# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 16a in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1412.73 _exptl_crystal_F_000 5092.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 25.9749 _cell_length_b 11.5450 _cell_length_c 23.2858 _cell_angle_alpha 90.000 _cell_angle_beta 108.806 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 78371.50 81837.61 1078.52 o 5 0 0 5570.07 5554.19 368.09 o 6 0 0 101612.86 93468.07 1585.72 o 7 0 0 627.56 731.30 410.51 o 8 0 0 1162.69 2638.84 583.54 o 9 0 0 316.98 153.80 468.15 o 10 0 0 7907.07 8100.24 599.84 o 11 0 0 702.78 846.31 449.29 o 12 0 0 29745.20 30838.65 948.82 o 13 0 0 1509.10 1659.02 501.49 o 14 0 0 18370.31 21103.58 810.53 o 15 0 0 1.63 -335.97 445.86 o 16 0 0 77425.70 81939.15 1918.00 o 17 0 0 5550.78 5249.70 796.10 o 18 0 0 39326.84 39698.46 1435.40 o 19 0 0 13532.96 14298.29 872.87 o 20 0 0 32599.41 36548.14 1717.31 o 21 0 0 2844.01 4547.36 826.31 o 22 0 0 61355.50 61503.44 1966.55 o 23 0 0 1420.79 1973.07 1011.94 o 24 0 0 606.38 718.81 685.61 o 25 0 0 11809.49 11733.04 953.86 o 26 0 0 168.19 526.69 972.71 o 27 0 0 17419.65 17715.89 1538.61 o 28 0 0 4964.83 4722.09 860.80 o 29 0 0 421.19 -90.67 977.92 o 3 1 0 362.99 345.77 217.92 o 4 1 0 4286.73 3511.91 306.22 o 5 1 0 7711.46 7023.89 458.76 o 6 1 0 37161.17 42134.49 814.15 o 7 1 0 2387.75 2348.55 367.22 o 8 1 0 52025.71 48949.27 794.68 o 9 1 0 4742.23 4075.54 379.53 o 10 1 0 174773.83 173396.55 2093.06 o 11 1 0 3951.84 2326.54 356.29 o 12 1 0 57290.71 55477.82 979.10 o 13 1 0 3933.80 3698.96 511.09 o 14 1 0 23070.33 27038.96 656.30 o 15 1 0 8302.93 7445.11 444.26 o 16 1 0 13712.11 13751.53 584.24 o 17 1 0 13156.84 13018.61 538.48 o 18 1 0 24855.28 25466.05 866.05 o 19 1 0 8818.57 10744.36 668.03 o 20 1 0 85277.04 83565.02 1395.79 o 21 1 0 55233.68 53704.54 1110.82 o 22 1 0 103756.34 105898.55 1672.54 o 23 1 0 15335.11 16439.91 705.85 o 24 1 0 584.71 1352.00 561.71 o 25 1 0 24.80 795.32 624.40 o 26 1 0 28507.15 28636.09 1153.95 o 27 1 0 221.42 -80.20 893.27 o 28 1 0 32.28 -274.50 570.62 o 29 1 0 5614.54 5020.47 1857.48 o 0 2 0 106395.05 106356.60 2492.23 o 1 2 0 15890.95 15483.10 483.24 o 2 2 0 53837.56 52420.49 1014.40 o 3 2 0 34046.74 31475.78 739.06 o 4 2 0 12544.02 14382.45 774.43 o 5 2 0 712.91 1566.19 583.33 o 6 2 0 547.06 702.77 764.82 o 7 2 0 5315.33 5236.70 1038.59 o 8 2 0 354.71 283.93 512.74 o 9 2 0 65.40 234.29 543.20 o 10 2 0 2495.23 5413.05 661.53 o 11 2 0 4434.50 4504.47 579.65 