# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 953.73 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.8109 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 22.0328 _cell_length_b 11.6648 _cell_length_c 8.0759 _cell_angle_alpha 90.000 _cell_angle_beta 103.313 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 114261.49 106209.93 11177.14 o 6 0 0 6216.62 5954.34 743.21 o 8 0 0 6964.45 6649.05 532.38 o 10 0 0 67015.00 62615.07 4896.49 o 12 0 0 347552.47 342529.03 26720.26 o 14 0 0 99776.51 104281.40 8155.62 o 16 0 0 18228.05 18762.15 1489.36 o 18 0 0 42923.74 49250.63 3878.80 o 20 0 0 42.42 0.00 189.17 o 22 0 0 18255.07 22470.31 2438.32 o 24 0 0 5576.71 7883.58 954.61 o 26 0 0 6764.40 10556.34 1237.14 o 1 1 0 318656.22 347690.31 36594.50 o 3 1 0 401.38 537.14 57.73 o 5 1 0 80919.02 72730.98 5609.54 o 7 1 0 4161.61 4005.59 252.03 o 9 1 0 407.32 480.10 50.43 o 11 1 0 41794.31 40958.10 2273.34 o 13 1 0 181438.33 208046.83 16981.21 o 15 1 0 4419.47 5319.05 311.58 o 17 1 0 63109.33 74739.69 4126.09 o 19 1 0 8385.74 10320.38 677.21 o 21 1 0 4456.22 5093.24 450.62 o 23 1 0 5258.61 7323.73 622.51 o 25 1 0 5143.54 7354.44 638.18 o 0 2 0 90117.40 103165.05 10867.98 o 2 2 0 2384.19 2943.86 159.38 o 4 2 0 184107.77 200040.94 12907.98 o 6 2 0 93043.80 95308.96 5358.06 o 8 2 0 16030.48 15587.69 783.84 o 10 2 0 17053.56 16846.58 959.83 o 12 2 0 14007.39 14628.35 827.78 o 14 2 0 23370.64 25171.36 1235.85 o 16 2 0 30496.10 35430.88 1733.11 o 18 2 0 38027.45 51285.87 4026.38 o 20 2 0 156.86 173.30 150.99 o 22 2 0 437.16 1068.08 461.20 o 24 2 0 342.23 447.00 214.20 o 26 2 0 3207.33 5070.60 488.05 o 1 3 0 35564.34 40106.16 1944.13 o 3 3 0 101233.03 113424.23 5528.31 o 5 3 0 46045.42 51648.64 2895.20 o 7 3 0 999.70 1131.07 64.53 o 9 3 0 50609.41 51137.84 2498.99 o 11 3 0 36088.98 34099.43 1937.39 o 13 3 0 3673.57 3966.81 210.81 o 15 3 0 4079.79 4686.98 246.20 o 17 3 0 5889.64 6982.39 663.54 o 19 3 0 558.11 523.91 115.76 o 21 3 0 985.86 1236.02 205.33 o 23 3 0 3054.34 3670.68 525.82 o 25 3 0 210.21 277.12 378.11 o 0 4 0 69648.68 73147.93 5684.75 o 2 4 0 75586.32 82738.57 4019.34 o 4 4 0 9708.14 10992.30 538.55 o 6 4 0 44976.43 45224.93 2260.05 o 8 4 0 5706.35 6118.66 278.42 o 10 4 0 22042.48 21936.27 934.64 o 12 4 0 35614.66 34393.15 1661.99 o 14 4 0 8457.45 7807.82 415.94 o 16 4 0 11118.39 10458.56 695.00 o 18 4 0 4613.34 6472.35 808.46 o 20 