# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_1 _shelx_title ' QJY20 in P-1 Co(C36H24N6O3Cl3).H2O' _shelx_refln_list_code 4 _shelx_F_calc_maximum 156.93 _exptl_crystal_F_000 788.00 _reflns_d_resolution_high 0.7652 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.4841 _cell_length_b 10.7961 _cell_length_c 18.7158 _cell_angle_alpha 102.378 _cell_angle_beta 93.416 _cell_angle_gamma 113.011 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 190.08 184.85 11.20 o 3 0 0 718.34 713.35 19.77 o 4 0 0 136.25 142.41 15.42 o 5 0 0 54.72 37.52 24.52 o 6 0 0 1201.64 1215.89 36.30 o 7 0 0 447.54 451.45 29.95 o 8 0 0 36.37 66.92 27.12 o 9 0 0 240.48 342.20 59.01 o 10 0 0 53.27 44.61 36.21 o -11 1 0 0.13 -26.83 50.31 o -10 1 0 67.91 113.84 37.02 o -9 1 0 32.61 37.69 29.63 o -8 1 0 0.37 29.65 26.07 o -7 1 0 1972.55 2022.61 118.75 o -6 1 0 583.09 548.98 63.76 o -5 1 0 376.40 350.72 21.52 o -4 1 0 1529.50 1218.88 26.19 o -3 1 0 8518.28 8636.91 60.96 o -2 1 0 6484.71 6310.56 44.32 o -1 1 0 13023.81 13369.32 89.18 o 1 1 0 66.64 74.01 6.73 o 2 1 0 1669.72 1698.23 46.97 o 3 1 0 3193.79 3207.53 30.11 o 4 1 0 234.45 249.42 14.50 o 5 1 0 1383.97 1384.15 56.43 o 6 1 0 370.40 376.35 40.73 o 7 1 0 3.86 14.34 26.46 o 8 1 0 145.08 144.08 31.83 o 9 1 0 195.94 229.14 42.55 o 10 1 0 3.40 -10.50 48.30 o -11 2 0 1.47 -14.52 51.58 o -10 2 0 0.83 37.41 34.30 o -9 2 0 18.12 36.95 28.55 o -8 2 0 142.18 159.30 28.01 o -7 2 0 129.22 150.66 24.15 o -6 2 0 0.04 11.72 16.17 o -5 2 0 395.66 335.25 61.75 o -4 2 0 11.81 2.83 9.74 o -3 2 0 1260.02 1296.03 61.07 o -2 2 0 133.59 135.79 9.98 o -1 2 0 5337.59 5775.29 153.75 o 0 2 0 6174.33 6691.74 69.45 o 1 2 0 20263.42 19359.47 147.05 o 2 2 0 2029.33 1787.41 56.10 o 3 2 0 228.88 171.67 13.90 o 4 2 0 571.85 503.58 19.84 o 5 2 0 514.07 507.02 30.09 o 6 2 0 106.90 75.30 43.50 o 7 2 0 132.34 180.36 29.60 o 8 2 0 98.40 164.45 54.13 o 9 2 0 18.46 44.89 52.52 o 10 2 0 158.48 84.37 60.62 o -12 3 0 60.85 16.39 58.21 o -11 3 0 0.55 -37.33 48.51 o -10 3 0 40.45 50.51 45.29 o -9 3 0 2.96 27.13 26.07 o -8 3 0 721.49 693.35 36.68 o -7 3 0 0.79 -14.16 25.66 o -6 3 0 440.69 373.47 28.57 o -5 3 0 586.14 553.85 23.50 o -4 3 0 4243.18 3969.06 127.99 o -3 3 0 1914.58 1651.51 88.85 o -2 3 0 5963.90 6210.48 77.34 o -1 3 0 1089.33 799.09 50.68 o 0 3 0 4174.01 3579.97 53.46 o 1 3 