# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_F_calc_maximum 313.12 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.8303 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.5492 _cell_length_b 8.2515 _cell_length_c 19.2229 _cell_angle_alpha 90.000 _cell_angle_beta 96.521 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 98044.04 490.85 16448.83 o 4 0 0 6832.91 7879.14 123.75 o 6 0 0 8474.53 8729.69 151.67 o 8 0 0 13433.69 13766.49 233.38 o 10 0 0 7283.42 7627.83 124.27 o 12 0 0 3453.74 3640.61 83.46 o 14 0 0 3081.42 2985.97 124.10 o 16 0 0 936.55 928.84 85.51 o 1 1 0 51.44 15.34 5.49 o 2 1 0 108.02 80.63 12.16 o 3 1 0 3691.35 3670.22 40.67 o 4 1 0 8281.64 8868.64 102.21 o 5 1 0 16.22 15.81 2.25 o 6 1 0 87.83 62.88 4.03 o 7 1 0 528.83 593.08 9.31 o 8 1 0 4643.77 4456.19 67.07 o 9 1 0 311.33 302.07 6.35 o 10 1 0 3797.35 3938.87 48.31 o 11 1 0 3.44 13.39 3.87 o 12 1 0 229.27 228.87 9.03 o 13 1 0 348.74 335.87 13.17 o 14 1 0 2000.34 2040.62 38.02 o 15 1 0 12.68 9.30 13.21 o 16 1 0 4101.25 4546.18 175.66 o 0 2 0 2436.49 2239.09 42.31 o 1 2 0 11846.95 13533.57 189.90 o 2 2 0 165.64 127.10 10.23 o 3 2 0 3746.63 3956.44 54.35 o 4 2 0 10499.80 10228.90 132.49 o 5 2 0 72.93 80.89 3.44 o 6 2 0 23413.53 25537.70 269.35 o 7 2 0 337.75 356.32 7.47 o 8 2 0 8423.10 8307.43 111.18 o 9 2 0 3470.21 3358.53 52.69 o 10 2 0 2033.16 1938.39 32.65 o 11 2 0 2071.67 2052.32 39.83 o 12 2 0 416.55 487.95 20.17 o 13 2 0 11.40 23.59 9.28 o 14 2 0 966.19 1036.84 27.83 o 15 2 0 140.26 164.94 18.48 o 1 3 0 7856.31 8182.54 111.53 o 2 3 0 4542.61 4853.82 97.56 o 3 3 0 12000.73 12943.75 170.44 o 4 3 0 1109.96 1076.33 17.51 o 5 3 0 326.35 257.40 12.19 o 6 3 0 20.14 40.19 4.19 o 7 3 0 5365.55 5500.34 74.77 o 8 3 0 2134.28 1955.56 27.46 o 9 3 0 47.18 51.51 4.99 o 10 3 0 4016.40 3893.54 74.29 o 11 3 0 6.40 28.93 7.32 o 12 3 0 1068.91 1141.23 52.88 o 13 3 0 1298.65 1243.42 42.51 o 14 3 0 1154.18 1224.84 35.59 o 15 3 0 381.72 379.45 23.95 o 0 4 0 9989.03 10275.72 186.70 o 1 4 0 1242.30 1196.32 21.74 o 2 4 0 14618.51 15492.85 202.75 o 3 4 0 1712.08 1520.16 28.78 o 4 4 0 17050.51 17582.70 264.84 o 5 4 0 163.43 133.91 7.02 o 6 4 0 8864.42 8732.71 131.05 o 7 4 0 743.94 739.54 18.11 o 8 4 0 2854.03 2984.21 58.11 o 9 4 0 1289.37 1262.91 