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In the title compound, [Zn4(C4H4O4)3(NO3)2(C12H10N2)2], the tetra­nuclear Zn4(gauche-succinato)2 building blocks are bridged by succinate and trans-di-4-pyridylethyl­ene ligands to form a distorted two-dimensional (4,4)-square grid. Packing of these square grids leads to a condensed metal–organic framework. One of the two independent Zn atoms shows tetra­hedral whereas the other shows octa­hedral coordination. They are bridged by three succinate ligands, with a Zn...Zn distance of 3.1505 (12) Å.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806002935/ng6284sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806002935/ng6284Isup2.hkl
Contains datablock I

CCDC reference: 298507

Key indicators

  • Single-crystal X-ray study
  • T = 110 K
  • Mean [sigma](C-C) = 0.005 Å
  • R factor = 0.050
  • wR factor = 0.086
  • Data-to-parameter ratio = 17.1

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.98 PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings Differ .... ? PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ? PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............ 2.00 Ratio
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion

Computing details top

Data collection: COLLECT (Nonius, 2000); cell refinement: DENZO and SCALEPACK (Otwinowski & Minor, 1997); data reduction: DENZO and SCALEPACK; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 for Windows (Farrugia, 1997); software used to prepare material for publication: SHELXL97.

Poly[bis(µ2-trans-di-4-pyridylethylene-κ2N:N')bis(nitrato-κ2O,O') bis(µ4-succinato-κ4O:O':O'':O''')(µ4-succinato- κ4O:O:O':O')tetrazinc(II) top
Crystal data top
[Zn4(C4H4O4)3(NO3)2(C12H10N2)2]Z = 1
Mr = 1098.16F(000) = 554
Triclinic, P1Dx = 1.794 Mg m3
Hall symbol: -P 1Mo Kα radiation, λ = 0.71073 Å
a = 9.615 (4) ÅCell parameters from 4442 reflections
b = 9.804 (4) Åθ = 2.6–28.3°
c = 11.729 (4) ŵ = 2.42 mm1
α = 82.58 (2)°T = 110 K
β = 80.87 (2)°Fragment, colorless
γ = 69.097 (14)°0.08 × 0.08 × 0.03 mm
V = 1016.6 (7) Å3
Data collection top
Nonius KappaCCD (with an Oxford Cryosystems Cryostream cooler)