0 1472.25 1353.80 39.94 o 2 3 0 126.86 145.27 13.52 o 3 3 0 5026.28 5197.70 71.12 o 4 3 0 3.76 19.13 17.93 o 5 3 0 46.72 37.66 39.00 o 6 3 0 73.99 48.04 22.98 o 7 3 0 23.44 -4.35 46.10 o 8 3 0 101.52 53.32 50.31 o 9 3 0 95.63 85.84 50.58 o -12 4 0 43.25 99.29 61.02 o -11 4 0 0.25 -1.00 50.78 o -10 4 0 27.95 54.73 46.10 o -9 4 0 529.47 516.25 36.35 o -8 4 0 373.72 406.81 36.09 o -7 4 0 684.79 681.40 54.36 o -6 4 0 14.18 -17.19 24.35 o -5 4 0 783.77 807.97 80.08 o -4 4 0 2.45 -10.83 10.83 o -3 4 0 3403.44 3474.60 124.11 o -2 4 0 4141.06 4120.92 40.81 o -1 4 0 5530.66 5805.99 77.54 o 0 4 0 2491.74 2198.13 49.71 o 1 4 0 96.94 75.20 20.61 o 2 4 0 2629.33 2961.30 70.45 o 3 4 0 5.90 -5.82 26.29 o 4 4 0 124.47 176.08 20.54 o 5 4 0 167.94 233.60 29.71 o 6 4 0 209.59 217.37 54.19 o 7 4 0 54.22 -9.30 49.91 o 8 4 0 39.47 31.18 53.66 o 9 4 0 41.92 -46.36 55.66 o -12 5 0 2.41 -44.22 52.32 o -11 5 0 39.85 71.72 51.72 o -10 5 0 33.60 72.19 44.62 o -9 5 0 892.92 958.33 59.01 o -8 5 0 1185.61 1368.45 65.90 o -7 5 0 351.60 396.34 45.03 o -6 5 0 111.75 106.77 39.94 o -5 5 0 1558.59 1411.63 33.66 o -4 5 0 2490.09 2149.02 37.46 o -3 5 0 380.53 319.82 19.10 o -2 5 0 938.75 1041.21 35.49 o -1 5 0 3476.41 3688.01 71.19 o 0 5 0 59.38 33.92 26.29 o 1 5 0 92.74 76.07 25.09 o 2 5 0 2097.90 1875.65 56.80 o 3 5 0 0.65 -11.64 23.42 o 4 5 0 68.31 54.93 30.44 o 5 5 0 331.95 401.62 46.83 o 6 5 0 19.43 -34.46 49.44 o 7 5 0 41.12 61.28 54.26 o 8 5 0 49.72 27.97 55.33 o -12 6 0 9.11 -19.07 57.27 o -11 6 0 31.89 48.24 50.38 o -10 6 0 21.28 22.08 46.50 o -9 6 0 166.36 237.98 49.98 o -8 6 0 299.88 330.64 47.23 o -7 6 0 331.91 266.41 40.95 o -6 6 0 0.36 -0.42 18.87 o -5 6 0 1021.77 1063.01 80.32 o -4 6 0 472.88 454.48 25.62 o -3 6 0 3858.62 3824.61 72.39 o -2 6 0 507.87 476.86 21.15 o -1 6 0 6.99 -22.41 22.41 o 0 6 0 257.08 292.30 38.27 o 1 6 0 3082.75 3663.26 89.25 o 2 6 0 45.13 49.71 32.11 o 3 6 0 19.40 20.41 36.53 o 4 6 0 265.54 399.22 53.59 o 5 6 0 8.46 8.36 43.96 o 6 6 0 47.62 -7.89 58.21 o 7 6 0 43.95 35.12 56.53 o -12 7 0 0.45 -1.54 58.61 o -11 7 0 54.05 59.75 52.65 o -10 7 0 8.97 57.67 48.10 o -9 7 0 317.73 316.46 56.07 o -8 7 0 46.48 83.70 42.08 o -7 7 0 0.63 2.21 23.01 o -6 7 0 1222.28 1151.63 39.08 o -5 7 0 112.32 129.19 23.03 o -4 7 0 43.37 21.65 19.69 o -3 7 0 445.32 449.96 69.58 o -2 7 0 141.18 136.91 