o 12 2 0 26205.52 30535.40 733.07 o 13 2 0 18762.22 18935.35 695.11 o 14 2 0 39476.39 40231.75 832.15 o 15 2 0 3451.97 3474.12 441.55 o 16 2 0 4180.12 5051.24 557.82 o 17 2 0 123.99 -377.71 473.32 o 18 2 0 13067.66 13434.18 728.70 o 19 2 0 5468.18 5040.24 557.90 o 20 2 0 20143.24 20580.49 982.27 o 21 2 0 20802.30 21355.59 942.39 o 22 2 0 53535.80 57260.08 1494.52 o 23 2 0 19423.79 19639.69 962.50 o 24 2 0 89405.70 90029.24 2285.73 o 25 2 0 1736.98 1457.42 625.64 o 26 2 0 8095.04 10587.73 1349.23 o 27 2 0 5216.60 4495.11 731.75 o 28 2 0 606.27 87.14 600.89 o 1 3 0 2527.22 2673.23 828.83 o 2 3 0 858636.63 886709.25 16306.62 o 3 3 0 9956.24 9439.88 960.52 o 4 3 0 209686.06 197412.52 3661.32 o 5 3 0 27690.49 26888.85 952.02 o 6 3 0 12565.65 16220.70 1323.15 o 7 3 0 7817.05 7179.58 687.66 o 8 3 0 78.83 186.07 578.83 o 9 3 0 560.80 781.28 495.17 o 10 3 0 2305.68 4603.79 667.96 o 11 3 0 2706.38 2794.09 363.89 o 12 3 0 82132.67 84003.79 1882.04 o 13 3 0 8186.01 6298.40 1032.23 o 14 3 0 31407.31 32158.05 884.11 o 15 3 0 6487.24 6170.55 647.98 o 16 3 0 201.03 1250.35 711.86 o 17 3 0 39350.89 40609.12 1278.87 o 18 3 0 35878.66 37199.46 1359.04 o 19 3 0 155.56 312.91 640.21 o 20 3 0 16555.61 16637.31 1041.49 o 21 3 0 46.40 404.08 575.11 o 22 3 0 353.47 372.87 527.84 o 23 3 0 2162.00 2714.05 957.28 o 24 3 0 5010.69 5950.22 960.17 o 25 3 0 4112.90 3541.17 728.67 o 26 3 0 4997.77 3867.03 785.46 o 27 3 0 1275.86 234.91 630.64 o 28 3 0 132.61 -33.46 811.99 o 0 4 0 46042.57 47613.61 3170.92 o 1 4 0 10071.11 9149.79 1137.44 o 2 4 0 92990.06 93024.20 2197.57 o 3 4 0 121056.68 109867.22 2646.06 o 4 4 0 188322.61 195082.39 3695.64 o 5 4 0 100829.47 97003.42 1866.66 o 6 4 0 23198.90 26274.20 1512.78 o 7 4 0 37872.68 41353.74 1261.14 o 8 4 0 68370.84 57313.34 4252.73 o 9 4 0 11034.09 10608.41 1019.54 o 10 4 0 92145.13 93814.41 2046.16 o 11 4 0 15294.12 15397.53 714.54 o 12 4 0 481.48 2.48 427.84 o 13 4 0 8653.68 8194.91 598.88 o 14 4 0 18201.21 19226.49 1433.49 o 15 4 0 182.87 313.23 465.63 o 16 4 0 1325.42 1682.35 525.08 o 17 4 0 522.63 658.70 601.71 o 18 4 0 3105.45 3776.92 608.51 o 19 4 0 21568.13 20592.35 804.36 o 20 4 0 6959.50 8211.29 951.41 o 21 4 0 291.08 146.67 455.29 o 22 4 0 20441.92 21219.56 806.93 o 23 4 0 4053.38 5021.40 593.91 o 24 4 0 5116.08 5574.65 626.80 o 25 4 0 6955.08 8328.27 713.76 o 26 4 0 6564.60 5047.01 720.98 o 27 4 0 1997.29 2636.70 938.12 o 1 5 0 38834.15 37451.84 1076.84 o 2 5 0 613.59 600.86 602.28 o 3 