30.41 o 10 4 0 4194.76 4069.87 73.67 o 11 4 0 195.48 222.86 10.46 o 12 4 0 3082.03 2978.79 130.55 o 13 4 0 23.07 13.48 14.73 o 14 4 0 790.69 732.80 50.67 o 1 5 0 185.26 210.56 8.80 o 2 5 0 11.98 12.72 7.73 o 3 5 0 509.10 555.77 16.50 o 4 5 0 1677.38 1539.32 27.59 o 5 5 0 1674.56 1646.16 43.47 o 6 5 0 867.98 771.17 18.22 o 7 5 0 9.60 6.76 4.92 o 8 5 0 122.56 127.94 8.65 o 9 5 0 733.34 640.79 18.38 o 10 5 0 646.72 672.74 18.36 o 11 5 0 88.93 116.44 33.57 o 12 5 0 2649.21 2620.16 81.85 o 13 5 0 538.43 472.67 56.94 o 14 5 0 1223.85 1002.05 44.83 o 0 6 0 85.87 11.52 46.45 o 1 6 0 1122.32 1150.65 61.67 o 2 6 0 3634.99 3412.22 65.93 o 3 6 0 4130.80 4090.11 110.97 o 4 6 0 11991.85 11762.07 339.94 o 5 6 0 2249.30 2044.92 92.05 o 6 6 0 2355.17 2193.09 49.27 o 7 6 0 747.20 793.08 36.02 o 8 6 0 663.65 611.88 32.76 o 9 6 0 327.03 290.99 26.01 o 10 6 0 2271.02 2288.38 65.00 o 11 6 0 1390.75 1506.53 55.21 o 12 6 0 643.17 616.99 41.86 o 1 7 0 1304.20 1370.06 110.94 o 2 7 0 31.26 18.83 18.97 o 3 7 0 1640.69 1735.66 85.40 o 4 7 0 317.13 285.21 19.90 o 5 7 0 12.68 24.55 17.04 o 6 7 0 293.69 251.84 18.18 o 7 7 0 36.05 68.01 22.40 o 8 7 0 764.38 696.27 26.34 o 9 7 0 409.84 399.21 23.92 o 10 7 0 315.53 314.82 25.37 o 11 7 0 212.01 214.05 59.87 o 0 8 0 2289.21 2492.51 121.74 o 1 8 0 1069.42 1145.23 70.15 o 2 8 0 2591.11 2825.93 98.93 o 3 8 0 1420.50 1481.01 56.30 o 4 8 0 3052.50 3263.27 138.19 o 5 8 0 1465.54 1641.61 78.13 o 6 8 0 526.98 517.70 37.53 o 7 8 0 615.97 704.78 43.18 o 8 8 0 404.55 376.69 33.37 o 9 8 0 251.98 272.07 29.36 o 1 9 0 66.79 86.89 28.06 o 2 9 0 51.91 36.08 28.01 o 3 9 0 135.52 195.73 57.12 o 4 9 0 117.86 172.92 31.66 o 5 9 0 52.46 53.62 25.27 o 6 9 0 527.81 440.08 36.76 o -15 0 1 1466.24 1530.59 59.31 o -13 0 1 889.33 1051.32 42.58 o -11 0 1 3506.93 3408.33 190.49 o -9 0 1 3286.24 3197.38 67.72 o -7 0 1 46.39 33.33 5.13 o -5 0 1 2123.27 2401.96 198.06 o -3 0 1 3671.20 3723.80 119.94 o 3 0 1 10281.14 11122.63 387.31 o 5 0 1 3872.63 3622.39 53.61 o 7 0 1 15499.81 16409.09 275.88 o 9 0 1 720.83 646.28 17.49 o 11 0 1 21.47 34.43 4.37 o 13 0 1 4107.49 4265.32 123.21 o 15 0 1 6234.34 7213.67 278.80 o -16 1 1 4.65 8.95 21.20 o -15 1 1 1818.69 1874.37 54.43 o -14 1 1 223.09 202.19 9.95 o -13 1 1 1217.32 1183.02 