4 0 601.41 588.31 126.07 o 22 4 0 826.39 1406.13 479.41 o 24 4 0 5159.51 7853.29 1765.88 o 1 5 0 48834.74 51582.12 2228.89 o 3 5 0 18407.58 19933.56 911.89 o 5 5 0 141831.36 145458.17 7370.86 o 7 5 0 115553.41 122657.03 7898.28 o 9 5 0 12664.36 12749.23 561.15 o 11 5 0 28555.88 28968.61 1388.65 o 13 5 0 20039.56 18470.70 892.20 o 15 5 0 1443.13 1414.07 110.47 o 17 5 0 44738.71 40032.37 3106.93 o 19 5 0 28080.54 26703.96 2097.29 o 21 5 0 254.89 140.18 141.93 o 23 5 0 4550.28 5812.57 1479.22 o 0 6 0 150376.44 156089.89 10451.03 o 2 6 0 2761.35 3050.47 139.38 o 4 6 0 196732.72 198821.19 8548.14 o 6 6 0 106576.86 107078.55 5069.30 o 8 6 0 66781.34 64323.84 3274.38 o 10 6 0 1430.94 1410.46 93.39 o 12 6 0 40881.77 38188.82 1982.58 o 14 6 0 1956.89 1694.32 95.88 o 16 6 0 36200.41 31580.79 2055.77 o 18 6 0 40775.54 34537.24 2681.51 o 20 6 0 4023.72 4847.07 1023.98 o 22 6 0 3045.83 4289.84 1101.22 o 24 6 0 2176.28 2845.48 658.99 o 1 7 0 59150.93 61944.13 2678.95 o 3 7 0 22763.97 22698.50 986.08 o 5 7 0 56005.46 55471.00 2400.78 o 7 7 0 20468.26 20719.66 981.67 o 9 7 0 5808.42 5761.49 278.50 o 11 7 0 1377.73 1623.94 172.77 o 13 7 0 44426.08 40441.22 2351.06 o 15 7 0 958.06 758.66 90.19 o 17 7 0 30443.22 24902.25 2050.01 o 19 7 0 5955.34 6784.54 1543.70 o 21 7 0 131.79 269.85 306.41 o 23 7 0 402.02 230.46 224.93 o 0 8 0 54572.23 54914.76 3690.42 o 2 8 0 18066.15 18819.45 899.74 o 4 8 0 2028.59 2266.11 120.93 o 6 8 0 339.72 320.08 77.95 o 8 8 0 6915.96 7310.11 392.40 o 10 8 0 1760.79 1917.55 141.39 o 12 8 0 14589.36 14363.04 748.80 o 14 8 0 43692.51 38177.54 2223.48 o 16 8 0 2000.20 1880.75 185.86 o 18 8 0 2905.95 2187.81 313.41 o 20 8 0 1827.54 2024.53 338.39 o 1 9 0 31457.16 31553.31 1939.17 o 3 9 0 2157.43 2475.20 451.19 o 5 9 0 14768.01 15206.83 945.60 o 7 9 0 38943.89 40544.98 2444.57 o 9 9 0 1186.34 1362.25 202.24 o 11 9 0 90.87 102.37 68.31 o 13 9 0 11493.47 10958.90 587.75 o 15 9 0 5883.90 5279.28 376.32 o 17 9 0 238.81 117.52 106.95 o 19 9 0 755.51 635.74 137.03 o 0 10 0 61.46 70.50 98.68 o 2 10 0 2394.21 2676.20 200.02 o 4 10 0 489.55 682.23 93.51 o 6 10 0 33314.12 36004.59 2142.98 o 8 10 0 2300.83 2078.66 164.18 o 10 10 0 11856.33 12960.05 964.91 o 12 10 0 2257.09 2440.58 250.04 o 14 10 0 750.43 676.11 156.28 o 16 10 0 1993.43 1740.99 229.08 o 18 10 0 602.85 366.86 220.42 o 1 11 0 13752.39 14474.26 895.62 o 3 11 0 7933.11 7591.21 483.89 o 5 