5 0 68230.66 71847.13 1743.34 o 4 5 0 114004.62 119705.91 2548.14 o 5 5 0 24758.36 24503.62 977.75 o 6 5 0 15747.73 14881.52 809.61 o 7 5 0 12328.94 11185.52 1035.61 o 8 5 0 43668.71 46061.52 1422.90 o 9 5 0 1446.60 54.66 697.53 o 10 5 0 3498.98 4058.86 1025.36 o 11 5 0 6424.57 6938.60 828.51 o 12 5 0 126319.07 125030.00 2850.44 o 13 5 0 7075.16 7089.87 728.10 o 14 5 0 44840.49 45216.79 1170.71 o 15 5 0 2717.24 3510.25 512.55 o 16 5 0 8905.82 9677.99 1260.18 o 17 5 0 36336.88 36505.03 1528.56 o 18 5 0 1395.40 1030.21 557.52 o 19 5 0 34099.82 32271.84 1301.54 o 20 5 0 5657.48 5632.62 787.33 o 21 5 0 93.39 -368.22 418.36 o 22 5 0 7115.38 7888.34 702.69 o 23 5 0 8489.83 9447.42 999.91 o 24 5 0 3508.60 3519.19 1027.38 o 25 5 0 976.24 1234.25 552.12 o 26 5 0 1801.32 3532.87 1067.06 o 27 5 0 1703.66 1419.01 866.77 o 0 6 0 60220.40 58604.63 3146.33 o 1 6 0 416.61 1121.14 1108.36 o 2 6 0 16347.24 15408.54 977.48 o 3 6 0 7238.35 7493.17 1061.52 o 4 6 0 15587.28 19610.12 1102.36 o 5 6 0 6546.19 9650.84 973.04 o 6 6 0 3006.76 3151.66 1022.18 o 7 6 0 6094.09 7077.68 828.21 o 8 6 0 13187.14 13021.97 827.06 o 9 6 0 5392.63 6297.47 1016.72 o 10 6 0 43643.26 42753.88 2415.65 o 11 6 0 14959.00 14754.59 1249.55 o 12 6 0 108.28 489.48 749.95 o 13 6 0 13486.14 12545.38 977.82 o 14 6 0 14712.36 13635.96 865.22 o 15 6 0 6699.86 6251.47 873.52 o 16 6 0 152.53 -913.65 609.10 o 17 6 0 36503.59 30005.83 1114.14 o 18 6 0 705.88 825.21 645.15 o 19 6 0 26217.55 24205.44 1031.82 o 20 6 0 10867.73 10884.03 643.75 o 21 6 0 160.66 -570.13 612.74 o 22 6 0 1377.44 1687.38 587.11 o 23 6 0 167.48 -868.38 578.92 o 24 6 0 381.51 367.66 403.15 o 25 6 0 4721.12 3663.90 495.21 o 26 6 0 1612.19 1326.58 433.73 o 1 7 0 6742.05 5994.34 1113.64 o 2 7 0 11264.04 13204.35 1626.66 o 3 7 0 8205.17 8877.59 987.61 o 4 7 0 8358.44 8204.50 1468.72 o 5 7 0 54042.16 50680.89 1654.52 o 6 7 0 202511.42 213457.69 4228.62 o 7 7 0 143949.39 139106.75 2916.76 o 8 7 0 93795.32 94295.40 2574.59 o 9 7 0 5690.12 5972.32 1144.07 o 10 7 0 3556.00 4773.05 1296.19 o 11 7 0 11122.73 7794.07 1497.84 o 12 7 0 25141.25 25683.55 2423.83 o 13 7 0 3240.13 3470.20 939.03 o 14 7 0 10942.49 9555.78 1320.95 o 15 7 0 3.10 -49.94 417.16 o 16 7 0 673.62 1799.71 893.55 o 17 7 0 974.30 1006.67 653.79 o 18 7 0 769.07 684.27 596.74 o 19 7 0 9.63 463.75 523.93 o 20 7 0 7193.01 7821.02 728.95 o 21 7 0 2947.58 2099.15 534.04 o 22 7 0 11743.77 12135.17 997.95 o 23 7 0 3316.58 3007.43 614.81 o 24 7 0 