data_CRYSTALS_cif # CIF000 _audit_creation_date 06-01-09 _audit_creation_method CRYSTALS _cell_length_a 14.048(6) _cell_angle_alpha 90 _cell_length_b 5.209(2) _cell_angle_beta 97.369(4) _cell_length_c 14.489(6) _cell_angle_gamma 90 # NOTE Fc on scale of Fo, 2.65192 # Status flags: # o - used in refinement # < - excluded by I/sigmaI cutoff # x - excluded for another reason loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 6 0 0 311.05 321.41 28.20 o 8 0 0 2673.40 2453.64 236.18 o 10 0 0 576.76 613.55 54.29 o 12 0 0 99.53 90.34 12.58 o 14 0 0 83.19 95.44 12.29 o 16 0 0 221.29 223.96 21.09 o 18 0 0 -3.44 0.01 7.05 < 1 1 0 647.90 916.47 57.79 o 3 1 0 538.70 451.83 48.78 o 4 1 0 46.36 65.71 6.60 o 6 1 0 315.19 318.46 29.37 o 7 1 0 176.06 197.50 17.46 o 8 1 0 4839.38 4705.80 453.88 o 9 1 0 24.70 16.95 6.16 o 10 1 0 58.37 87.49 8.84 o 11 1 0 330.64 340.90 32.12 o 12 1 0 19.84 11.66 7.03 o 13 1 0 25.95 24.49 7.44 o 14 1 0 0.13 1.59 6.25 < 15 1 0 24.24 25.67 7.89 o 16 1 0 18.38 17.42 7.63 o 17 1 0 -2.64 0.44 6.32 < 18 1 0 19.09 9.23 8.25 o 0 2 0 4710.22 4766.93 428.16 o 1 2 0 3521.28 3468.35 315.26 o 2 2 0 1711.49 1678.13 151.88 o 3 2 0 5193.80 5432.84 515.42 o 4 2 0 1728.38 1800.75 153.04 o 5 2 0 575.00 701.02 53.19 o 6 2 0 764.17 814.35 70.02 o 7 2 0 136.09 105.37 15.27 o 8 2 0 18.28 24.54 6.54 o 9 2 0 11.18 9.42 6.03 < 10 2 0 113.22 107.51 13.54 o 11 2 0 4.84 2.06 6.40 < 12 2 0 29.13 27.80 7.58 o 13 2 0 92.99 98.37 12.33 o 14 2 0 13.87 12.18 7.09 o 15 2 0 -1.54 10.60 6.74 < 16 2 0 6.42 7.57 7.48 < 17 2 0 1.21 2.15 7.91 < 18 2 0 -5.12 2.76 9.58 < 1 3 0 23.02 25.75 6.31 o 2 3 0 16.18 21.12 6.65 o 3 3 0 417.78 427.31 38.67 o 4 3 0 121.91 133.68 14.63 o 5 3 0 325.25 355.15 32.41 o 6 3 0 106.51 124.09 14.34 o 7 3 0 218.17 247.18 22.38 o 8 3 0 135.65 126.76 15.63 o 9 3 0 226.04 260.84 22.84 o 10 3 0 240.23 278.13 24.35 o 11 3 0 2.24 6.25 6.28 < 12 3 0 7.09 5.81 6.52 < 13 3 0 52.11 59.34 9.19 o 14 3 0 17.94 13.73 7.54 o 15 3 0 3.87 0.48 7.10 < 16 3 0 4.13 3.33 8.21 < 0 4 0 5.37 0.04 8.63 < 2 4 0 15.80 10.51 7.52 o 3 4 0 202.84 182.84 22.40 o 4 4 0 335.79 297.09 33.90 o 5 4 0 19.40 14.50 7.59 o 6 4 0 64.62 60.39 11.00 o 7 4 0 243.86 242.20 25.51 o 8 4 0 82.84 98.78 12.05 o 9 4 0 192.75 222.53 21.50 o 10 4 0 10.79 5.34 7.25 < 11 4 0 4.46 8.27 7.23 < 12 4 0 36.25 52.26 8.53 o 13 4 0 8.31 4.23 11.77 < 14 4 0 3.96 6.09 7.15 < 15 4 0 11.47 0.00 6.87 < 1 5 0 174.77 149.29 23.27 o 2 5 0 25.06 29.69 9.99 o 3 5 0 87.58 93.76 13.63 o 4 5 0 197.57 169.69 22.25 o 5 5 0 14.73 2.84 8.66 < 6 5 0 30.46 41.54 9.49 o 7 5 0 192.28 168.76 21.63 o 8 5 0 0.58 5.81 7.65 < 9 5 0 66.48 66.12 12.05 o 10 5 0 7.09 4.14 7.86 < 11 5 0 -4.08 2.15 7.46 < 12 5 0 32.12 22.12 9.31 o 2 6 0 15.37 24.76 10.97 < 3 6 0 2.14 9.46 9.71 < 4 6 0 7.31 2.20 10.64 < 5 6 0 27.05 32.86 11.65 o 6 6 0 22.67 20.73 11.32 o 7 6 0 6.35 18.13 10.33 < 8 6 0 4.79 7.65 10.72 < -17 0 1 5.29 4.24 6.40 < -15 0 1 42.29 56.35 9.12 o -13 0 1 9.05 14.51 6.26 < -11 0 1 4952.08 5121.40 451.27 o -9 0 1 158.86 184.72 16.15 o -7 0 1 842.99 771.67 75.25 o 7 0 1 16.17 17.04 4.12 o 9 0 1 1291.19 1323.59 114.86 o 11 0 1 550.67 588.46 52.18 o 13 0 1 25.98 35.67 7.63 o 15 0 1 16.17 14.82 6.62 o 17 0 1 49.81 41.15 9.20 o -18 1 1 -5.40 1.28 6.34 < -17 1 1 2.45 8.76 7.15 < -16 1 1 53.27 43.31 9.95 o -15 1 1 10.20 14.96 6.92 < -14 1 1 24.70 20.72 7.32 o -13 1 1 70.20 85.10 10.87 o -12 1 1 7.51 2.51 6.34 < -11 1 1 33.30 40.11 7.33 o -10 1 1 0.95 0.62 6.01 < -9 1 1 57.03 64.38 8.35 o -8 1 1 3258.79 3149.48 291.72 o -7 1 1 1683.30 1692.72 151.06 o -6 1 1 50.45 25.33 6.92 o -5 1 1 2901.15 2872.08 259.64 o -4 1 1 2740.08 3509.04 272.45 o -3 1 1 2557.04 2954.15 233.48 o -1 1 1 73.73 41.02 8.91 o 2 1 1 694.77 962.79 61.27 o 4 1 1 1.87 0.00 3.99 < 5 1 1 1715.87 1524.05 153.65 o 6 1 1 240.60 214.95 22.51 o 7 1 1 253.24 231.39 23.75 o 8 1 1 5230.10 5336.31 475.67 o 9 1 1 488.41 525.61 45.45 o 10 1 1 178.68 149.73 18.80 o 11 1 1 1651.64 1834.87 144.79 o 12 1 1 -0.43 0.08 5.71 < 13 1 1 85.02 83.73 11.78 o 14 1 1 -0.05 1.34 6.78 < 15 1 1 55.67 57.15 10.00 o 16 1 1 -3.17 0.01 5.63 < 17 1 1 13.48 7.41 7.18 < 18 1 1 -0.52 3.62 10.89 < -17 2 1 5.32 8.86 7.65 < -16 2 1 6.32 1.49 7.38 < -15 2 1 36.81 33.42 8.60 o -14 2 1 48.42 44.20 9.47 o -13 2 1 4.80 0.49 6.07 < -12 2 1 0.98 1.43 5.94 < -11 2 1 175.18 187.57 18.70 o -10 2 1 83.18 69.30 11.26 o -9 2 1 243.19 229.38 24.88 o -8 2 1 867.28 879.71 76.76 o -7 2 1 373.19 340.77 34.38 o -6 2 1 897.70 860.00 82.48 o -5 2 1 1087.60 1093.46 98.86 o -4 2 1 287.41 277.20 28.23 o -3 2 1 722.01 801.26 64.95 o -2 2 1 3279.11 3440.82 293.45 o -1 