Acta Cryst. (2005). E61, m2419-m2420  [ doi:10.1107/S1600536805034471 ]

Decacarbonyl-1³C,2³C,3⁴C-(-pentafluorophenylhydrazine-1N:2N')-triangulo-triosmium: a hydrazino-edge-bridged triangular triosmium cluster

B.-W. Sun, M.-S. Zhang, G.-Y. Yang, S. G. Ang and H. G. Ang

Online 31 October 2005

Key indicators

• Single-crystal X-ray study
• T = 285 K
• Mean (C-C) = 0.013 Å
• R factor = 0.040
• wR factor = 0.112
• Data-to-parameter ratio = 19.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Os1    -   N2      ..       5.25 su    
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         13       
PLAT431_ALERT_2_C Short Inter HL..A Contact  F2     ..  O7      ..       2.97 Ang.  
PLAT431_ALERT_2_C Short Inter HL..A Contact  F3     ..  O2      ..       2.91 Ang.  
PLAT431_ALERT_2_C Short Inter HL..A Contact  F3     ..  O8      ..       2.92 Ang.  
PLAT432_ALERT_2_C Short Inter X...Y Contact  O5     ..  C13     ..       3.01 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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