Acta Cryst. (2006). E62, m518-m519  [ doi:10.1107/S1600536806004867 ]

Bis[4-nitro-N-(quinolin-8-yl)benzenesulfonamidato-²N,N']copper(II)

L. E. da Silva, A. C. Joussef, S. Foro and B. Schmidt

Online 15 February 2006

Key indicators

• Single-crystal X-ray study
• T = 299 K
• Mean (C-C) = 0.006 Å
• R factor = 0.071
• wR factor = 0.202
• Data-to-parameter ratio = 12.7

checkCIF/PLATON results

No syntax errors found




Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.10
            Rint given   0.108
PLAT020_ALERT_3_C The value of Rint is greater than 0.10 .........       0.11       
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.95       
PLAT213_ALERT_2_C Atom O4      has ADP max/min Ratio .............       3.10 prolat
PLAT220_ALERT_2_C Large Non-Solvent    O     Ueq(max)/Ueq(min) ...       2.61 Ratio 
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         N3     
PLAT432_ALERT_2_C Short Inter X...Y Contact  O4     ..  C1      ..       2.94 Ang.  
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      47.00 A   3  
PLAT733_ALERT_1_C Torsion Calc    -29.1(6), Rep  -29.15(19) ......       3.16 su-Rat
              S1  -N1  -CU1 -N1     1.555   1.555   1.555   2.555               

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   9 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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