diffractometer
4947 independent reflections
Radiation source: fine-focus sealed tube3320 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.059
ω scans with κ offsetsθmax = 28.3°, θmin = 2.6°
Absorption correction: multi-scan
(DENZO and SCALEPACK; Otwinowski & Minor, 1997)
h = 1212
Tmin = 0.861, Tmax = 0.930k = 1312
16627 measured reflectionsl = 1514
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.050Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.086H-atom parameters constrained
S = 1.01 w = 1/[σ2(Fo2) + (0.0226P)2 + 1.0067P]
where P = (Fo2 + 2Fc2)/3
4947 reflections(Δ/σ)max = 0.001
289 parametersΔρmax = 0.59 e Å3
0 restraintsΔρmin = 0.52 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Zn10.28403 (5)0.39548 (4)0.66022 (3)0.01422 (12)
Zn20.35078 (5)0.64970 (5)0.75451 (3)0.01649 (12)
O10.5071 (3)0.3385 (3)0.6503 (2)0.0173 (6)
O20.5581 (3)0.5169 (3)0.7182 (2)0.0201 (6)
O30.2140 (3)0.5894 (3)0.56497 (19)0.0172 (6)
O40.2745 (3)0.7706 (3)0.61817 (19)0.0180 (6)
O50.2621 (3)0.4998 (3)0.82363 (19)0.0164 (6)
O60.0626 (3)0.6969 (3)0.8629 (2)0.0217 (6)
O70.2530 (3)0.2062 (3)0.7716 (2)0.0219 (6)
O80.0602 (3)0.3910 (3)0.7258 (2)0.0188 (6)
O90.0270 (3)0.2037 (3)0.8337 (2)0.0312 (7)
N10.2890 (3)0.2883 (3)0.5148 (2)0.0161 (7)
N20.3659 (3)0.7616 (3)0.8804 (2)0.0168 (7)
N30.1108 (4)0.2644 (4)0.7786 (3)0.0211 (7)
C10.1649 (4)0.3185 (4)0.4644 (3)0.0210 (9)
H10.07430.38520.49920.025*
C20.1595 (4)0.2595 (4)0.3653 (3)0.0203 (9)
H20.06820.28650.33260.024*
C30.2915 (4)0.1587 (4)0.3137 (3)0.0171 (8)
C40.4213 (4)0.1268 (4)0.3657 (3)0.0181 (8)
H40.51340.05940.33380.022*
C50.4156 (4)0.1936 (4)0.4640 (3)0.0169 (8)
H50.50570.17150.49740.020*
C60.4812 (4)0.7078 (4)0.9445 (3)0.0184 (8)
H60.55960.61940.92480.022*
C70.4898 (4)0.7752 (4)1.0367 (3)0.0182 (8)
H70.57310.73341.07960.022*
C80.3769 (4)0.9050 (4)1.0680 (3)0.0176 (8)
C90.2581 (4)0.9610 (4)1.0009 (3)0.0215 (9)
H90.17931.05001.01840.026*
C100.2552 (4)0.8874 (4)0.9095 (3)0.0220 (9)
H100.17270.92610.86560.026*
C110.3885 (4)0.9753 (4)1.1671 (3)0.0187 (8)
H110.47870.93491.20200.022*
C120.2820 (4)1.0919 (4)1.2124 (3)0.0200 (8)
H120.19331.13451.17580.024*