27.82 o -12 1 1 71.38 68.12 6.42 o -11 1 1 2404.22 2371.79 89.83 o -10 1 1 743.13 742.03 11.90 o -9 1 1 14193.00 15086.53 173.09 o -8 1 1 7.74 8.57 3.31 o -7 1 1 8707.82 8352.96 92.07 o -6 1 1 544.26 604.99 8.75 o -5 1 1 3355.45 3139.00 34.40 o -4 1 1 268.33 290.06 4.58 o -3 1 1 40643.58 53106.25 587.36 o -2 1 1 1437.51 1231.15 82.59 o -1 1 1 30417.95 12215.15 2283.88 o 0 1 1 904.55 67.42 45.29 o 1 1 1 36512.02 20100.71 3377.76 o 2 1 1 2447.84 2218.41 144.11 o 3 1 1 22916.07 26639.65 330.11 o 4 1 1 5246.80 5443.13 60.08 o 5 1 1 11207.35 11631.56 136.27 o 6 1 1 1050.73 1132.61 16.19 o 7 1 1 13968.94 14269.29 166.72 o 8 1 1 2090.67 2108.44 30.36 o 9 1 1 2856.94 2885.45 36.78 o 10 1 1 1330.29 1362.05 23.33 o 11 1 1 560.49 552.11 11.05 o 12 1 1 17.88 15.06 4.52 o 13 1 1 1509.00 1517.93 47.10 o 14 1 1 410.30 432.71 17.19 o 15 1 1 662.67 668.90 23.28 o 16 1 1 8.14 16.74 16.34 o -15 2 1 274.76 348.35 72.09 o -14 2 1 183.30 147.86 20.78 o -13 2 1 225.70 241.06 16.66 o -12 2 1 17.29 18.61 7.38 o -11 2 1 363.15 350.31 8.67 o -10 2 1 34.45 32.28 4.26 o -9 2 1 574.02 536.86 19.00 o -8 2 1 1284.91 1260.40 27.59 o -7 2 1 3989.07 4244.05 48.71 o -6 2 1 1505.18 1308.83 18.11 o -5 2 1 414.86 406.23 8.15 o -4 2 1 5858.43 5975.34 75.22 o -3 2 1 2983.75 3066.36 42.92 o -2 2 1 16440.77 19053.86 260.49 o -1 2 1 106.13 117.23 4.27 o 0 2 1 10604.80 11747.45 164.07 o 1 2 1 118.10 98.82 5.56 o 2 2 1 43592.65 59787.24 804.16 o 3 2 1 14.23 30.29 2.86 o 4 2 1 5158.97 5354.26 64.21 o 5 2 1 9051.54 9481.35 115.29 o 6 2 1 4700.62 4929.92 57.51 o 7 2 1 18315.08 20083.06 276.30 o 8 2 1 643.46 655.76 18.64 o 9 2 1 4922.02 4902.41 63.49 o 10 2 1 165.09 158.16 6.43 o 11 2 1 1673.82 1697.03 64.97 o 12 2 1 112.79 103.59 11.81 o 13 2 1 1194.82 1336.60 61.40 o 14 2 1 278.68 287.67 21.29 o 15 2 1 1761.28 1827.96 53.67 o -15 3 1 760.90 777.72 53.52 o -14 3 1 347.71 333.53 25.37 o -13 3 1 1541.18 1527.19 54.83 o -12 3 1 434.40 460.37 24.61 o -11 3 1 3907.83 4018.99 72.91 o -10 3 1 693.03 673.70 17.26 o -9 3 1 8352.83 8438.52 110.81 o -8 3 1 112.22 110.05 5.16 o -7 3 1 12054.35 12143.84 141.56 o -6 3 1 4091.25 4316.29 52.70 o -5 3 1 8375.88 8105.52 99.24 o -4 3 1 3936.46 3932.88 54.62 o -3 3 1 22577.64 24983.09 350.81 o -2 3 1 55.58 55.24 5.16 o -1 3 1 