11 0 2180.59 2221.64 177.17 o 7 11 0 7069.36 7752.93 556.65 o 9 11 0 3302.48 3944.48 348.26 o 11 11 0 23924.43 23736.50 1642.83 o 13 11 0 3249.97 3074.97 224.73 o 15 11 0 94.22 59.33 225.15 o 17 11 0 59.46 129.30 220.36 o 0 12 0 25770.40 27210.20 2350.04 o 2 12 0 8859.12 8664.32 560.22 o 4 12 0 39.68 139.66 92.58 o 6 12 0 1147.71 1275.27 195.67 o 8 12 0 1375.82 1541.64 290.24 o 10 12 0 9704.42 10897.75 1129.99 o 12 12 0 14815.05 15855.47 1284.11 o 1 13 0 3765.04 3818.28 286.74 o 3 13 0 299.24 73.06 107.36 o 5 13 0 3158.86 3189.92 244.73 o 7 13 0 905.00 1006.65 136.24 o 9 13 0 18.75 1.61 112.77 o 11 13 0 237.27 266.30 117.03 o 0 14 0 15.15 0.00 151.84 o 2 14 0 307.46 451.87 122.51 o 4 14 0 1225.20 1472.26 207.15 o 6 14 0 1811.61 1775.43 180.07 o -21 1 1 7362.04 9618.74 564.13 o -19 1 1 0.45 0.00 102.42 o -17 1 1 77.80 278.54 88.35 o -15 1 1 669.09 811.92 96.19 o -13 1 1 18103.03 20212.76 1097.49 o -11 1 1 157736.31 161570.45 8830.83 o -9 1 1 10721.21 9747.81 553.24 o -7 1 1 24502.59 24162.25 1992.47 o -5 1 1 3061.81 2948.09 173.30 o -3 1 1 34488.22 32898.14 2690.11 o -1 1 1 36479.16 43237.69 2630.08 o 1 1 1 89109.22 99338.98 7394.41 o 3 1 1 10466.10 11414.87 847.84 o 5 1 1 48190.77 47990.46 3573.07 o 7 1 1 123753.26 122725.46 9137.71 o 9 1 1 17571.36 17025.63 941.37 o 11 1 1 10636.15 10685.18 511.59 o 13 1 1 1387.59 1649.70 94.72 o 15 1 1 1660.71 1664.11 163.15 o 17 1 1 9545.62 8708.15 841.71 o 19 1 1 49006.50 50584.41 3740.55 o 21 1 1 4287.73 4696.55 487.66 o 23 1 1 683.42 706.76 313.54 o 25 1 1 484.68 0.00 649.15 o -26 2 1 1700.88 2506.36 399.54 o -24 2 1 32784.07 48641.70 4615.52 o -20 2 1 255.70 120.77 132.99 o -18 2 1 406.85 593.89 91.27 o -16 2 1 11758.63 14089.41 815.48 o -14 2 1 64.99 87.44 51.85 o -12 2 1 157157.20 169648.83 8387.00 o -10 2 1 219786.30 216129.64 10757.64 o -8 2 1 8693.94 8817.74 449.36 o -6 2 1 123443.24 119074.36 5321.16 o -4 2 1 35420.27 37328.43 1836.55 o -2 2 1 863.42 1192.96 61.68 o 0 2 1 107664.73 113908.25 8840.42 o 2 2 1 224511.23 235797.69 14733.68 o 4 2 1 1799.13 1655.84 110.43 o 6 2 1 365797.56 386345.22 40648.73 o 8 2 1 92636.01 90015.11 4481.54 o 10 2 1 5316.79 4847.38 221.80 o 12 2 1 14766.27 14031.35 624.76 o 14 2 1 7750.90 7895.72 415.43 o 16 2 1 545.77 373.56 94.99 o 18 2 1 64866.32 67614.23 5705.41 o 20 2 1 56363.62 52845.88 5594.10 o 22 2 1 65.32 108.69 163.49 o 24 2 1 6278.80 7358.55 1572.57 o -25 3 1 12037.92 18113.42 2183.89 o -23 3 1 15113.01 20104.53 1577.02 o -21 3 1 365.95 493.85 329.06 o -19 3 1 4634.83 6242.50 396.45 o -17 3 1 42283.23 45888.13 2583.26 o -15 3 1 32665.78 33628.29 1888.51 o -13 3 1 30792.71 33068.26 1601.43 o -11 3 1 177265.59 169880.83 8448.77 o -9 3 1 34937.65 32325.01 1623.57 o -7 3 1 168510.75 166143.81 7457.63 o -5 3 1 183920.48 184945.23 8994.48 o -3 3 1 328.60 495.08 31.89 o -1 3 1 1564.14 1830.03 124.42 o 1 3 1 275232.13 293430.69 18905.89 o 3 3 1 192784.44 210126.36 13548.66 o 5 3 1 218458.48 238685.45 15388.42 o 7 3 1 251636.42 260064.23 15007.49 o 9 3 1 1981.22 1747.54 85.53 o 11 3 1 27717.50 25335.55 1117.76 o 13 3 1 47674.59 45063.33 2317.83 o 15 3 1 25237.54 25070.26 1373.30 o 17 3 1 19636.92 20371.11 1814.04 o 19 3 1 37526.64 33715.73 3576.87 o 21 3 1 2844.62 4201.21 762.62 o 23 3 1 11235.14 13654.90 2330.55 o 25 3 1 9705.84 12740.17 3431.46 o -24 4 1 7430.76 10874.60 2314.12 o -22 4 1 79.19 0.00 135.56 o -20 4 1 21242.14 23858.58 1552.32 o -18 4 1 14298.76 17355.56 1127.17 o -16 4 1 36517.72 36680.76 2073.65 o -14 4 1 30334.74 28216.95 1598.80 o -12 4 1 62805.55 60873.97 2808.19 o -10 4 1 58132.91 55300.57 2768.36 o -8 4 1 69333.91 67914.14 3040.20 o -6 4 1 151059.02 155635.80 6969.11 o -4 4 1 13192.27 14256.49 635.31 o -2 4 1 5257.94 5567.51 310.89 o 0 4 1 42338.86 45164.03 2910.22 o 2 4 1 254893.98 226440.31 29773.74 o 4 4 1 853.22 900.85 53.96 o 6 4 1 168943.31 177018.75 9333.23 o 8 4 1 35756.85 37132.24 1765.47 o 10 4 1 47104.24 46351.09 2034.76 o 12 4 1 38067.52 36139.40 1570.06 o 14 4 1 40832.45 35192.95 2105.75 o 16 4 1 27304.06 23425.61 1578.15 o 18 4 1 10541.11 11630.00 1923.82 o 20 4 1 17547.80 15563.18 1673.31 o 22 4 1 9932.16 8977.97 1001.77 o 24 4 1 23124.61 21539.32 2326.05 o -25 5 1 431.03 1136.89 445.33 o -23 5 1 1263.91 1761.94 193.95 o -21 5 1 9578.00 12490.56 1493.38 o -19 5 1 12650.24 12519.77 723.62 o -17 5 1 2020.13 1942.82 168.24 o -15 5 1 30654.28 28794.26 1632.18 o -13 5 1 2575.77 2487.98 131.84 o -11 5 1 65681.19 61598.61 2877.49 o -9 5 1 5778.74 5218.25 239.33 o -7 5 1 89708.56 88411.07 3565.89 o -5 5 1 1689.62 1973.66 94.63 o -3 5 1 9860.70 11437.87 536.88 o -1 5 1 790.25 969.95 133.72 o 1 5 1 49785.42 52355.02 2486.51 o 3 5 1 36374.75 36443.26 1947.29 o 5 5 1 7740.39 7725.67 375.19 o 7 5 1 36596.07 37622.88 1785.26 o 9 5 1 5940.90 6163.12 300.16 o 11 5 1 22679.70 