C130.5958 (4)0.3931 (4)0.6789 (3)0.0140 (8)
C140.2293 (4)0.7125 (4)0.5472 (3)0.0157 (8)
C150.1916 (4)0.7978 (4)0.4326 (3)0.0183 (8)
H15A0.24300.87080.41590.022*
H15B0.08220.85130.43760.022*
C160.2396 (4)0.6962 (4)0.3340 (3)0.0144 (8)
H16A0.18140.62890.34800.017*
H16B0.21460.75590.26040.017*
C170.1320 (4)0.5673 (4)0.8835 (3)0.0187 (8)
C180.0843 (4)0.4747 (4)0.9842 (3)0.0210 (9)
H18A0.13170.47821.05230.025*
H18B0.12060.37160.96430.025*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Zn10.0126 (2)0.0158 (2)0.0149 (2)0.00524 (18)0.00110 (17)0.00323 (17)
Zn20.0195 (2)0.0181 (2)0.0140 (2)0.00821 (19)0.00057 (18)0.00527 (18)
O10.0080 (12)0.0241 (15)0.0206 (14)0.0044 (11)0.0015 (10)0.0081 (11)
O20.0155 (14)0.0214 (15)0.0249 (15)0.0071 (11)0.0012 (11)0.0089 (12)
O30.0209 (14)0.0136 (14)0.0166 (13)0.0055 (11)0.0029 (10)0.0005 (10)
O40.0228 (14)0.0197 (14)0.0123 (13)0.0088 (11)0.0004 (10)0.0028 (11)
O50.0148 (13)0.0210 (14)0.0129 (13)0.0063 (11)0.0023 (10)0.0046 (11)
O60.0177 (14)0.0215 (16)0.0226 (14)0.0037 (12)0.0007 (11)0.0007 (12)
O70.0131 (14)0.0261 (15)0.0264 (15)0.0064 (12)0.0055 (11)0.0013 (12)
O80.0175 (14)0.0179 (14)0.0186 (14)0.0040 (11)0.0038 (11)0.0031 (11)
O90.0208 (15)0.0381 (18)0.0385 (17)0.0192 (14)0.0074 (13)0.0143 (14)
N10.0196 (17)0.0156 (17)0.0157 (16)0.0077 (14)0.0030 (13)0.0049 (13)
N20.0202 (17)0.0147 (17)0.0156 (16)0.0060 (14)0.0023 (13)0.0012 (13)
N30.0197 (18)0.0247 (19)0.0221 (18)0.0108 (16)0.0061 (14)0.0000 (14)
C10.017 (2)0.021 (2)0.025 (2)0.0037 (17)0.0030 (16)0.0058 (17)
C20.017 (2)0.023 (2)0.024 (2)0.0051 (17)0.0080 (16)0.0068 (17)
C30.023 (2)0.015 (2)0.0158 (19)0.0115 (16)0.0002 (16)0.0012 (15)
C40.0156 (19)0.019 (2)0.018 (2)0.0049 (16)0.0002 (15)0.0029 (16)
C50.0166 (19)0.014 (2)0.021 (2)0.0053 (16)0.0038 (15)0.0019 (16)
C60.0135 (19)0.021 (2)0.018 (2)0.0030 (16)0.0019 (15)0.0039 (16)
C70.018 (2)0.023 (2)0.0135 (19)0.0053 (17)0.0038 (15)0.0030 (16)
C80.023 (2)0.017 (2)0.0141 (19)0.0085 (16)0.0019 (15)0.0005 (15)
C90.021 (2)0.016 (2)0.023 (2)0.0004 (17)0.0011 (16)0.0070 (16)
C100.024 (2)0.016 (2)0.024 (2)0.0010 (17)0.0088 (17)0.0032 (17)
C110.019 (2)0.019 (2)0.019 (2)0.0067 (17)0.0032 (15)0.0001 (16)
