# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_F_calc_maximum 374.73 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.6999 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.8600 _cell_length_b 7.1830 _cell_length_c 13.7930 _cell_angle_alpha 90.000 _cell_angle_beta 101.584 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 42785.68 41068.36 1568.01 o 4 0 0 53379.74 53833.83 2572.22 o 5 0 0 23229.54 23347.55 733.72 o 6 0 0 337.38 125.42 45.27 o 7 0 0 1919.00 2165.20 83.92 o 8 0 0 319.93 307.41 70.28 o 9 0 0 883.14 772.24 70.41 o 10 0 0 32.95 32.95 71.59 o 11 0 0 2291.73 2388.98 91.95 o 12 0 0 464.70 600.76 56.90 o 13 0 0 5428.17 5955.39 217.32 o 14 0 0 2664.32 2909.16 216.24 o 15 0 0 3600.23 4275.76 403.93 o 3 1 0 1606.20 2097.08 136.98 o 4 1 0 11057.32 11148.51 313.01 o 5 1 0 1310.96 1484.65 49.15 o 6 1 0 1523.94 1685.96 61.69 o 7 1 0 5363.07 5057.98 126.35 o 8 1 0 3792.27 3941.35 175.18 o 9 1 0 12457.81 12242.72 465.05 o 10 1 0 11644.17 12088.90 284.15 o 11 1 0 14707.17 15025.09 488.65 o 12 1 0 13306.30 13633.45 365.68 o 13 1 0 8866.97 9969.74 302.29 o 14 1 0 4226.63 4225.64 260.91 o 15 1 0 2052.45 2153.16 205.28 o 0 2 0 29790.95 31011.38 1626.90 o 1 2 0 107.02 230.03 21.08 o 2 2 0 9768.17 9531.08 360.40 o 3 2 0 3798.27 3936.56 242.72 o 4 2 0 1699.28 1791.91 64.39 o 5 2 0 2493.58 2341.83 71.65 o 6 2 0 94.11 81.15 24.08 o 7 2 0 116.93 79.44 36.31 o 8 2 0 233.20 144.85 29.94 o 9 2 0 381.08 391.79 48.11 o 10 2 0 1.95 69.96 52.99 o 11 2 0 668.18 586.09 60.51 o 12 2 0 5.46 22.72 95.63 o 13 2 0 1232.70 1315.99 90.81 o 14 2 0 90.65 78.77 71.67 o 1 3 0 45.87 108.13 22.10 o 2 3 0 1002.11 1230.67 81.62 o 3 3 0 4465.73 4383.91 130.95 o 4 3 0 108.22 128.46 22.52 o 5 3 0 6440.12 6295.58 180.84 o 6 3 0 2774.30 2809.91 108.72 o 7 3 0 337.77 303.32 66.37 o 8 3 0 3050.05 3251.98 90.32 o 9 3 0 958.69 946.30 110.53 o 10 3 0 4958.56 4965.91 207.47 o 11 3 0 5670.20 5813.70 271.33 o 12 3 0 5479.22 6129.05 177.82 o 13 3 0 3287.28 3511.57 1037.71 o 14 3 0 1613.72 1658.98 87.17 o 0 4 0 90517.41 84220.76 4594.03 o 1 4 0 91301.30 84804.57 3510.89 o 2 4 0 33527.10 30764.67 896.47 o 3 4 0 27673.48 25866.64 968.10 o 4 4 0 20945.54 20829.75 689.90 o 5 4 0 7260.75 6695.81 178.72 o 6 4 0 753.52 623.85 77.30 o 7 4 0 415.60 457.59 40.66 o 8 4 0 56.66 48.84 38.74 o 9 4 0 1.59 47.26 35.03 o 10 4 0 274.75 368.77 53.74 o 11 4 0 41.53 -33.33 126.10 o 12 4 0 2140.40 2504.55 101.34 o 13 4 0 1384.95 1659.68 109.08 o 1 5 0 3219.31 3356.09 113.24 o 2 5 0 6484.87 6135.99 214.27 o 3 5 0 5943.91 5989.68 156.68 o 4 5 0 1640.17 1596.62 90.07 o 5 5 0 5777.26 5885.20 151.65 o 6 5 0 197.72 315.40 119.27 o 7 