2 1 4598.23 5010.47 418.54 o 1 2 1 94.32 72.55 10.43 o 2 2 1 2924.82 2865.62 267.26 o 3 2 1 927.45 1084.70 82.89 o 4 2 1 183.75 188.36 18.59 o 5 2 1 1365.84 1282.62 121.70 o 6 2 1 5.99 5.43 4.98 < 7 2 1 43.31 59.56 7.57 o 8 2 1 396.08 334.01 36.41 o 9 2 1 65.28 63.28 9.63 o 10 2 1 56.36 44.29 9.45 o 11 2 1 242.60 272.58 24.25 o 12 2 1 8.38 9.63 9.80 < 13 2 1 13.41 10.88 7.03 < 14 2 1 11.79 10.06 7.14 < 15 2 1 17.28 11.35 7.87 o 16 2 1 59.93 75.92 11.03 o 17 2 1 4.35 1.86 8.34 < -16 3 1 -7.43 0.16 7.53 < -15 3 1 3.69 0.23 6.99 < -14 3 1 9.07 0.97 6.78 < -13 3 1 26.69 32.89 8.20 o -12 3 1 28.15 38.99 7.98 o -11 3 1 38.59 40.39 8.66 o -10 3 1 37.36 43.98 8.58 o -9 3 1 26.36 17.47 7.31 o -8 3 1 24.43 16.88 8.42 o -7 3 1 117.90 128.23 15.46 o -6 3 1 394.50 517.35 38.37 o -5 3 1 147.06 142.77 17.45 o -4 3 1 300.90 419.32 28.05 o -3 3 1 449.06 448.38 40.61 o -2 3 1 448.94 604.85 42.22 o -1 3 1 4562.66 4602.53 416.69 o 0 3 1 11.25 25.13 5.88 < 1 3 1 42.89 107.57 8.54 o 2 3 1 75.25 80.20 10.69 o 3 3 1 1998.33 2189.96 178.11 o 4 3 1 313.78 348.78 30.84 o 5 3 1 234.98 317.62 25.68 o 6 3 1 29.14 42.77 7.29 o 7 3 1 653.62 795.70 59.30 o 8 3 1 94.44 93.05 12.70 o 9 3 1 37.43 38.84 8.68 o 10 3 1 46.51 45.24 9.15 o 11 3 1 -0.36 0.00 6.76 < 12 3 1 50.76 60.56 9.68 o 13 3 1 15.99 12.44 10.24 < 14 3 1 1.41 1.67 6.63 < 15 3 1 15.67 22.56 7.67 o 16 3 1 -5.87 1.15 7.61 < -15 4 1 11.99 3.28 6.33 < -14 4 1 12.59 8.62 7.19 < -13 4 1 -3.30 0.94 6.93 < -12 4 1 4.59 4.43 7.32 < -11 4 1 86.15 81.12 12.60 o -10 4 1 -1.66 1.84 8.13 < -9 4 1 200.38 189.48 22.13 o -8 4 1 48.85 60.13 10.20 o -7 4 1 175.58 180.39 19.52 o -6 4 1 15.06 5.88 7.99 < -5 4 1 301.13 360.35 32.60 o -4 4 1 349.60 367.72 36.57 o -3 4 1 712.16 860.58 68.73 o -2 4 1 602.47 626.09 56.48 o -1 4 1 957.98 984.36 84.83 o 0 4 1 -1.82 3.19 7.61 < 1 4 1 2892.99 3286.17 257.13 o 2 4 1 115.15 118.25 15.32 o 3 4 1 118.52 105.57 14.67 o 4 4 1 44.81 47.04 9.27 o 5 4 1 961.51 1015.52 86.30 o 6 4 1 101.25 111.23 13.33 o 7 4 1 112.97 104.75 14.39 o 8 4 1 53.03 55.20 9.92 o 9 4 1 63.85 62.72 10.76 o 10 4 1 74.47 73.24 11.70 o 11 4 1 32.98 30.54 8.90 o 12 4 1 41.76 49.51 9.46 o 13 4 1 12.22 11.76 7.90 < 14 4 1 3.32 2.24 7.46 < 15 4 1 16.67 10.73 7.30 o -12 5 1 -5.80 0.96 8.73 < -11 5 1 8.55 7.27 8.31 < -10 5 1 14.26 