C120.019 (2)0.021 (2)0.020 (2)0.0063 (17)0.0038 (16)0.0023 (16)
C130.0172 (19)0.019 (2)0.0059 (17)0.0072 (16)0.0005 (14)0.0003 (14)
C140.0109 (18)0.019 (2)0.0124 (19)0.0003 (15)0.0034 (14)0.0058 (15)
C150.0149 (19)0.022 (2)0.0168 (19)0.0066 (16)0.0007 (15)0.0013 (16)
C160.0146 (18)0.019 (2)0.0099 (18)0.0064 (15)0.0036 (14)0.0008 (15)
C170.020 (2)0.028 (2)0.0116 (19)0.0098 (18)0.0052 (15)0.0018 (16)
C180.019 (2)0.017 (2)0.021 (2)0.0012 (17)0.0004 (16)0.0009 (16)
Geometric parameters (Å, º) top
Zn1—O12.002 (2)C3—C12i1.458 (5)
Zn1—O32.023 (3)C4—C51.382 (5)
Zn1—N12.102 (3)C4—H40.9500
Zn1—O82.182 (3)C5—H50.9500
Zn1—O72.210 (3)C6—C71.366 (5)
Zn1—O52.233 (2)C6—H60.9500
Zn1—Zn23.1505 (12)C7—C81.394 (5)
Zn2—O41.940 (3)C7—H70.9500
Zn2—O21.968 (2)C8—C91.397 (5)
Zn2—O51.977 (2)C8—C111.463 (5)
Zn2—N22.001 (3)C9—C101.377 (5)
O1—C131.261 (4)C9—H90.9500
O2—C131.263 (4)C10—H100.9500
O3—C141.254 (4)C11—C121.336 (5)
O4—C141.272 (4)C11—H110.9500
O5—C171.321 (4)C12—C3ii1.458 (5)
O6—C171.219 (4)C12—H120.9500
O7—N31.273 (4)C13—C16iii1.504 (5)
O8—N31.276 (4)C14—C151.512 (5)
O9—N31.224 (4)C15—C161.531 (5)
N1—C11.338 (5)C15—H15A0.9900
N1—C51.343 (4)C15—H15B0.9900
N2—C61.348 (4)C16—C13iii1.504 (5)
N2—C101.352 (4)C16—H16A0.9900
C1—C21.379 (5)C16—H16B0.9900
C1—H10.9500C17—C181.510 (5)
C2—C31.403 (5)C18—C18iv1.515 (7)
C2—H20.9500C18—H18A0.9900
C3—C41.394 (5)C18—H18B0.9900
O1—Zn1—O3105.79 (10)C4—C3—C12i124.9 (3)
O1—Zn1—N195.03 (10)C2—C3—C12i118.0 (3)
O3—Zn1—N189.11 (11)C5—C4—C3119.8 (3)
O1—Zn1—O8157.64 (10)C5—C4—H4120.1
O3—Zn1—O895.84 (10)C3—C4—H4120.1
N1—Zn1—O890.85 (10)N1—C5—C4123.3 (3)
O1—Zn1—O799.52 (10)N1—C5—H5118.3
O3—Zn1—O7154.69 (10)C4—C5—H5118.3
N1—Zn1—O788.64 (11)N2—C6—C7122.7 (3)
O8—Zn1—O759.00 (9)N2—C6—H6118.7
O1—Zn1—O588.94 (9)C7—C6—H6118.7
O3—Zn1—O593.65 (9)C6—C7—C8120.2 (3)
N1—Zn1—O5174.38 (10)C6—C7—H7119.9
O8—Zn1—O584.00 (9)C8—C7—H7119.9
O7—Zn1—O586.78 (9)C7—C8—C9117.0 (3)
O1—Zn1—Zn272.62 (7)C7—C8—C11119.2 (3)
O3—Zn1—Zn266.04 (7)C9—C8—C11123.7 (3)
N1—Zn1—Zn2146.75 (8)C10—C9—C8120.1 (3)
O8—Zn1—Zn2112.44 (7)C10—C9—H9120.0
O7—Zn1—Zn2123.34 (7)C8—C9—H9120.0
O5—Zn1—Zn238.57 (6)N2—C10—C9122.0 (3)
O4—Zn2—O2111.41 (10)N2—C10—H10119.0