22397.72 1057.24 o 13 5 1 1613.56 1283.32 91.96 o 15 5 1 25648.35 22051.08 1487.65 o 17 5 1 14205.51 13151.28 1034.52 o 19 5 1 11588.67 9590.43 1042.59 o 21 5 1 18.51 74.29 155.62 o 23 5 1 11110.82 13085.89 2768.53 o -24 6 1 2151.33 2525.64 259.60 o -22 6 1 3102.31 4311.95 659.43 o -20 6 1 2088.87 2787.75 677.97 o -18 6 1 2347.28 2605.10 201.67 o -16 6 1 577.03 598.39 68.74 o -14 6 1 8.96 68.56 44.55 o -12 6 1 1055.85 1221.74 96.77 o -10 6 1 447.57 446.10 45.38 o -8 6 1 14592.68 15165.11 613.32 o -6 6 1 32.14 11.05 24.96 o -4 6 1 24533.85 24744.20 1071.69 o -2 6 1 646.62 660.53 42.52 o 0 6 1 21372.13 21956.52 1051.81 o 2 6 1 13194.89 13740.46 707.31 o 4 6 1 4066.81 4183.99 212.57 o 6 6 1 16665.15 17406.68 827.74 o 8 6 1 3303.54 3602.59 181.84 o 10 6 1 235.49 231.53 41.46 o 12 6 1 7840.98 8105.67 428.28 o 14 6 1 30.11 0.00 54.81 o 16 6 1 6021.08 6213.37 609.15 o 18 6 1 14.37 0.00 92.62 o 20 6 1 2366.12 2000.26 253.88 o 22 6 1 123.03 196.72 203.26 o -23 7 1 339.67 475.96 290.22 o -21 7 1 1612.89 2119.22 326.11 o -19 7 1 10324.59 9271.70 809.98 o -17 7 1 24189.83 21600.52 1221.74 o -15 7 1 6845.43 6965.26 542.33 o -13 7 1 29.99 73.77 42.37 o -11 7 1 2226.11 2424.25 155.26 o -9 7 1 102.02 290.19 77.36 o -7 7 1 3642.23 3630.85 170.31 o -5 7 1 43131.99 42535.65 1987.06 o -3 7 1 24895.17 25909.89 1126.27 o -1 7 1 39664.41 41439.74 1971.90 o 1 7 1 35890.14 35876.25 1916.40 o 3 7 1 2204.84 2355.70 140.21 o 5 7 1 554.96 974.09 155.37 o 7 7 1 5624.80 6184.53 339.53 o 9 7 1 4061.13 3944.49 218.49 o 11 7 1 36814.18 37803.27 1997.87 o 13 7 1 38714.66 37787.83 2248.24 o 15 7 1 207.45 110.87 68.82 o 17 7 1 2009.08 2121.52 286.33 o 19 7 1 45.69 22.64 143.89 o 21 7 1 3554.93 3760.22 452.58 o -22 8 1 1086.78 1247.94 186.27 o -20 8 1 468.63 331.38 129.12 o -18 8 1 16861.98 14990.40 1010.11 o -16 8 1 23622.45 21288.27 1385.29 o -14 8 1 943.99 1114.81 88.98 o -12 8 1 4365.78 4396.07 285.90 o -10 8 1 12859.57 13248.97 628.29 o -8 8 1 410.00 516.23 108.81 o -6 8 1 44584.10 44048.49 2087.27 o -4 8 1 47148.30 47698.93 2257.50 o -2 8 1 618.64 718.15 52.52 o 0 8 1 36400.83 36632.77 1942.30 o 2 8 1 28004.51 27968.15 1486.38 o 4 8 1 251.18 203.29 40.95 o 6 8 1 28158.10 29223.59 1546.59 o 8 8 1 8935.63 8891.41 481.84 o 10 8 1 2996.82 3686.99 209.79 o 12 8 1 35954.32 36720.50 2180.60 o 14 8 1 22650.28 21313.66 1274.14 o 16 8 1 21.72 61.39 80.93 o 18 8 1 3894.96 3491.69 