16019.56 17019.40 211.19 o 0 3 1 4139.76 4303.04 63.66 o 1 3 1 3285.18 2931.11 47.46 o 2 3 1 5516.99 5752.80 78.47 o 3 3 1 12311.00 12598.88 179.36 o 4 3 1 2285.72 2563.51 43.93 o 5 3 1 9450.47 9574.88 121.65 o 6 3 1 807.77 890.91 21.97 o 7 3 1 7907.70 7930.26 100.72 o 8 3 1 368.64 344.28 11.84 o 9 3 1 1844.75 1798.48 34.61 o 10 3 1 1311.35 1323.30 28.59 o 11 3 1 1048.40 1036.74 31.49 o 12 3 1 3.77 5.56 8.82 o 13 3 1 890.43 871.76 28.32 o 14 3 1 111.01 107.53 12.84 o 15 3 1 4.60 22.71 12.79 o -14 4 1 68.75 80.37 16.76 o -13 4 1 1619.90 1639.44 56.64 o -12 4 1 50.69 27.77 9.74 o -11 4 1 1470.92 1453.91 46.61 o -10 4 1 214.34 220.00 10.84 o -9 4 1 84.40 104.10 8.20 o -8 4 1 205.44 198.75 8.39 o -7 4 1 212.53 218.80 8.83 o -6 4 1 1838.56 1801.99 27.76 o -5 4 1 839.03 804.17 30.61 o -4 4 1 359.62 426.08 10.34 o -3 4 1 48.67 52.63 4.57 o -2 4 1 5955.54 6078.20 84.86 o -1 4 1 2516.82 2611.65 46.28 o 0 4 1 837.55 892.65 21.22 o 1 4 1 9074.80 9372.32 141.69 o 2 4 1 1468.01 1541.07 25.93 o 3 4 1 1720.56 1535.83 28.80 o 4 4 1 130.98 129.22 9.94 o 5 4 1 412.11 322.60 14.50 o 6 4 1 366.45 346.93 9.81 o 7 4 1 240.15 232.73 6.65 o 8 4 1 19.32 20.55 5.01 o 9 4 1 1185.82 1133.97 22.40 o 10 4 1 531.02 523.09 16.88 o 11 4 1 8846.08 9149.40 146.54 o 12 4 1 1145.84 1185.98 37.92 o 13 4 1 3117.03 2958.09 88.34 o 14 4 1 174.04 203.36 33.54 o -14 5 1 171.20 157.56 28.60 o -13 5 1 3262.05 3163.72 178.07 o -12 5 1 2051.40 2079.28 69.74 o -11 5 1 2756.87 2635.13 159.83 o -10 5 1 811.17 841.85 34.82 o -9 5 1 186.11 201.77 16.87 o -8 5 1 8.08 12.92 5.28 o -7 5 1 5267.22 5086.50 82.11 o -6 5 1 1364.20 1284.46 23.40 o -5 5 1 26220.90 27699.63 452.92 o -4 5 1 1423.63 1277.02 36.46 o -3 5 1 13460.94 13508.08 172.63 o -2 5 1 812.22 752.80 30.49 o -1 5 1 5.27 18.19 6.67 o 0 5 1 1628.61 1506.29 28.74 o 1 5 1 2569.63 2326.32 60.06 o 2 5 1 2380.74 2142.59 40.41 o 3 5 1 19456.62 20123.08 267.77 o 4 5 1 955.22 851.94 17.41 o 5 5 1 6124.94 6101.75 119.43 o 6 5 1 205.37 172.45 10.41 o 7 5 1 1378.09 1328.13 43.43 o 8 5 1 580.75 599.55 14.18 o 9 5 1 1594.44 1629.06 43.08 o 10 5 1 526.61 480.53 15.34 o 11 5 1 2195.25 2215.22 55.27 o 12 5 1 137.48 137.75 38.10 o 13 5 1 906.78 845.07 35.96 o -12 6 1 13.39 -22.14 20.68 o -11 6 1 1179.03 1052.37 102.02 o -10 6 1 9.17 12.00 13.78 o -9 6 1 21.65 19.00 8.87 o -8 6 1 210.59 175.67 13.48 o -7 6 1 1.20 6.91 7.27 o -6 6 1 1.17 15.68 9.07 o -5 6 1 115.77 125.18 19.13 o -4 6 1 166.47 175.68 10.70 o -3 6 1 330.68 341.12 31.89 o -2 6 1 0.04 10.67 9.63 o -1 6 1 23.25 21.63 16.60 o 0 6 1 0.27 3.68 16.29 o 1 6 1 22.37 2.04 8.89 o 2 6 1 797.26 774.24 44.46 o 3 6 1 2253.43 2076.68 39.71 o 4 6 1 1163.23 1096.03 56.82 o 5 6 1 3262.86 3271.80 116.83 o 6 6 1 694.16 658.05 30.48 o 7 6 1 839.21 810.71 48.32 o 8 6 1 669.88 634.73 26.79 o 9 6 1 1750.57 1876.03 59.57 o 10 6 1 522.12 541.76 32.24 o 11 6 1 3033.42 3106.48 104.16 o 12 6 1 59.38 29.86 22.25 o -11 7 1 1417.75 1280.63 152.18 o -10 7 1 228.92 213.73 31.40 o -9 7 1 1343.78 1412.62 51.90 o -8 7 1 2739.79 2819.29 78.66 o -7 7 1 2183.58 2178.32 65.72 o -6 7 1 3433.96 3474.75 118.34 o -5 7 1 3446.52 3528.74 109.58 o -4 7 1 1936.75 2216.24 201.28 o -3 7 1 3953.20 4202.62 115.59 o -2 7 1 1922.27 2095.16 69.25 o -1 7 1 1748.94 1750.67 57.59 o 0 7 1 529.88 482.49 27.55 o 1 7 1 3788.65 3871.68 113.66 o 2 7 1 323.33 324.02 19.40 o 3 7 1 4721.70 4825.46 140.59 o 4 7 1 3345.33 3532.23 89.15 o 5 7 1 1382.82 1376.54 43.15 o 6 7 1 2720.20 2804.32 89.30 o 7 7 1 125.45 106.57 17.54 o 8 7 1 215.08 171.39 15.67 o 9 7 1 843.14 886.48 45.68 o 10 7 1 78.72 81.63 21.04 o 11 7 1 1169.86 1144.48 55.54 o -9 8 1 21.53 33.98 39.73 o -8 8 1 26.38 14.52 37.34 o -7 8 1 1289.00 1244.52 60.03 o -6 8 1 570.62 453.18 26.46 o -5 8 1 445.74 342.68 35.88 o -4 8 1 0.31 10.17 28.03 o -3 8 1 81.87 100.61 24.64 o -2 8 1 800.14 821.69 42.68 o -1 8 1 17.97 11.32 27.25 o 0 8 1 311.48 316.25 26.72 o 1 8 1 25.18 18.40 22.26 o 2 8 1 2563.82 2640.46 92.05 o 3 8 1 1131.04 1140.20 76.89 o 4 8 1 139.48 143.92 26.30 o 5 8 1 2000.63 1943.57 61.51 o 6 8 1 82.31 83.46 29.31 o 7 8 1 307.69 263.07 27.20 o 8 8 1 1269.85 1319.44 63.56 o 9 8 1 247.24 250.05 38.46 o -6 9 1 1276.64 1443.70 78.03 o -5 9 1 270.10 258.85 33.47 o -4 9 1 1108.19 1131.68 56.97 o -3 9 1 1751.64 1755.72 105.48 o -2 9 1 1684.88 1798.92 82.48 o -1 9 1 3816.43 3768.29 150.36 o 0 9 1 2272.49 2148.33 182.26 o 1 9 1 3147.22 3161.82 148.37 o 2 9 1 1267.11 1226.24 124.13 o 3 9 1 1290.11 1439.81 94.75 o 4 9 1 1255.37 1178.71 58.09 o 5 9 1 456.71 424.60 37.73 o 6 9 1 