8905.18 8706.02 841.26 o 25 7 0 1474.90 1151.60 593.56 o 0 8 0 41897.92 42729.27 3538.93 o 1 8 0 15792.13 13617.19 1213.66 o 2 8 0 25074.74 28098.13 1526.55 o 3 8 0 720.23 533.42 820.16 o 4 8 0 421.35 170.52 765.04 o 5 8 0 157306.41 152296.11 4190.56 o 6 8 0 10021.26 11125.83 1445.26 o 7 8 0 64227.76 64518.83 2470.79 o 8 8 0 1778.47 1772.86 1268.85 o 9 8 0 1733.51 2924.44 900.74 o 10 8 0 3047.60 3316.06 801.62 o 11 8 0 13465.72 15578.56 1214.12 o 12 8 0 1106.57 873.85 928.79 o 13 8 0 423.67 1714.01 805.09 o 14 8 0 35288.74 37778.01 1673.82 o 15 8 0 26166.49 24371.39 1650.52 o 16 8 0 24797.83 24986.30 1137.37 o 17 8 0 4472.93 4503.53 720.33 o 18 8 0 1435.85 2941.44 814.91 o 19 8 0 2164.78 3069.43 645.48 o 20 8 0 399.35 115.23 650.40 o 21 8 0 1181.67 1050.53 442.11 o 22 8 0 39.45 487.41 606.29 o 23 8 0 9571.51 9747.93 941.75 o 1 9 0 11003.79 9483.93 1824.41 o 2 9 0 3073.04 4561.99 1224.82 o 3 9 0 932.90 2150.17 1657.03 o 4 9 0 388.50 773.53 811.16 o 5 9 0 6020.77 5877.93 1217.06 o 6 9 0 6609.39 7709.77 1236.98 o 7 9 0 94.70 221.46 1341.34 o 8 9 0 5849.35 7335.50 1606.67 o 9 9 0 32.42 193.02 770.11 o 10 9 0 7347.16 10777.37 1607.54 o 11 9 0 2200.87 2654.04 1048.10 o 12 9 0 148.17 -143.83 685.88 o 13 9 0 7267.40 9940.32 1128.13 o 14 9 0 14729.07 17854.69 1848.75 o 15 9 0 92814.62 95221.16 3001.23 o 16 9 0 3790.98 4172.91 1066.17 o 17 9 0 50345.22 49113.75 1732.26 o 18 9 0 98.32 -107.58 630.20 o 19 9 0 10042.06 10770.20 977.37 o 20 9 0 210.49 624.55 614.77 o 21 9 0 14305.26 10758.87 2004.22 o 22 9 0 1650.14 1271.09 963.03 o 0 10 0 16688.64 17762.33 2915.44 o 1 10 0 3995.48 3444.30 1003.36 o 2 10 0 6492.18 7100.83 1467.70 o 3 10 0 2476.99 2137.23 1050.91 o 4 10 0 59.17 601.93 1162.82 o 5 10 0 89067.99 90408.04 2700.21 o 6 10 0 1824.41 4311.68 2972.56 o 7 10 0 25711.26 24525.70 2445.86 o 8 10 0 865.50 280.01 984.78 o 9 10 0 40994.98 36796.80 1964.66 o 10 10 0 3776.12 6931.76 2128.41 o 11 10 0 7287.36 10257.82 1324.36 o 12 10 0 458.85 2512.78 1028.79 o 13 10 0 149.75 -233.57 953.00 o 14 10 0 4616.29 5488.30 1672.24 o 15 10 0 127.31 -498.73 1032.53 o 16 10 0 10149.67 8986.62 1078.35 o 17 10 0 243.14 1041.53 934.42 o 18 10 0 0.06 367.62 689.98 o 19 10 0 1317.66 1088.95 695.15 o 20 10 0 284.72 78.84 707.74 o 1 11 0 277.90 788.53 1622.42 o 2 11 0 228.19 -144.43 1029.78 o 3 11 0 30901.94 29283.17 1510.27 o 4 11 0 886.68 1749.39 1791.00 o 5 11 0 6546.93 9650.15 1728.73 o 6 11 0 262.34 -477.32 911.24 o 7 11 0 15992.65 16123.71 