9.46 8.73 < -9 5 1 34.38 46.15 9.76 o -8 5 1 -5.53 1.51 7.59 < -7 5 1 4.33 5.06 7.96 < -6 5 1 -0.35 3.34 7.36 < -5 5 1 98.27 102.65 14.54 o -4 5 1 2.93 5.36 7.98 < -3 5 1 57.18 47.77 11.65 o -2 5 1 -2.89 0.13 7.20 < -1 5 1 170.91 173.47 22.15 o 0 5 1 32.55 29.70 10.80 o 1 5 1 123.32 88.90 16.54 o 2 5 1 299.01 295.65 32.73 o 3 5 1 524.56 659.12 53.05 o 4 5 1 -0.10 0.71 7.92 < 5 5 1 84.77 86.99 13.07 o 6 5 1 -3.11 1.09 8.04 < 7 5 1 282.89 255.63 29.26 o 8 5 1 9.69 1.65 8.12 < 9 5 1 11.86 2.93 7.80 < 10 5 1 43.25 40.28 9.88 o 11 5 1 -0.05 0.30 7.26 < 12 5 1 -2.26 5.55 5.18 < -10 6 1 0.01 2.77 1.14 < -9 6 1 -4.01 5.22 5.56 < -8 6 1 7.41 8.97 9.54 < -7 6 1 10.18 6.05 10.74 < -6 6 1 8.91 4.36 10.81 < -5 6 1 22.10 28.69 11.85 < -4 6 1 5.17 2.25 9.72 < -3 6 1 45.51 46.23 13.30 o -2 6 1 -7.32 0.01 5.73 < 2 6 1 24.94 15.04 11.96 o 3 6 1 15.18 3.83 10.95 < 4 6 1 40.14 42.08 12.91 o 5 6 1 1.61 6.58 12.34 < 6 6 1 18.40 11.46 13.36 < 7 6 1 3.73 3.84 9.54 < 8 6 1 11.85 9.74 9.59 < -18 0 2 42.73 19.32 8.88 o -16 0 2 72.60 79.32 11.69 o -14 0 2 -3.36 12.91 6.01 < -12 0 2 43.28 48.90 8.23 o -10 0 2 629.86 711.34 59.11 o -4 0 2 258.91 233.53 23.57 o 4 0 2 743.80 579.83 66.23 o 8 0 2 8986.40 7000.34 890.42 o 10 0 2 505.02 571.29 46.35 o 12 0 2 3.59 21.71 9.13 < 14 0 2 81.90 84.93 10.66 o 16 0 2 68.44 46.37 9.96 o -18 1 2 6.51 12.10 7.94 < -17 1 2 1.61 0.36 7.10 < -16 1 2 43.29 26.24 9.07 o -15 1 2 2.37 2.21 6.20 < -14 1 2 41.33 43.52 8.77 o -13 1 2 7.78 5.76 6.28 < -12 1 2 47.62 50.48 8.53 o -11 1 2 225.82 193.54 23.05 o -10 1 2 263.87 316.38 26.06 o -9 1 2 299.84 291.12 28.83 o -8 1 2 -1.28 0.44 4.36 < -7 1 2 938.52 859.29 84.95 o -6 1 2 507.91 508.83 46.83 o -5 1 2 3628.17 3235.52 360.14 o -4 1 2 209.36 203.90 20.74 o -3 1 2 3382.13 4192.30 336.52 o -2 1 2 1064.44 1170.06 97.65 o -1 1 2 1875.59 1725.37 175.72 o 2 1 2 1613.66 1434.61 133.10 o 5 1 2 32.18 40.85 5.20 o 6 1 2 512.08 454.13 46.19 o 7 1 2 178.12 150.71 17.51 o 8 1 2 1906.30 1680.05 168.81 o 9 1 2 -1.12 0.53 5.62 < 10 1 2 93.81 135.56 11.53 o 11 1 2 552.33 520.73 49.85 o 12 1 2 162.19 162.72 17.52 o 13 1 2 5.47 8.60 6.88 < 14 1 2 8.93 21.33 6.91 < 15 1 2 3.80 0.81 5.96 < 16 1 2 36.40 34.76 7.75 o 17 1 2 16.48 14.01 6.94 o -17 2 2 -1.31 2.65 7.79 < -16 2 2 15.48 17.74 7.84 o -15 2 2 -5.84 0.23 6.47 < -14 2 2 17.81 22.10 7.21 o -13 2 2 3.14 4.53 7.49 < -12 2 2 98.26 116.95 12.34 o -11 2 2 48.76 45.67 9.05 o -10 2 2 3.86 3.70 7.39 < -9 2 2 599.62 576.54 54.14 o -8 2 2 10.02 0.41 5.77 < -7 2 2 331.46 291.11 31.53 o -6 2 2 1309.85 1221.98 121.27 o -5 2 2 2353.66 2484.28 211.60 o -4 2 2 100.59 122.66 12.33 o -3 2 2 1198.10 1517.63 108.40 o -2 2 2 348.40 364.67 32.60 o -1 2 2 6051.14 6694.00 601.09 o 1 2 2 733.40 791.51 65.92 o 2 2 2 62.54 66.33 8.33 o 3 2 2 280.26 229.96 27.25 o 4 2 2 66.64 62.24 8.95 o 5 2 2 37.44 10.13 6.57 o 6 2 2 16.16 15.27 5.75 o 7 2 2 221.59 279.67 21.78 o 8 2 2 18.44 31.66 6.52 o 9 2 2 279.49 285.38 27.30 o 10 2 2 15.60 29.16 7.22 o 11 2 2 393.72 422.57 37.24 o 12 2 2 8.37 0.67 6.94 < 13 2 2 4.32 0.76 8.23 < 14 2 2 0.91 8.09 7.18 < 15 2 2 2.31 12.44 7.46 < 16 2 2 23.61 21.59 8.79 o 17 2 2 8.44 1.46 7.97 < -16 3 2 -2.34 3.99 7.25 < -15 3 2 8.43 11.50 7.31 < -14 3 2 -3.72 1.01 8.06 < -13 3 2 31.91 30.00 8.50 o -12 3 2 147.17 168.32 16.88 o -11 3 2 0.84 2.09 7.39 < -10 3 2 16.52 21.70 7.32 o -9 3 2 236.59 287.73 25.87 o -8 3 2 4.68 2.13 8.84 < -7 3 2 2.73 0.41 8.40 < -6 3 2 6.13 12.02 7.49 < -5 3 2 18.82 16.04 8.23 o -4 3 2 18.91 11.22 8.06 o -3 3 2 25.88 24.36 7.96 o -2 3 2 1287.48 1400.46 117.48 o -1 3 2 1422.08 1398.16 127.54 o 0 3 2 465.39 369.44 44.43 o 1 3 2 60.26 65.91 8.96 o 2 3 2 2511.26 2728.00 216.92 o 3 3 2 1719.82 1828.45 153.81 o 4 3 2 11.95 4.28 5.70 o 5 3 2 -0.52 0.35 6.29 < 6 3 2 34.67 32.08 8.09 o 7 3 2 1189.98 1339.22 105.17 o 8 3 2 569.11 595.38 51.42 o 9 3 2 33.85 41.38 8.08 o 10 3 2 11.01 10.70 7.09 < 11 3 2 2.42 1.20 6.81 < 12 3 2 91.02 112.78 12.63 o 13 3 2 4.78 8.25 7.08 < 14 3 2 37.30 39.13 9.30 o 15 3 2 -0.91 0.15 7.45 < 16 3 2 -9.73 9.71 9.49 < -14 4 2 42.51 39.00 10.07 o -13 4 2 40.10 35.97 9.47 o -12 4 2 8.99 2.98 7.40 < -11 4 2 12.58 13.77 7.32 < -10 4 2 142.55 162.92 17.25 o -9 4 2 -4.63 0.04 8.82 < -8 4 2 82.22 77.88 12.60 o -7 4 2 7.12 13.87 7.18 < -6 4 2 -1.38 2.79 8.76 < -5 4 2 35.30 37.57 10.79 o -4 4 2 213.51 230.90 25.04 o -3 4 2 292.46 309.87 31.82 o -2 4 2 121.35 114.79 17.46 o -1 4 2 412.82 368.13 40.29 o 0 4 2 852.35 902.94 79.60 o 1 4 2 427.08 460.04 41.24 o 2 4 2 236.83 280.77 24.04 o 3 4 2 81.89 79.01 12.11 o 4 4 2 250.86 287.62 25.55 o 5 4 2 -2.58 5.57 6.68 < 6 4 2 123.62 