1191.52 1057.13 75.35 o -16 0 2 2630.59 2833.47 154.94 o -14 0 2 422.68 460.24 22.55 o -12 0 2 2486.93 2585.25 85.16 o -10 0 2 14403.00 15061.33 246.81 o -8 0 2 7848.58 7521.42 490.83 o -6 0 2 33.04 76.95 5.91 o -4 0 2 1817.21 1456.18 37.05 o -2 0 2 34108.13 20753.47 4033.34 o 0 0 2 68814.12 -2.31 1.54 o 2 0 2 10858.63 9734.96 1111.70 o 4 0 2 5076.86 4789.85 104.31 o 6 0 2 16694.96 18361.41 314.14 o 8 0 2 4461.46 4832.87 90.29 o 10 0 2 314.80 337.21 18.22 o 12 0 2 16.65 19.99 6.85 o 14 0 2 86.26 94.14 13.68 o -16 1 2 2218.63 2269.78 103.66 o -15 1 2 14.75 4.34 11.08 o -14 1 2 49.37 74.21 12.69 o -13 1 2 649.27 586.20 15.90 o -12 1 2 220.99 193.54 11.90 o -11 1 2 1967.54 1931.59 31.82 o -10 1 2 478.52 433.81 40.55 o -9 1 2 329.75 323.73 23.59 o -8 1 2 131.99 139.23 12.54 o -7 1 2 1801.71 1780.57 84.65 o -6 1 2 759.26 797.49 16.25 o -5 1 2 150.77 152.20 5.07 o -4 1 2 13.47 24.45 2.83 o -3 1 2 151.07 157.13 2.99 o -2 1 2 3157.84 3055.79 117.89 o -1 1 2 3184.38 2023.62 302.91 o 0 1 2 10904.70 2633.71 948.21 o 1 1 2 17837.50 11799.65 1377.54 o 2 1 2 5850.16 5780.67 85.60 o 3 1 2 7665.37 8379.27 116.58 o 4 1 2 15740.69 17188.65 201.35 o 5 1 2 6247.21 6687.41 82.02 o 6 1 2 9938.87 9849.95 110.13 o 7 1 2 191.11 244.02 7.30 o 8 1 2 7048.97 6672.81 101.12 o 9 1 2 211.47 202.67 7.78 o 10 1 2 1560.99 1620.28 23.85 o 11 1 2 217.61 233.00 6.67 o 12 1 2 1413.67 1462.05 25.35 o 13 1 2 462.68 446.17 19.81 o 14 1 2 6083.61 6314.92 119.24 o 15 1 2 38.15 28.51 8.79 o -15 2 2 147.50 133.42 16.03 o -14 2 2 2991.59 2943.75 92.20 o -13 2 2 118.28 105.56 14.26 o -12 2 2 5292.26 5329.57 101.12 o -11 2 2 80.33 71.53 5.23 o -10 2 2 7675.12 7579.41 96.46 o -9 2 2 6.91 14.21 2.81 o -8 2 2 10032.96 9725.64 127.42 o -7 2 2 324.18 298.26 10.72 o -6 2 2 21418.82 23400.47 260.77 o -5 2 2 1576.79 1640.67 21.01 o -4 2 2 8252.11 7837.74 85.31 o -3 2 2 45.28 50.18 2.96 o -2 2 2 12537.90 13089.97 157.57 o -1 2 2 7893.90 8756.98 116.04 o 0 2 2 48178.39 66511.45 1007.56 o 1 2 2 1765.45 1864.11 29.38 o 2 2 2 1906.59 1789.41 30.33 o 3 2 2 34.55 43.63 14.97 o 4 2 2 2044.62 1841.56 29.78 o 5 2 2 2763.94 2695.83 37.02 o 6 2 2 8621.69 8577.53 135.22 o 7 2 2 1953.47 2034.70 26.40 o 8 2 2 2645.75 2473.80 33.32 o 9 2 2 3113.96 3120.48 42.98 o 10 2 2 670.31 634.59 