O4—Zn2—O5118.65 (10)C9—C10—H10119.0
O2—Zn2—O597.71 (11)C12—C11—C8125.1 (4)
O4—Zn2—N2114.37 (11)C12—C11—H11117.5
O2—Zn2—N2103.29 (11)C8—C11—H11117.5
O5—Zn2—N2109.12 (11)C11—C12—C3ii125.1 (4)
O4—Zn2—Zn187.16 (8)C11—C12—H12117.5
O2—Zn2—Zn180.92 (8)C3ii—C12—H12117.5
O5—Zn2—Zn144.76 (7)O1—C13—O2125.4 (3)
N2—Zn2—Zn1153.64 (9)O1—C13—C16iii117.7 (3)
C13—O1—Zn1135.4 (2)O2—C13—C16iii116.9 (3)
C13—O2—Zn2125.5 (2)O3—C14—O4125.0 (3)
C14—O3—Zn1142.3 (2)O3—C14—C15117.4 (3)
C14—O4—Zn2117.4 (2)O4—C14—C15117.7 (3)
C17—O5—Zn2107.8 (2)C14—C15—C16111.2 (3)
C17—O5—Zn1123.6 (2)C14—C15—H15A109.4
Zn2—O5—Zn196.68 (9)C16—C15—H15A109.4
N3—O7—Zn191.8 (2)C14—C15—H15B109.4
N3—O8—Zn193.07 (19)C16—C15—H15B109.4
C1—N1—C5116.6 (3)H15A—C15—H15B108.0
C1—N1—Zn1120.5 (2)C13iii—C16—C15113.5 (3)
C5—N1—Zn1122.8 (2)C13iii—C16—H16A108.9
C6—N2—C10118.0 (3)C15—C16—H16A108.9
C6—N2—Zn2120.8 (2)C13iii—C16—H16B108.9
C10—N2—Zn2120.9 (2)C15—C16—H16B108.9
O9—N3—O7122.3 (3)H16A—C16—H16B107.7
O9—N3—O8121.6 (3)O6—C17—O5121.8 (3)
O7—N3—O8116.1 (3)O6—C17—C18123.3 (3)
N1—C1—C2124.4 (3)O5—C17—C18114.7 (3)
N1—C1—H1117.8C17—C18—C18iv112.5 (4)
C2—C1—H1117.8C17—C18—H18A109.1
C1—C2—C3118.7 (3)C18iv—C18—H18A109.1
C1—C2—H2120.6C17—C18—H18B109.1
C3—C2—H2120.6C18iv—C18—H18B109.1
C4—C3—C2117.1 (3)H18A—C18—H18B107.8
O1—Zn1—Zn2—O4111.76 (10)N1—Zn1—O8—N387.19 (19)
O3—Zn1—Zn2—O45.05 (10)O7—Zn1—O8—N30.71 (17)
N1—Zn1—Zn2—O439.81 (17)O5—Zn1—O8—N390.55 (18)
O8—Zn1—Zn2—O491.43 (10)Zn2—Zn1—O8—N3117.16 (17)
O7—Zn1—Zn2—O4158.14 (10)O1—Zn1—N1—C1164.4 (3)
O5—Zn1—Zn2—O4137.05 (12)O3—Zn1—N1—C158.7 (3)
O1—Zn1—Zn2—O20.45 (10)O8—Zn1—N1—C137.2 (3)
O3—Zn1—Zn2—O2117.26 (11)O7—Zn1—N1—C196.1 (3)
N1—Zn1—Zn2—O272.40 (17)Zn2—Zn1—N1—C198.8 (3)
O8—Zn1—Zn2—O2156.35 (10)O1—Zn1—N1—C511.8 (3)
O7—Zn1—Zn2—O289.64 (11)O3—Zn1—N1—C5117.6 (3)
O5—Zn1—Zn2—O2110.74 (13)O8—Zn1—N1—C5146.6 (3)
O1—Zn1—Zn2—O5111.19 (13)O7—Zn1—N1—C587.6 (3)
O3—Zn1—Zn2—O5132.00 (13)Zn2—Zn1—N1—C577.4 (3)
N1—Zn1—Zn2—O5176.86 (18)O4—Zn2—N2—C6142.7 (3)
O7—Zn1—Zn2—O521.10 (12)O2—Zn2—N2—C621.4 (3)
O1—Zn1—Zn2—N2102.1 (2)O5—Zn2—N2—C681.8 (3)
O3—Zn1—Zn2—N2141.1 (2)Zn1—Zn2—N2—C675.0 (4)
N1—Zn1—Zn2—N2174.0 (3)O4—Zn2—N2—C1042.6 (3)
O8—Zn1—Zn2—N254.7 (2)O2—Zn2—N2—C10163.9 (3)