5 0 349.19 495.22 92.26 o 8 5 0 8264.43 7826.37 211.28 o 9 5 0 8867.41 9140.96 218.88 o 10 5 0 12721.32 13951.13 383.69 o 11 5 0 12740.40 13251.90 329.21 o 12 5 0 12805.57 12683.93 356.77 o 13 5 0 8936.49 9340.06 332.11 o 0 6 0 11734.57 11951.85 489.70 o 1 6 0 25916.67 25371.56 706.13 o 2 6 0 8307.43 8273.60 261.11 o 3 6 0 16291.64 15877.88 548.85 o 4 6 0 5677.01 5195.80 162.98 o 5 6 0 3640.22 3368.07 118.18 o 6 6 0 712.92 722.64 67.58 o 7 6 0 117.39 109.38 43.88 o 8 6 0 369.49 386.92 60.27 o 9 6 0 18.72 67.23 69.31 o 10 6 0 136.86 49.62 88.72 o 11 6 0 4.81 -99.53 83.42 o 12 6 0 943.52 1049.59 125.46 o 1 7 0 8.95 152.85 120.13 o 2 7 0 97.10 313.00 51.12 o 3 7 0 841.72 807.21 60.93 o 4 7 0 1510.23 1541.43 80.41 o 5 7 0 81.04 249.38 135.26 o 6 7 0 501.56 598.42 72.38 o 7 7 0 14.72 -55.34 62.22 o 8 7 0 145.11 171.73 84.50 o 9 7 0 51.97 193.97 194.87 o 10 7 0 99.99 157.27 56.62 o 11 7 0 356.35 421.31 179.40 o 0 8 0 17977.57 19877.42 2808.65 o 1 8 0 10662.06 12200.51 633.92 o 2 8 0 12217.25 13389.06 680.21 o 3 8 0 5495.27 5690.72 182.46 o 4 8 0 4220.86 4064.85 179.40 o 5 8 0 822.68 839.66 77.67 o 6 8 0 30.48 6.02 92.25 o 7 8 0 152.47 89.71 80.95 o 8 8 0 370.58 391.65 127.57 o 9 8 0 248.60 165.78 109.52 o 1 9 0 628.73 696.58 80.78 o 2 9 0 1467.21 1589.29 147.40 o 3 9 0 897.71 990.09 84.43 o 4 9 0 1184.76 1024.72 95.93 o 5 9 0 115.24 261.30 74.40 o 6 9 0 86.42 26.81 63.29 o 7 9 0 1237.92 1291.45 184.77 o 0 10 0 13691.42 15113.88 890.30 o 1 10 0 11126.76 12872.74 620.20 o 2 10 0 9387.76 9770.40 343.70 o 3 10 0 6155.48 6469.93 361.10 o -15 1 1 2763.65 2864.00 224.21 o -14 1 1 4096.42 4714.90 216.77 o -13 1 1 3906.78 4237.79 144.21 o -12 1 1 3437.50 3586.18 121.06 o -11 1 1 527.41 632.37 56.77 o -10 1 1 302.13 245.06 80.64 o -9 1 1 554.55 561.34 45.37 o -8 1 1 482.38 572.99 40.33 o -7 1 1 5339.69 5604.84 140.64 o -6 1 1 11496.99 11268.48 271.66 o -5 1 1 10004.96 10032.18 256.76 o -4 1 1 5885.50 6196.67 155.51 o -3 1 1 463.78 367.78 36.65 o 2 1 1 1387.39 1747.23 84.55 o 3 1 1 137.31 199.73 13.02 o 4 1 1 862.84 696.00 34.91 o 5 1 1 11599.81 10836.47 267.48 o 6 1 1 16740.45 15370.42 362.99 o 7 1 1 17378.64 17091.54 619.82 o 8 1 1 14500.37 14245.69 312.21 o 9 1 1 14657.42 13732.88 353.62 o 10 1 1 12953.37 13286.06 324.77 o 11 1 1 10378.60 10544.70 300.83 o 12 1 1 4548.63 4575.34 160.23 o 13 1 1 1921.67 1889.27 76.01 o 14 1 1 895.73 1143.24 81.14 o -15 2 1 915.12 935.16 206.07 o -14 2 1 694.18 802.95 89.97 o -13 2 1 99.66 146.02 87.86 o -12 2 1 39.06 162.63 76.85 o -11 2 1 201.44 269.74 56.37 o -10 2 1 483.87 657.95 329.73 o -9 2 1 3018.33 2771.91 155.33 o -8 2 1 4862.24 4990.92 139.97 o -7 2 1 12975.91 12032.35 266.81 o -6 2 1 42440.55 40299.80 998.19 o -5 2 1 66571.73 63637.75 2359.11 o -4 2 1 100832.21 102819.14 2833.35 o -3 2 1 47900.09 40755.68 1228.79 o -2 2 1 75218.93 63084.63 2167.86 o -1 2 1 126896.20 122985.60 3618.98 o 0 2 1 80837.05 81083.64 2472.08 o 1 2 1 25236.44 23399.49 1174.57 o 2 2 1 2667.45 1610.03 65.22 o 3 2 1 864.03 698.45 71.96 o 4 2 1 2172.56 2464.33 87.73 o 5 2 1 204.63 263.46 26.98 o 6 2 1 3480.16 3646.84 135.47 o 7 2 1 2536.86 2488.73 79.99 o 8 2 1 482.39 544.39 40.55 o 9 2 1 1192.81 1067.63 83.79 o 10 2 1 6186.50 6057.25 156.10 o 11 2 1 2973.19 3021.74 107.51 o 12 2 1 4702.04 4713.06 156.42 o 13 2 1 2926.03 3003.87 122.09 o 14 2 1 1607.04 1500.14 131.23 o -14 3 1 6503.65 6645.13 249.04 o -13 3 1 6591.96 6742.17 230.55 o -12 3 1 4857.83 4952.51 144.48 o -11 3 1 917.38 1015.53 70.66 o -10 3 1 553.91 646.93 82.38 o -9 3 1 329.76 301.93 34.03 o -8 3 1 115.25 162.20 33.85 o -7 3 1 3533.99 3708.62 131.80 o -6 3 1 6446.14 5942.95 141.21 o -5 3 1 2736.18 2654.96 68.44 o -4 3 1 835.66 942.65 58.15 o -3 3 1 928.35 922.47 54.91 o -2 3 1 305.19 309.93 47.47 o -1 3 1 492.45 575.69 31.86 o 0 3 1 487.59 508.38 46.73 o 1 3 1 881.19 886.87 53.90 o 2 3 1 799.43 730.61 34.24 o 3 3 1 1830.27 1794.94 78.22 o 4 3 1 6176.05 5614.87 184.80 o 5 3 1 11336.27 9705.67 317.66 o 6 3 1 27176.30 24835.64 860.41 o 7 3 1 27780.17 27125.95 708.38 o 8 3 1 35530.09 34367.93 1168.31 o 9 3 1 28321.00 27225.77 608.20 o 10 3 1 22052.83 23526.21 639.11 o 11 3 1 15870.99 15724.55 409.16 o 12 3 1 6655.74 6614.16 176.60 o 13 3 1 3206.34 3313.16 121.60 o 14 3 1 1043.25 1083.10 148.64 o -14 4 1 240.23 342.11 77.37 o -13 4 1 12.34 63.30 53.71 o -12 4 1 35.61 94.72 56.90 o -11 4 1 2.85 20.90 35.63 o -10 4 1 153.27 119.60 53.76 o -9 4 1 1305.17 1199.38 96.45 o -8 4 1 49.78 48.57 32.18 o -7 4 1 1649.21 1469.93 122.09 o -6 4 1 1071.54 974.23 49.49 o -5 4 1 8104.93 7399.24 335.25 o -4 4 1 11022.00 10705.35 316.30 o -3 4 1 10960.19 10343.92 232.38 o -2 4 1 6692.54 6204.83 152.09 o -1 4 1 13347.11 12550.56 657.98 o 0 4 1 4658.34 4607.74 164.43 o 1 4 1 4364.52 3813.54 138.38 o 2 4 1 1443.85 1272.92 69.95 o 3 4 1 103.71 98.94 28.44 o 4 4 1 92.68 175.35 42.28 o 5 4 1 32.53 57.57 31.45 o 6 4 1 8.85 140.85 52.73 o 7 4 1 1.37 -31.92 43.53 o 8 4 1 89.27 136.71 96.18 o 9 4 1 112.58 213.17 47.03 o 10 4 1 54.54 103.99 87.10 o 11 4 1 2.95 -26.84 54.09 o 12 4 1 222.28 166.12 61.33 o 13 4 1 188.29 291.19 232.22 o -13 5 1 940.00 976.19 89.51 o -12 5 1 656.55 720.97 60.15 o -11 5 1 434.02 312.37 46.11 o -10 5 1 1.24 43.65 36.99 o -9 5 1 18.30 68.63 55.31 o -8 5 1 731.67 714.07 71.66 o -7 5 1 908.18 