140.99 15.41 o 7 4 2 17.64 13.80 7.26 o 8 4 2 82.30 80.56 12.04 o 9 4 2 -1.39 0.20 8.26 < 10 4 2 300.67 331.95 29.84 o 11 4 2 17.88 17.12 7.62 o 12 4 2 21.58 29.64 7.89 o 13 4 2 -0.15 0.59 9.19 < 14 4 2 27.11 37.99 8.86 o -12 5 2 -1.11 0.21 7.44 < -11 5 2 11.76 14.34 8.77 < -10 5 2 56.41 46.64 11.64 o -9 5 2 59.57 47.57 11.16 o -8 5 2 41.96 47.41 10.71 o -7 5 2 96.46 98.01 14.27 o -6 5 2 14.05 19.21 8.83 < -5 5 2 -2.18 0.10 10.68 < -4 5 2 40.86 26.51 10.71 o -3 5 2 245.60 204.99 28.82 o -2 5 2 205.50 197.24 26.87 o -1 5 2 327.37 327.00 35.43 o 0 5 2 10.09 3.74 9.74 < 1 5 2 7.61 6.39 8.66 < 2 5 2 119.42 118.83 17.52 o 3 5 2 5.16 0.08 9.49 < 4 5 2 200.65 150.85 23.66 o 5 5 2 7.43 2.42 8.31 < 6 5 2 117.87 120.26 17.32 o 7 5 2 -4.00 0.60 8.12 < 8 5 2 58.41 54.85 10.66 o 9 5 2 74.20 76.05 12.33 o 10 5 2 4.02 2.45 7.81 < 11 5 2 5.62 6.08 7.94 < 12 5 2 7.42 13.20 5.72 < -9 6 2 3.87 1.62 9.80 < -8 6 2 1.92 0.47 9.33 < -7 6 2 4.75 7.98 11.43 < -6 6 2 0.56 5.17 9.95 < -5 6 2 25.22 23.25 10.75 o -4 6 2 19.03 17.66 11.55 < -3 6 2 1.88 19.77 6.60 < -2 6 2 107.19 75.95 13.94 o -1 6 2 66.92 62.32 11.04 o 0 6 2 17.85 4.99 15.16 < 1 6 2 50.60 27.78 16.12 o 2 6 2 40.91 34.14 12.62 o 3 6 2 28.91 16.49 11.81 o 4 6 2 1.58 0.56 9.62 < 5 6 2 46.14 27.57 12.84 o 6 6 2 7.11 2.36 10.26 < 7 6 2 0.70 0.22 16.38 < 8 6 2 6.15 3.36 8.86 < -17 0 3 4.20 1.61 7.40 < -15 0 3 29.08 25.16 7.82 o -13 0 3 333.42 370.58 33.21 o -11 0 3 182.18 196.69 19.34 o -9 0 3 635.42 629.91 57.47 o -7 0 3 616.14 670.15 55.47 o -5 0 3 1208.44 1290.50 107.11 o 3 0 3 1265.94 924.92 112.27 o 5 0 3 3511.62 3088.55 319.79 o 7 0 3 62.56 41.90 7.90 o 9 0 3 1948.96 1867.25 172.79 o 11 0 3 2433.18 1923.57 200.94 o 13 0 3 8.94 10.83 5.32 < 15 0 3 162.53 140.33 16.60 o 17 0 3 52.96 35.83 9.98 o -18 1 3 16.96 12.91 8.50 o -17 1 3 1.45 3.16 7.28 < -16 1 3 14.48 5.45 7.28 o -15 1 3 17.10 20.66 7.46 o -14 1 3 56.76 53.73 9.77 o -13 1 3 71.66 61.73 10.70 o -12 1 3 2.28 1.40 4.38 < -11 1 3 2134.59 2219.88 192.25 o -10 1 3 234.65 255.09 23.58 o -9 1 3 8.44 16.15 5.39 < -8 1 3 378.77 386.59 35.63 o -7 1 3 854.84 765.39 77.76 o -6 1 3 268.22 267.84 25.92 o -5 1 3 969.24 1008.27 85.63 o -4 1 3 520.65 512.49 48.39 o -3 1 3 111.76 90.95 13.17 o 1 1 3 106.25 88.23 11.51 o 4 1 3 2.12 0.16 3.72 < 5 1 3 4197.09 3485.06 