19.57 o -1 7 0 35.04 -3.95 30.04 o 0 7 0 783.09 726.24 49.17 o 1 7 0 1037.88 1174.16 62.76 o 2 7 0 594.57 667.57 60.88 o 3 7 0 3.35 -18.93 36.73 o 4 7 0 28.41 30.91 43.42 o 5 7 0 60.46 21.34 46.63 o 6 7 0 167.94 136.75 67.51 o 7 7 0 0.83 -40.48 58.07 o -12 8 0 7.82 34.92 64.76 o -11 8 0 4.10 1.07 50.85 o -10 8 0 9.56 62.15 50.24 o -9 8 0 94.00 50.18 46.36 o -8 8 0 17.53 41.08 41.48 o -7 8 0 159.13 115.04 29.17 o -6 8 0 230.88 255.96 31.59 o -5 8 0 148.83 169.32 26.46 o -4 8 0 2.16 -31.55 31.55 o -3 8 0 4.94 -16.74 17.63 o -2 8 0 254.84 292.37 43.35 o -1 8 0 1136.35 1306.63 67.04 o 0 8 0 0.81 -31.38 31.38 o 1 8 0 68.16 76.54 40.01 o 2 8 0 38.22 33.32 39.47 o 3 8 0 0.68 -39.01 39.01 o 4 8 0 2.25 -8.36 43.02 o 6 8 0 3.91 -17.46 69.04 o -11 9 0 15.09 21.34 48.44 o -10 9 0 53.85 23.15 41.28 o -9 9 0 0.69 2.01 44.56 o -8 9 0 137.35 143.31 45.90 o -7 9 0 34.17 68.35 28.91 o -6 9 0 167.23 229.59 33.92 o -5 9 0 5.26 -34.46 34.46 o -4 9 0 1.04 -44.22 44.22 o -3 9 0 87.16 70.05 47.70 o -2 9 0 12.23 4.68 35.33 o -1 9 0 8.11 -16.66 36.26 o 0 9 0 0.84 -11.44 41.95 o 1 9 0 129.46 168.00 51.32 o 2 9 0 15.40 29.04 47.50 o 3 9 0 2.61 24.62 48.77 o 4 9 0 15.27 36.46 53.79 o -11 10 0 5.41 -7.43 46.03 o -10 10 0 0.03 -13.25 40.95 o -9 10 0 0.49 -23.15 46.10 o -8 10 0 10.59 -7.09 43.22 o -7 10 0 0.07 -30.86 30.86 o -6 10 0 322.38 478.40 67.81 o -5 10 0 268.96 368.57 60.82 o -4 10 0 15.16 -54.26 54.26 o -3 10 0 60.93 125.38 54.93 o -2 10 0 147.45 327.70 63.09 o -1 10 0 104.64 70.52 37.20 o 0 10 0 23.16 20.34 28.17 o 1 10 0 191.47 231.35 53.79 o 2 10 0 0.02 5.62 22.61 o 3 10 0 32.35 -1.87 19.80 o 4 10 0 18.16 12.51 22.61 o -10 11 0 29.04 -7.89 39.14 o -9 11 0 84.21 20.07 38.67 o -7 11 0 325.33 484.05 69.51 o -6 11 0 132.35 187.40 65.03 o -5 11 0 0.34 -25.36 52.92 o -4 11 0 4.13 -48.97 57.87 o -3 11 0 126.10 206.06 57.27 o -2 11 0 80.46 240.12 68.71 o -1 11 0 26.86 -5.89 58.41 o 0 11 0 55.13 74.73 51.05 o 1 11 0 0.52 27.03 42.22 o 2 11 0 3.10 -5.62 32.18 o -7 12 0 268.89 399.95 76.54 o -6 12 0 78.92 83.43 66.77 o -5 12 0 1.83 -20.47 58.54 o -4 12 0 71.41 157.63 74.66 o -3 12 0 41.26 179.37 77.68 o -2 12 0 199.96 362.35 69.18 o -1 12 0 38.18 132.47 70.99 o 0 12 0 0.88 -3.41 60.48 o 1 12 0 2.59 36.53 47.43 o -7 13 0 0.94 57.40 73.26 o -6 13 0 3.05 -45.49 70.85 o -5 13 0 44.03 123.24 79.28 o -4 13 