833.58 64.15 o -6 5 1 1293.74 1239.66 83.91 o -5 5 1 2044.46 1956.13 90.70 o -4 5 1 539.93 537.00 57.38 o -3 5 1 17.14 21.50 23.33 o -2 5 1 1530.38 1486.52 60.82 o -1 5 1 3338.44 3368.08 109.60 o 0 5 1 1880.37 2024.37 91.72 o 1 5 1 901.77 892.73 57.26 o 2 5 1 1733.65 1622.35 97.31 o 3 5 1 46.61 20.96 67.11 o 4 5 1 37.43 29.13 40.80 o 5 5 1 4278.68 3948.91 166.20 o 6 5 1 1978.09 1822.63 102.54 o 7 5 1 4326.25 3994.99 129.19 o 8 5 1 1215.47 1201.43 81.51 o 9 5 1 1653.84 1532.83 54.14 o 10 5 1 1814.58 1613.49 112.27 o 11 5 1 601.78 573.92 80.05 o 12 5 1 350.57 337.40 71.66 o 13 5 1 11.45 115.36 634.43 o -12 6 1 138.64 153.27 72.80 o -11 6 1 115.11 301.90 156.87 o -10 6 1 3.74 -42.11 28.33 o -9 6 1 114.12 97.12 54.51 o -8 6 1 1998.98 2092.89 117.82 o -7 6 1 3995.48 4005.69 153.28 o -6 6 1 17969.87 17635.99 501.94 o -5 6 1 29139.52 28361.28 707.52 o -4 6 1 47647.03 48229.38 1325.34 o -3 6 1 41904.85 41993.92 1550.85 o -2 6 1 51624.12 49954.97 1404.87 o -1 6 1 34149.15 34719.87 1024.40 o 0 6 1 28210.37 28126.42 698.09 o 1 6 1 5804.81 5680.77 265.53 o 2 6 1 1538.64 1488.44 65.62 o 3 6 1 7.85 -1.47 35.90 o 4 6 1 121.23 209.42 53.93 o 5 6 1 679.80 623.12 53.10 o 6 6 1 753.06 702.66 55.48 o 7 6 1 29.75 164.59 72.78 o 8 6 1 101.94 190.70 58.82 o 9 6 1 1469.22 1401.30 75.59 o 10 6 1 1112.12 1193.68 90.94 o 11 6 1 2572.77 2569.30 122.72 o 12 6 1 1690.57 1740.07 93.02 o -11 7 1 1690.51 1744.41 105.52 o -10 7 1 6.71 -25.73 1861.19 o -9 7 1 59.65 58.82 59.64 o -8 7 1 2103.11 2353.65 245.28 o -7 7 1 2714.83 2608.69 115.00 o -6 7 1 4367.56 4371.24 176.28 o -5 7 1 2222.93 2194.09 137.23 o -4 7 1 472.85 530.93 163.12 o -3 7 1 472.39 489.68 52.38 o -2 7 1 62.31 161.34 68.98 o -1 7 1 396.78 472.47 106.82 o 0 7 1 2674.14 2799.28 177.38 o 1 7 1 1512.07 1607.75 79.90 o 2 7 1 479.95 447.99 69.12 o 3 7 1 627.41 696.28 116.92 o 4 7 1 832.70 775.07 61.05 o 5 7 1 7344.64 7152.32 240.08 o 6 7 1 10431.81 11150.34 393.35 o 7 7 1 20135.15 19984.29 648.53 o 8 7 1 21168.19 21880.69 625.18 o 9 7 1 18055.41 17780.92 860.38 o 10 7 1 15108.85 15272.16 445.22 o -9 8 1 959.79 1062.91 138.37 o -8 8 1 1850.18 1725.05 103.99 o -7 8 1 2650.69 2562.86 118.03 o -6 8 1 6433.48 6582.16 488.33 o -5 8 1 10385.31 10360.65 413.33 o -4 8 1 15531.68 14944.16 449.74 o -3 8 1 12650.75 12747.57 736.94 o -2 8 1 14441.04 14831.71 686.40 o -1 8 1 9472.37 10424.46 628.58 o 0 8 1 8645.55 9538.34 607.55 o 1 8 1 3180.21 4250.86 262.45 o 2 8 1 1910.04 1919.13 95.90 o 3 8 1 487.64 654.81 74.65 o 4 8 1 65.12 72.58 102.16 o 5 8 1 33.06 119.96 64.52 o 6 8 1 1.48 15.14 50.24 o 7 8 1 523.64 692.03 143.72 o 8 8 1 190.22 222.88 558.36 o 9 8 1 886.71 