1648.92 o 8 11 0 867.47 894.35 1173.95 o 9 11 0 32954.23 32168.57 1983.30 o 10 11 0 3949.14 2362.21 1218.94 o 11 11 0 28391.83 32009.59 1622.91 o 12 11 0 8263.85 11552.61 2102.67 o 13 11 0 7546.22 8975.60 1430.57 o 14 11 0 73.58 430.68 1520.13 o 15 11 0 2845.69 3959.32 1078.07 o 16 11 0 8487.51 7863.56 1770.49 o 17 11 0 3885.92 3775.95 1140.00 o 1 12 0 1858.65 3251.97 1472.12 o 2 12 0 2965.95 7727.42 2204.07 o 3 12 0 3048.53 1546.33 1826.11 o 4 12 0 12.55 -755.44 826.58 o 5 12 0 52.88 714.84 1196.27 o 6 12 0 8.50 -277.40 1172.53 o 7 12 0 498.80 1548.28 1340.90 o 8 12 0 2070.76 2828.34 1607.13 o 9 12 0 708.94 1133.79 1128.00 o 10 12 0 16.11 -869.87 1399.75 o 11 12 0 1413.69 2117.83 971.21 o 12 12 0 5822.21 8689.10 1011.87 o 13 12 0 21149.50 25460.04 4005.16 o 14 12 0 6950.17 8014.13 1542.79 o 1 13 0 796.22 2427.77 1977.09 o 2 13 0 564.31 -717.15 1973.80 o 3 13 0 11981.76 13950.74 1719.27 o 4 13 0 258.15 185.29 1499.85 o 5 13 0 61.69 -953.03 816.62 o 6 13 0 1446.30 1981.73 1276.94 o 7 13 0 25156.68 22574.83 2455.51 o 8 13 0 53.03 684.53 825.34 o 9 13 0 1979.61 2165.77 1373.70 o -29 1 1 3275.33 3076.24 980.94 o -28 1 1 325.76 3026.08 1059.23 o -27 1 1 12704.44 10480.33 1200.12 o -26 1 1 666.70 330.37 737.83 o -25 1 1 70.67 -334.69 476.50 o -24 1 1 3065.88 4570.10 836.92 o -23 1 1 15268.38 15678.10 785.87 o -22 1 1 10712.14 10800.51 648.08 o -21 1 1 8816.02 9608.97 634.88 o -20 1 1 1814.70 1902.77 522.12 o -19 1 1 1599.42 2183.25 534.71 o -18 1 1 19494.83 21107.37 671.79 o -17 1 1 5359.86 6919.40 630.72 o -16 1 1 44188.00 46042.53 991.81 o -15 1 1 1495.77 1930.89 494.41 o -14 1 1 17588.01 18322.87 672.30 o -13 1 1 1199.08 977.08 362.51 o -12 1 1 106.71 467.53 402.50 o -11 1 1 1491.18 1302.10 324.42 o -10 1 1 47156.15 41853.14 837.47 o -9 1 1 1316.75 1778.18 348.84 o -8 1 1 177605.83 182249.84 2125.02 o -7 1 1 3444.76 3639.49 461.96 o -6 1 1 7018.49 5342.74 382.90 o -5 1 1 1185.14 1211.91 384.48 o -4 1 1 175520.95 184728.77 2239.82 o 3 1 1 4020.73 3038.89 909.70 o 4 1 1 387128.91 425926.47 6275.71 o 5 1 1 7567.67 7366.30 577.63 o 6 1 1 120283.42 113128.01 1341.71 o 7 1 1 2513.85 2283.02 314.59 o 8 1 1 267.75 1604.71 374.49 o 9 1 1 2804.66 2257.31 486.65 o 10 1 1 2221.63 1939.89 400.69 o 11 1 1 3.47 286.28 312.01 o 12 1 1 6272.12 7180.45 453.54 o 13 1 1 8174.64 7738.78 512.66 o 14 1 1 57116.75 60652.09 1074.22 o 15 1 1 12722.22 12277.75 633.24 o 16 1 1 8771.59 9747.53 529.86 o 17 1 1 2770.73 2412.30 608.12 o 18 1 1 376.01 