0 34.68 107.45 77.07 o -3 13 0 51.83 160.77 82.16 o -2 13 0 166.08 333.11 89.45 o 2 -13 1 0.07 70.12 71.25 o 3 -13 1 80.60 243.33 81.49 o 4 -13 1 12.58 17.66 73.66 o 5 -13 1 0.83 -14.52 72.06 o 6 -13 1 2.92 30.51 74.66 o 7 -13 1 54.29 19.80 78.55 o -1 -12 1 28.49 5.95 43.55 o 0 -12 1 18.69 14.79 53.79 o 1 -12 1 16.88 74.00 69.85 o 2 -12 1 28.04 91.73 71.72 o 3 -12 1 151.32 236.30 72.39 o 4 -12 1 35.30 118.82 73.46 o 5 -12 1 73.00 142.97 72.19 o 6 -12 1 332.87 534.30 79.48 o 7 -12 1 5.59 24.89 63.02 o -2 -11 1 19.85 -6.02 56.33 o -1 -11 1 11.21 -11.64 52.05 o 0 -11 1 0.66 8.36 49.64 o 1 -11 1 35.05 20.14 35.73 o 2 -11 1 476.88 673.66 63.22 o 3 -11 1 172.05 322.28 69.18 o 4 -11 1 222.06 264.47 57.54 o 5 -11 1 95.51 134.48 66.37 o 6 -11 1 117.96 152.74 60.08 o 7 -11 1 141.33 153.88 62.62 o 8 -11 1 154.01 160.30 50.85 o 9 -11 1 7.83 38.20 43.89 o 10 -11 1 72.19 33.12 44.96 o -4 -10 1 9.38 56.27 60.21 o -3 -10 1 18.15 -6.49 56.67 o -2 -10 1 43.83 70.58 49.91 o -1 -10 1 96.01 145.18 46.97 o 0 -10 1 104.06 94.74 50.71 o 1 -10 1 447.18 625.89 65.63 o 2 -10 1 9.28 48.51 44.29 o 3 -10 1 263.28 350.98 62.22 o 4 -10 1 409.86 544.33 68.98 o 5 -10 1 59.83 53.72 55.40 o 6 -10 1 7.27 -2.20 30.12 o 7 -10 1 317.97 374.62 39.60 o 8 -10 1 0.21 -39.54 40.08 o 9 -10 1 168.99 73.33 48.10 o 10 -10 1 79.43 104.70 50.65 o 11 -10 1 11.73 -48.10 48.10 o -4 -9 1 35.13 59.34 52.99 o -3 -9 1 0.44 -22.75 41.95 o -2 -9 1 42.72 20.61 39.87 o -1 -9 1 0.38 -13.78 37.27 o 0 -9 1 784.37 889.09 62.96 o 1 -9 1 22.76 14.52 36.20 o 2 -9 1 151.95 167.26 44.49 o 3 -9 1 36.44 -28.30 32.85 o 4 -9 1 3.83 -50.88 50.88 o 5 -9 1 27.57 -30.44 30.44 o 6 -9 1 206.32 267.27 33.98 o 7 -9 1 11.09 38.59 45.93 o 8 -9 1 33.02 3.81 42.42 o 9 -9 1 229.21 165.65 49.98 o 10 -9 1 8.79 -4.08 47.97 o 11 -9 1 16.57 19.74 53.05 o -6 -8 1 74.81 81.82 66.97 o -5 -8 1 3.81 -44.29 46.03 o -4 -8 1 16.85 50.85 48.77 o -3 -8 1 6.39 -33.65 43.09 o -2 -8 1 20.18 16.39 39.94 o -1 -8 1 661.51 798.10 63.96 o 0 -8 1 57.10 51.78 37.67 o 1 -8 1 15.81 3.01 31.38 o 2 -8 1 36.13 18.13 18.00 o 3 -8 1 145.46 123.94 22.30 o 4 -8 1 5.54 -11.43 19.32 o 5 -8 1 423.21 467.22 48.41 o 6 -8 1 32.19 10.83 24.63 o 7 -8 1 300.20 269.00 42.99 o 8 -8 1 162.46 145.25 46.83 o 9 -8 1 116.22 89.52 47.70 o 10 -8 1 82.90 50.04 56.27 o 11 -8 1 7.17 6.82 54.66 o -7 -7 1 59.22 