O7—Zn1—Zn2—N212.0 (2)O5—Zn2—N2—C1093.0 (3)
O5—Zn1—Zn2—N29.1 (2)Zn1—Zn2—N2—C1099.7 (3)
O3—Zn1—O1—C1361.1 (3)Zn1—O7—N3—O9179.6 (3)
N1—Zn1—O1—C13151.6 (3)Zn1—O7—N3—O81.2 (3)
O8—Zn1—O1—C13103.7 (4)Zn1—O8—N3—O9179.6 (3)
O7—Zn1—O1—C13118.9 (3)Zn1—O8—N3—O71.2 (3)
O5—Zn1—O1—C1332.3 (3)C5—N1—C1—C20.1 (6)
Zn2—Zn1—O1—C133.2 (3)Zn1—N1—C1—C2176.4 (3)
O4—Zn2—O2—C1384.9 (3)N1—C1—C2—C31.2 (6)
O5—Zn2—O2—C1340.0 (3)C1—C2—C3—C41.1 (5)
N2—Zn2—O2—C13151.8 (3)C1—C2—C3—C12i177.0 (3)
Zn1—Zn2—O2—C131.6 (3)C2—C3—C4—C50.1 (5)
O1—Zn1—O3—C1446.1 (4)C12i—C3—C4—C5177.8 (3)
N1—Zn1—O3—C14141.0 (4)C1—N1—C5—C41.0 (5)
O8—Zn1—O3—C14128.2 (3)Zn1—N1—C5—C4177.4 (3)
O7—Zn1—O3—C14134.0 (3)C3—C4—C5—N11.0 (5)
O5—Zn1—O3—C1443.9 (3)C10—N2—C6—C70.1 (5)
Zn2—Zn1—O3—C1416.2 (3)Zn2—N2—C6—C7174.9 (3)
O2—Zn2—O4—C1479.3 (3)N2—C6—C7—C80.1 (6)
O5—Zn2—O4—C1433.0 (3)C6—C7—C8—C90.4 (5)
N2—Zn2—O4—C14164.1 (2)C6—C7—C8—C11180.0 (3)
Zn1—Zn2—O4—C140.2 (2)C7—C8—C9—C100.9 (5)
O4—Zn2—O5—C1777.6 (2)C11—C8—C9—C10179.5 (3)
O2—Zn2—O5—C17162.8 (2)C6—N2—C10—C90.6 (6)
N2—Zn2—O5—C1755.8 (2)Zn2—N2—C10—C9175.5 (3)
Zn1—Zn2—O5—C17128.5 (2)C8—C9—C10—N21.0 (6)
O4—Zn2—O5—Zn150.86 (13)C7—C8—C11—C12173.5 (4)
O2—Zn2—O5—Zn168.73 (11)C9—C8—C11—C126.9 (6)
N2—Zn2—O5—Zn1175.74 (10)C8—C11—C12—C3ii177.7 (3)
O1—Zn1—O5—C17179.4 (3)Zn1—O1—C13—O25.8 (6)
O3—Zn1—O5—C1773.6 (3)Zn1—O1—C13—C16iii173.9 (2)
O8—Zn1—O5—C1721.8 (3)Zn2—O2—C13—O14.4 (5)
O7—Zn1—O5—C1781.0 (3)Zn2—O2—C13—C16iii175.3 (2)
Zn2—Zn1—O5—C17116.5 (3)Zn1—O3—C14—O422.4 (6)
O1—Zn1—O5—Zn262.87 (11)Zn1—O3—C14—C15157.5 (3)
O3—Zn1—O5—Zn242.88 (11)Zn2—O4—C14—O38.8 (4)
O8—Zn1—O5—Zn2138.38 (11)Zn2—O4—C14—C15171.1 (2)
O7—Zn1—O5—Zn2162.47 (10)O3—C14—C15—C1637.5 (4)
O1—Zn1—O7—N3174.02 (18)O4—C14—C15—C16142.4 (3)
O3—Zn1—O7—N36.1 (3)C14—C15—C16—C13iii57.7 (4)
N1—Zn1—O7—N391.11 (19)Zn2—O5—C17—O623.1 (4)
O8—Zn1—O7—N30.71 (17)Zn1—O5—C17—O688.0 (4)
O5—Zn1—O7—N385.64 (19)Zn2—O5—C17—C18152.0 (3)
Zn2—Zn1—O7—N398.62 (18)Zn1—O5—C17—C1896.9 (3)
O1—Zn1—O8—N318.3 (3)O6—C17—C18—C18iv30.6 (6)
O3—Zn1—O8—N3176.38 (18)O5—C17—C18—C18iv154.4 (4)
Symmetry codes: (i) x, y1, z1; (ii) x, y+1, z+1; (iii) x+1, y+1, z+1; (iv) x, y+1, z+2.
 

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