954.54 216.14 o -7 9 1 206.74 124.14 157.60 o -6 9 1 19.76 -34.08 60.10 o -5 9 1 30.11 83.02 67.26 o -4 9 1 2.85 -22.23 68.21 o -3 9 1 32.21 71.95 62.68 o -2 9 1 46.00 143.76 54.82 o -1 9 1 222.73 428.90 172.24 o 0 9 1 42.30 149.48 66.42 o 1 9 1 220.48 313.02 61.64 o 2 9 1 201.43 236.82 47.01 o 3 9 1 881.45 919.01 82.89 o 4 9 1 82.80 168.66 54.72 o 5 9 1 393.02 447.97 76.24 o 6 9 1 2.30 9.78 75.15 o 7 9 1 115.70 278.27 81.96 o -3 10 1 9170.82 9102.29 389.72 o -2 10 1 6048.43 6465.78 411.88 o -1 10 1 5541.21 6062.71 303.03 o 0 10 1 2063.77 2518.87 183.20 o 1 10 1 829.52 1014.21 90.66 o 2 10 1 23.66 243.03 109.60 o 3 10 1 198.64 257.59 90.14 o -15 0 2 116.49 262.97 104.49 o -14 0 2 153.03 435.47 7708.54 o -13 0 2 137.91 130.61 84.89 o -12 0 2 263.56 354.56 86.64 o -11 0 2 1341.13 1853.55 337.28 o -10 0 2 17205.23 17311.18 882.51 o -9 0 2 23591.78 23941.72 983.89 o -8 0 2 64454.37 61189.07 2022.95 o -7 0 2 67593.77 63884.69 4699.40 o -6 0 2 131182.97 123159.82 4023.11 o -5 0 2 140006.72 144547.45 4583.16 o -4 0 2 121448.68 122522.58 6009.40 o -3 0 2 36173.65 36239.90 1517.44 o 2 0 2 22408.11 25638.47 779.64 o 3 0 2 217.91 462.16 26.50 o 4 0 2 489.89 609.97 51.05 o 5 0 2 9.17 131.29 44.04 o 6 0 2 2813.49 2605.77 87.01 o 7 0 2 1620.55 1593.90 68.56 o 8 0 2 3289.42 3275.24 115.62 o 9 0 2 8281.83 8408.75 226.16 o 10 0 2 1171.88 1290.64 114.34 o 11 0 2 1288.01 1376.20 137.55 o 12 0 2 3.88 147.62 42.75 o 13 0 2 369.91 584.39 113.42 o 14 0 2 557.82 733.63 409.15 o -15 1 2 2168.09 2280.16 179.29 o -14 1 2 535.08 515.74 69.57 o -13 1 2 202.02 266.21 75.54 o -12 1 2 1326.79 1307.08 103.41 o -11 1 2 1292.09 1393.32 66.66 o -10 1 2 7538.04 7958.19 231.11 o -9 1 2 713.28 780.95 58.66 o -8 1 2 5762.18 5518.79 160.17 o -7 1 2 2868.26 2843.58 130.87 o -6 1 2 6.73 -6.16 31.89 o -5 1 2 386.28 380.24 38.94 o -4 1 2 15950.96 16511.25 573.38 o -3 1 2 194.92 94.59 16.25 o -2 1 2 15286.60 15721.60 417.21 o 2 1 2 7857.07 7483.53 204.00 o 3 1 2 43846.58 42740.86 1012.42 o 4 1 2 43391.72 39313.44 983.66 o 5 1 2 60510.00 58180.77 1265.86 o 6 1 2 42849.66 42047.86 883.78 o 7 1 2 22773.54 22647.07 453.76 o 8 1 2 18566.11 17234.83 470.67 o 9 1 2 6630.09 6471.36 204.30 o 10 1 2 7145.64 7095.82 196.03 o 11 1 2 141.23 189.05 74.48 o 12 1 2 260.51 327.45 46.65 o 13 1 2 94.48 213.06 49.18 o 14 1 2 274.54 304.58 114.37 o -15 2 2 128.44 175.63 68.60 o -14 2 2 4.08 -19.00 192.92 o -13 2 2 71.31 150.17 67.45 o -12 2 2 214.54 181.20 76.97 o -11 2 2 202.00 167.36 54.30 o -10 2 2 3239.92 3188.54 112.89 o -9 2 2 415.46 430.08 61.08 o -8 2 2 4910.12 4904.73 135.33 o -7 2 2 149.71 142.64 39.18 o -6 2 2 6400.26 6398.81 