31.85 60.68 o -6 -7 1 9.10 29.84 57.34 o -5 -7 1 179.15 274.84 57.47 o -4 -7 1 138.59 196.10 51.11 o -3 -7 1 8.50 -18.87 34.25 o -2 -7 1 520.10 499.84 51.38 o -1 -7 1 22.80 80.28 31.71 o 0 -7 1 125.77 72.66 40.54 o 1 -7 1 1101.34 1098.63 55.00 o 2 -7 1 923.61 695.36 27.04 o 3 -7 1 993.47 807.85 59.68 o 4 -7 1 695.22 617.74 30.07 o 5 -7 1 16.11 -24.49 28.23 o 6 -7 1 368.09 378.03 30.72 o 7 -7 1 34.23 18.53 34.66 o 8 -7 1 547.58 561.39 50.71 o 9 -7 1 22.57 101.16 46.97 o 10 -7 1 89.03 178.03 55.26 o 11 -7 1 3.69 19.67 54.33 o 12 -7 1 20.42 18.20 58.94 o -8 -6 1 26.30 35.06 57.20 o -7 -6 1 14.25 -21.14 57.94 o -6 -6 1 184.69 68.78 54.79 o -5 -6 1 233.51 276.38 47.57 o -4 -6 1 245.35 276.05 43.09 o -3 -6 1 38.33 -5.15 33.12 o -2 -6 1 488.30 453.74 46.10 o -1 -6 1 6.18 -18.33 26.90 o 0 -6 1 690.29 633.31 39.21 o 1 -6 1 1222.19 1238.86 51.45 o 2 -6 1 19.45 -16.10 25.59 o 3 -6 1 1021.71 865.20 28.61 o 4 -6 1 1693.68 1602.13 68.51 o 5 -6 1 375.82 345.58 24.85 o 6 -6 1 227.45 188.34 25.05 o 7 -6 1 419.57 494.29 44.83 o 8 -6 1 12.44 99.22 40.14 o 9 -6 1 1194.52 1197.18 63.02 o 10 -6 1 106.71 119.96 42.89 o 11 -6 1 16.06 73.73 50.04 o 12 -6 1 10.10 1.14 59.48 o -8 -5 1 14.24 -16.06 51.05 o -7 -5 1 126.13 117.68 51.58 o -6 -5 1 31.92 -28.97 51.58 o -5 -5 1 6.80 8.36 37.00 o -4 -5 1 5.75 -32.78 32.78 o -3 -5 1 351.06 348.64 40.95 o -2 -5 1 408.24 407.45 40.01 o -1 -5 1 924.60 795.69 41.55 o 0 -5 1 3976.85 3604.12 71.59 o 1 -5 1 0.02 -1.74 12.38 o 2 -5 1 1528.74 1384.20 63.26 o 3 -5 1 2.94 -12.78 12.78 o 4 -5 1 1270.15 1318.42 32.23 o 5 -5 1 3.45 22.02 17.53 o 6 -5 1 283.37 275.13 34.76 o 7 -5 1 368.32 404.37 42.68 o 8 -5 1 2500.39 2328.39 75.87 o 9 -5 1 708.01 825.46 57.87 o 10 -5 1 0.79 -11.78 43.62 o 11 -5 1 58.25 46.57 50.85 o 12 -5 1 6.95 54.06 59.34 o -9 -4 1 16.39 -20.94 50.24 o -8 -4 1 13.88 -24.55 49.64 o -7 -4 1 7.68 13.58 51.58 o -6 -4 1 212.46 202.56 33.97 o -5 -4 1 45.67 -27.43 33.92 o -4 -4 1 239.80 244.68 22.64 o -3 -4 1 1564.28 1615.87 92.03 o -2 -4 1 705.50 473.86 24.23 o -1 -4 1 219.30 267.08 30.51 o 0 -4 1 329.53 325.89 30.24 o 1 -4 1 3.81 -4.41 31.34 o 2 -4 1 765.76 649.83 21.29 o 3 -4 1 55.72 29.68 10.93 o 4 -4 1 1986.40 1652.73 47.13 o 5 -4 1 468.68 336.33 62.72 o 6 -4 1 1275.75 1196.47 34.29 o 7 -4 1 21.52 35.32 20.13 o 8 -4 1 1227.23 1201.25 43.67 o 9 -4 1 44.34 