801.69 382.91 o 19 1 1 1990.04 2308.02 441.11 o 20 1 1 6997.10 8631.34 704.26 o 21 1 1 6705.43 7729.17 629.58 o 22 1 1 30028.48 31370.37 1100.96 o 23 1 1 7298.53 7989.20 708.83 o 24 1 1 13014.72 13765.10 607.96 o 25 1 1 109.10 258.42 848.29 o 26 1 1 188.95 491.90 683.63 o 27 1 1 3620.82 4190.98 756.09 o 28 1 1 324.80 -478.68 1334.45 o -29 2 1 23.36 377.37 627.80 o -28 2 1 0.95 255.30 568.43 o -27 2 1 3368.71 4920.83 632.50 o -26 2 1 20356.70 20860.87 1081.56 o -25 2 1 10638.42 10182.69 1226.72 o -24 2 1 509.67 1047.74 705.78 o -23 2 1 2378.36 1803.49 568.25 o -22 2 1 24589.63 25532.60 954.62 o -21 2 1 1292.08 1264.44 720.14 o -20 2 1 59460.48 60642.22 1274.02 o -19 2 1 94.90 160.43 557.15 o -18 2 1 32559.45 35671.30 922.06 o -17 2 1 5586.56 6599.64 657.52 o -16 2 1 111.21 107.19 418.96 o -15 2 1 610.76 449.64 540.92 o -14 2 1 43944.77 45380.89 869.96 o -13 2 1 103.34 -75.37 459.14 o -12 2 1 3747.79 2578.93 418.35 o -11 2 1 1493.69 2730.40 540.41 o -10 2 1 114748.05 109863.23 2394.83 o -9 2 1 486.69 23.68 492.36 o -8 2 1 125.40 550.93 450.63 o -7 2 1 27334.42 24157.31 742.18 o -6 2 1 249970.34 256501.69 4380.85 o -5 2 1 20142.02 20334.90 1023.13 o -4 2 1 48556.25 49280.41 1056.61 o -3 2 1 3343.50 3395.71 477.57 o -2 2 1 3476.92 4626.37 552.88 o -1 2 1 59.96 -56.03 455.08 o 0 2 1 14138.05 14340.11 530.20 o 1 2 1 564.28 411.48 376.27 o 2 2 1 106023.11 108901.91 1723.71 o 3 2 1 6335.42 5823.02 662.01 o 4 2 1 1638.79 1716.66 556.89 o 5 2 1 4248.17 3481.43 740.44 o 6 2 1 468.32 338.60 546.84 o 7 2 1 555.36 500.61 705.33 o 8 2 1 291.46 1053.27 593.30 o 9 2 1 805.09 534.63 342.45 o 10 2 1 25539.27 23631.89 579.55 o 11 2 1 13741.51 13414.48 655.54 o 12 2 1 87781.23 87014.18 1404.55 o 13 2 1 21772.85 23618.51 658.85 o 14 2 1 3478.84 4347.61 502.74 o 15 2 1 6593.98 6219.89 730.55 o 16 2 1 25595.64 27440.53 838.35 o 17 2 1 30618.52 30669.08 1128.05 o 18 2 1 8682.12 9141.98 645.75 o 19 2 1 10270.17 9589.03 737.28 o 20 2 1 52611.05 55313.75 1226.22 o 21 2 1 59804.20 55548.76 1568.15 o 22 2 1 8895.13 10659.92 741.48 o 23 2 1 1337.06 3197.50 886.37 o 24 2 1 42315.60 41504.91 1431.95 o 25 2 1 20003.62 18848.47 831.01 o 26 2 1 52432.54 45581.29 2395.61 o 27 2 1 6741.36 6185.23 1969.26 o 28 2 1 939.42 598.18 485.80 o -28 3 1 5989.43 6839.60 848.85 o -27 3 1 476.75 1189.79 833.82 o -26 3 1 18381.86 18346.87 1491.58 o -25 3 1 55.63 293.92 649.27 o -24 3 1 9915.84 11194.22 952.31 o 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