203.40 o -5 2 2 327.90 289.76 26.85 o -4 2 2 6462.53 6041.97 263.37 o -3 2 2 1463.28 1782.78 48.00 o -2 2 2 2835.52 2661.16 72.36 o -1 2 2 1.59 10.17 17.62 o 0 2 2 175.57 180.57 14.89 o 1 2 2 5482.45 5937.65 225.14 o 2 2 2 5599.93 6238.02 202.78 o 3 2 2 3313.61 3247.37 109.02 o 4 2 2 758.87 723.37 40.71 o 5 2 2 1520.64 1490.81 44.93 o 6 2 2 430.53 448.85 39.24 o 7 2 2 1856.46 1720.29 76.66 o 8 2 2 1.13 0.47 34.87 o 9 2 2 1472.19 1491.87 62.62 o 10 2 2 48.48 158.47 59.91 o 11 2 2 287.88 252.72 52.06 o 12 2 2 50.14 177.85 54.65 o 13 2 2 242.73 217.19 48.94 o 14 2 2 56.14 106.46 53.99 o -14 3 2 412.56 380.31 90.65 o -13 3 2 141.96 230.40 85.22 o -12 3 2 213.83 254.23 68.20 o -11 3 2 1890.98 1811.84 72.06 o -10 3 2 298.95 350.03 73.02 o -9 3 2 1989.75 2070.67 79.31 o -8 3 2 340.62 375.57 50.32 o -7 3 2 1507.15 1529.49 101.57 o -6 3 2 984.99 970.58 52.46 o -5 3 2 138.33 113.17 19.28 o -4 3 2 891.25 871.42 47.59 o -3 3 2 672.64 614.57 28.82 o -2 3 2 267.50 268.87 34.50 o -1 3 2 36.49 73.16 17.40 o 0 3 2 266.50 227.95 37.62 o 1 3 2 2084.11 1918.41 56.94 o 2 3 2 3161.41 2786.22 100.32 o 3 3 2 6751.02 6235.01 267.09 o 4 3 2 20368.77 18623.33 512.89 o 5 3 2 24868.80 25871.77 742.32 o 6 3 2 20796.14 19891.19 502.24 o 7 3 2 13765.28 13151.54 269.85 o 8 3 2 5156.71 5121.02 143.67 o 9 3 2 5572.30 5622.57 175.67 o 10 3 2 1171.98 1347.03 65.71 o 11 3 2 372.16 332.14 76.44 o 12 3 2 267.08 335.59 66.74 o 13 3 2 18.15 58.59 93.94 o 14 3 2 117.49 155.39 56.05 o -14 4 2 196.44 462.43 94.24 o -13 4 2 108.41 92.90 89.60 o -12 4 2 166.78 180.72 58.89 o -11 4 2 3025.67 2981.44 113.14 o -10 4 2 5725.34 5670.15 157.24 o -9 4 2 21271.36 21861.10 551.13 o -8 4 2 20494.36 20295.12 488.02 o -7 4 2 44138.84 42743.22 1125.45 o -6 4 2 39029.26 39194.43 1023.27 o -5 4 2 68103.67 67561.13 1910.00 o -4 4 2 26472.88 25917.76 814.82 o -3 4 2 32056.03 29730.39 718.57 o -2 4 2 8569.88 8177.58 242.00 o -1 4 2 3710.98 3542.13 101.03 o 0 4 2 472.66 447.92 41.55 o 1 4 2 7021.10 7321.04 237.98 o 2 4 2 326.89 407.75 37.44 o 3 4 2 5925.80 5707.54 172.98 o 4 4 2 351.42 329.43 46.96 o 5 4 2 592.30 599.17 49.25 o 6 4 2 2503.90 2590.12 100.48 o 7 4 2 1204.79 1129.09 71.67 o 8 4 2 7752.50 7474.58 201.21 o 9 4 2 3176.65 2868.32 115.23 o 10 4 2 4838.43 5005.34 160.36 o 11 4 2 644.35 679.35 149.78 o 12 4 2 116.26 100.21 60.84 o 13 4 2 143.72 273.43 59.96 o -13 5 2 4.10 152.77 107.24 o -12 5 2 113.86 132.99 56.93 o -11 5 2 3476.08 3555.38 117.41 o -10 5 2 3107.73 3138.27 115.18 o -9 5 2 7205.61 7112.12 332.81 o -8 5 2 4441.27 4288.15 131.29 o -7 5 2 5761.42 5865.30 230.97 o -6 5 2 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