 4 13 53.73 53.50 30.77 o 5 4 13 41.22 12.91 46.04 o 0 0 14 269.96 186.73 73.99 o 1 0 14 33.42 59.47 38.55 o 2 0 14 282.11 287.13 70.73 o 3 0 14 23.21 39.05 37.09 o 4 0 14 96.36 168.19 71.11 o 5 0 14 47.06 87.36 53.63 o 1 1 14 50.53 38.74 28.44 o 2 1 14 179.09 225.03 36.08 o 3 1 14 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