382.19 o 6 1 3 81.38 77.52 9.67 o 7 1 3 4090.91 3653.12 361.12 o 8 1 3 36.75 39.70 6.74 o 9 1 3 87.96 84.59 11.06 o 10 1 3 6.32 2.29 6.03 < 11 1 3 55.37 58.16 9.47 o 12 1 3 21.19 15.21 7.87 o 13 1 3 7.50 3.72 7.37 < 14 1 3 8.22 7.12 6.29 < 15 1 3 33.04 26.48 7.84 o 16 1 3 35.03 31.40 8.54 o 17 1 3 23.99 25.84 7.80 o -17 2 3 0.04 2.03 7.17 < -16 2 3 24.90 21.31 8.25 o -15 2 3 1.63 0.56 8.04 < -14 2 3 7.89 1.29 6.43 < -13 2 3 4.59 5.06 6.59 < -12 2 3 0.78 6.83 6.41 < -11 2 3 418.45 518.27 39.62 o -10 2 3 -1.82 0.01 6.27 < -9 2 3 -3.13 7.65 6.23 < -8 2 3 88.74 55.80 12.13 o -7 2 3 139.59 170.45 16.26 o -6 2 3 3334.39 3632.44 299.36 o -5 2 3 8.82 23.00 6.35 < -4 2 3 167.25 158.06 17.85 o -3 2 3 294.20 332.97 27.86 o -2 2 3 894.98 982.83 82.01 o -1 2 3 481.41 620.44 43.26 o 0 2 3 2541.45 2834.87 227.86 o 1 2 3 331.98 339.81 31.24 o 2 2 3 94.34 74.17 10.82 o 3 2 3 946.25 1075.08 82.85 o 4 2 3 1221.41 1141.75 106.47 o 5 2 3 1461.37 1490.93 127.12 o 6 2 3 826.04 968.25 69.29 o 7 2 3 3.55 0.99 5.62 < 8 2 3 102.44 60.29 12.65 o 9 2 3 220.30 225.88 22.42 o 10 2 3 556.86 639.72 51.24 o 11 2 3 -2.51 0.76 7.90 < 12 2 3 9.74 4.36 6.98 < 13 2 3 22.92 27.63 8.20 o 14 2 3 14.35 21.77 7.59 < 15 2 3 26.38 24.58 9.14 o 16 2 3 9.51 10.01 6.95 < 17 2 3 9.27 5.68 8.39 < -16 3 3 7.64 9.94 7.86 < -15 3 3 3.14 0.67 7.15 < -14 3 3 19.55 13.82 7.82 o -13 3 3 37.43 36.79 8.76 o -12 3 3 5.65 13.51 6.73 < -11 3 3 39.70 25.04 8.62 o -10 3 3 185.16 202.50 21.69 o -9 3 3 219.65 246.81 24.93 o -8 3 3 38.82 36.33 10.60 o -7 3 3 36.87 11.75 12.11 o -6 3 3 -1.98 0.17 9.94 < -5 3 3 95.15 108.75 14.08 o -4 3 3 300.77 297.50 31.49 o -3 3 3 554.67 581.35 50.82 o -2 3 3 436.59 432.65 41.27 o -1 3 3 29.11 50.41 7.97 o 0 3 3 460.55 566.72 43.25 o 1 3 3 65.86 50.37 9.71 o 2 3 3 5758.10 5872.15 525.33 o 3 3 3 96.73 99.94 12.02 o 4 3 3 249.88 266.95 24.42 o 5 3 3 361.66 415.75 34.59 o 6 3 3 792.03 837.90 71.52 o 7 3 3 40.57 44.09 8.68 o 8 3 3 23.00 19.22 7.88 o 9 3 3 313.06 322.89 30.70 o 10 3 3 231.55 244.54 23.80 o 11 3 3 128.77 161.51 15.48 o 12 3 3 16.00 12.85 7.65 o 13 3 3 1.65 4.25 7.24 < 14 3 3 11.68 11.79 8.00 < 15 3 3 -2.73 1.06 10.29 < 16 3 3 -1.12 0.23 9.72 < -15 4 3 51.92 42.20 10.74 o -14 4 3 7.98 7.08 7.81 < -13 4 3 1.32 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