11.30 o 11 2 2 241.64 256.22 12.24 o 12 2 2 359.07 377.63 18.89 o 13 2 2 1068.92 1045.16 27.45 o 14 2 2 269.88 244.90 17.38 o 15 2 2 186.26 176.25 24.91 o -15 3 2 1093.40 1104.69 48.90 o -14 3 2 457.83 400.11 24.93 o -13 3 2 131.33 109.02 23.56 o -12 3 2 996.19 930.16 24.34 o -11 3 2 535.69 524.52 21.03 o -10 3 2 936.59 876.32 20.42 o -9 3 2 1214.62 1222.08 36.31 o -8 3 2 291.68 337.84 9.18 o -7 3 2 7606.21 8032.76 93.48 o -6 3 2 1072.07 1029.67 19.13 o -5 3 2 2087.17 2119.54 27.02 o -4 3 2 298.05 357.83 9.66 o -3 3 2 15085.80 16294.98 205.42 o -2 3 2 2226.99 2082.66 33.19 o -1 3 2 150.06 183.11 8.35 o 0 3 2 618.92 505.56 14.96 o 1 3 2 10420.22 11374.38 182.69 o 2 3 2 4231.48 4003.35 65.04 o 3 3 2 1431.59 1653.83 35.72 o 4 3 2 5002.21 4790.35 74.69 o 5 3 2 137.83 92.32 7.09 o 6 3 2 1138.98 969.05 20.09 o 7 3 2 536.15 566.11 14.22 o 8 3 2 6116.37 5999.16 77.56 o 9 3 2 349.18 365.72 9.32 o 10 3 2 5823.49 5997.16 82.60 o 11 3 2 237.92 229.45 10.64 o 12 3 2 3301.83 3409.72 81.15 o 13 3 2 219.35 208.50 13.55 o 14 3 2 1257.64 1361.85 81.99 o 15 3 2 174.03 208.38 21.02 o -14 4 2 2661.01 2835.35 88.82 o -13 4 2 721.96 696.16 30.35 o -12 4 2 1952.73 2047.01 52.97 o -11 4 2 2637.82 2650.33 59.94 o -10 4 2 2704.92 2708.91 65.25 o -9 4 2 1047.00 1048.41 20.69 o -8 4 2 4413.10 4555.94 55.03 o -7 4 2 16.12 25.31 4.39 o -6 4 2 14672.20 14903.85 190.27 o -5 4 2 914.93 797.26 14.45 o -4 4 2 12684.25 12358.95 170.95 o -3 4 2 1424.31 1378.31 23.11 o -2 4 2 9107.54 9695.58 130.25 o -1 4 2 1388.49 1430.37 33.50 o 0 4 2 14889.47 15796.58 242.52 o 1 4 2 4830.58 4926.95 89.28 o 2 4 2 12472.45 12705.31 174.00 o 3 4 2 1281.93 1280.06 30.00 o 4 4 2 7584.20 7588.42 146.50 o 5 4 2 402.25 450.34 11.47 o 6 4 2 109.56 79.36 5.18 o 7 4 2 1352.33 1340.20 25.90 o 8 4 2 1887.11 1769.34 29.18 o 9 4 2 4136.44 4172.19 64.82 o 10 4 2 5243.36 5157.65 103.57 o 11 4 2 15.03 21.35 7.64 o 12 4 2 646.52 661.80 46.35 o 13 4 2 270.62 269.44 19.21 o 14 4 2 85.51 99.50 17.15 o -14 5 2 1585.89 1597.56 98.80 o -13 5 2 35.33 12.78 16.71 o -12 5 2 403.33 355.92 22.29 o -11 5 2 620.23 571.47 37.35 o -10 5 2 23.37 34.58 8.04 o -9 5 2 24.51 32.58 5.98 o -8 5 2 55.59 47.33 5.53 o -7 5 2 71.99 80.54 9.53 o -6 5 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