27.00 25.69 o 10 -4 1 0.49 -3.06 30.03 o 11 -4 1 70.48 90.39 53.59 o 12 -4 1 20.09 21.88 55.86 o -9 -3 1 1.47 33.99 55.46 o -8 -3 1 1.19 19.07 47.64 o -7 -3 1 65.98 47.84 48.04 o -6 -3 1 128.91 122.50 21.19 o -5 -3 1 1292.30 1213.39 31.70 o -4 -3 1 1575.37 1501.90 60.18 o -3 -3 1 478.09 325.38 53.79 o -2 -3 1 174.49 160.63 13.44 o -1 -3 1 7.59 8.48 7.89 o 0 -3 1 2783.42 2352.92 36.06 o 1 -3 1 20220.68 20092.55 133.77 o 2 -3 1 2627.92 2307.36 125.11 o 3 -3 1 2160.67 1977.73 28.35 o 4 -3 1 328.87 362.28 21.28 o 5 -3 1 54.25 76.92 17.69 o 6 -3 1 108.57 86.17 19.18 o 7 -3 1 370.22 373.11 27.72 o 8 -3 1 17.89 35.92 25.13 o 9 -3 1 46.68 82.13 31.58 o 10 -3 1 117.67 218.77 53.22 o 11 -3 1 10.62 -15.72 45.36 o -10 -2 1 34.62 64.29 56.73 o -9 -2 1 190.12 201.31 60.35 o -8 -2 1 180.39 185.20 33.56 o -7 -2 1 0.14 -22.11 22.11 o -6 -2 1 1884.31 1976.97 88.68 o -5 -2 1 970.25 905.96 34.96 o -4 -2 1 1429.94 1311.11 30.22 o -3 -2 1 224.34 244.11 17.38 o -2 -2 1 427.14 341.08 20.41 o -1 -2 1 5345.55 4692.65 38.82 o 0 -2 1 1865.67 1671.04 87.31 o 1 -2 1 1735.34 1432.33 19.18 o 2 -2 1 2314.14 2027.01 110.46 o 3 -2 1 457.08 405.08 16.77 o 4 -2 1 418.38 322.85 20.97 o 5 -2 1 106.67 80.72 20.24 o 6 -2 1 2.13 3.31 21.74 o 7 -2 1 414.53 421.49 30.06 o 8 -2 1 541.90 509.94 33.34 o 9 -2 1 43.98 73.72 29.34 o 10 -2 1 172.79 208.12 38.35 o 11 -2 1 33.10 14.25 54.46 o -10 -1 1 60.39 54.93 54.79 o -9 -1 1 108.69 176.15 36.81 o -8 -1 1 11.41 17.19 25.61 o -7 -1 1 589.15 630.27 34.51 o -6 -1 1 412.68 410.81 22.64 o -5 -1 1 157.25 170.76 20.62 o -4 -1 1 263.09 288.70 25.86 o -3 -1 1 61.20 31.31 14.38 o -2 -1 1 3253.52 3126.29 42.22 o -1 -1 1 6219.88 5988.78 56.07 o 0 -1 1 5142.15 5326.63 55.53 o 1 -1 1 6239.72 6080.16 86.84 o 2 -1 1 15335.92 14967.81 82.83 o 3 -1 1 1588.48 1726.37 27.02 o 4 -1 1 1539.15 1459.45 29.21 o 5 -1 1 1531.16 1340.56 86.34 o 6 -1 1 1163.08 1166.29 35.74 o 7 -1 1 42.10 97.96 24.42 o 8 -1 1 411.69 433.23 32.20 o 9 -1 1 257.35 264.50 40.64 o 10 -1 1 4.72 12.64 44.56 o 11 -1 1 26.91 35.26 52.19 o -11 0 1 1.61 -49.44 49.44 o -10 0 1 1.51 0.47 45.16 o -9 0 1 57.86 33.95 41.05 o -8 0 1 115.19 131.59 29.22 o -7 0 1 713.73 682.10 33.09 o -6 0 1 151.36 157.13 20.78 o -5 0 1 448.83 430.88 23.31 o -4 0 1 542.36 446.12 19.78 o -3 0 1 199.57 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