456.98 o 20 8 1 592.93 393.54 173.12 o -21 9 1 497.06 512.27 224.94 o -19 9 1 943.96 564.24 232.04 o -17 9 1 13781.70 11899.44 1006.31 o -15 9 1 1726.39 1589.69 154.14 o -13 9 1 9253.56 8758.22 835.38 o -11 9 1 20274.66 18659.97 1288.20 o -9 9 1 8504.52 9665.26 880.01 o -7 9 1 18273.23 17714.49 1082.28 o -5 9 1 44956.51 44967.39 2386.53 o -3 9 1 313.21 270.39 53.20 o -1 9 1 9475.67 9678.02 521.86 o 1 9 1 34153.45 34561.39 1987.43 o 3 9 1 16588.23 15934.71 855.99 o 5 9 1 32319.88 34035.43 1794.34 o 7 9 1 32851.49 33435.40 1758.15 o 9 9 1 287.80 290.57 56.28 o 11 9 1 3578.31 3831.54 248.29 o 13 9 1 19495.49 18890.10 1125.67 o 15 9 1 2217.27 1955.20 256.35 o 17 9 1 6849.43 6256.77 548.78 o 19 9 1 7122.44 5590.41 470.64 o -18 10 1 95.39 44.78 189.17 o -16 10 1 33.55 0.00 106.25 o -14 10 1 22.07 5.38 164.91 o -12 10 1 23256.82 20166.89 1411.36 o -10 10 1 18283.54 17931.67 1248.18 o -8 10 1 2343.24 2391.40 246.15 o -6 10 1 5088.00 4855.72 326.98 o -4 10 1 713.86 579.43 91.90 o -2 10 1 1002.29 1029.93 109.82 o 0 10 1 7627.82 7664.67 486.90 o 2 10 1 17726.84 17880.19 1257.62 o 4 10 1 4.11 0.00 74.27 o 6 10 1 19742.88 21523.15 1295.93 o 8 10 1 21044.86 21221.98 1270.12 o 10 10 1 57.61 423.49 158.34 o 12 10 1 461.63 210.79 111.75 o 14 10 1 585.61 417.27 125.85 o 16 10 1 333.50 182.80 155.68 o 18 10 1 8499.65 6491.75 811.28 o -17 11 1 2910.21 2578.47 388.94 o -15 11 1 143.49 6.73 109.21 o -13 11 1 1556.05 1312.53 138.67 o -11 11 1 18741.31 16860.12 1171.27 o -9 11 1 26.11 118.01 103.33 o -7 11 1 6323.35 5810.35 447.71 o -5 11 1 443.35 663.33 100.90 o -3 11 1 413.06 306.38 84.97 o -1 11 1 388.74 520.76 157.01 o 1 11 1 4697.98 4346.42 301.02 o 3 11 1 2290.28 2363.25 188.40 o 5 11 1 3262.16 3392.98 260.61 o 7 11 1 10211.22 9914.06 619.50 o 9 11 1 243.22 101.38 87.60 o 11 11 1 78.84 113.38 234.49 o 13 11 1 2361.34 2559.04 275.97 o 15 11 1 920.28 491.80 209.89 o -14 12 1 112.88 287.14 114.87 o -12 12 1 55.48 30.35 101.64 o -10 12 1 227.29 272.75 125.20 o -8 12 1 2735.36 2740.11 215.49 o -6 12 1 117.18 158.85 95.68 o -4 12 1 6428.18 7123.14 463.57 o -2 12 1 600.07 623.34 109.04 o 0 12 1 7177.76 8815.21 747.89 o 2 12 1 3689.90 3748.90 266.24 o 4 12 1 1760.40 2078.88 262.21 o 6 12 1 3086.52 2676.24 254.43 o 8 12 1 1294.98 1867.84 330.62 o 10 12 1 81.50 61.91 134.66 o 12 12 1 4148.02 5105.75 418.90 o -11 13 1 593.18 807.03 164.04 o -9 13 1 2091.20 2541.53 245.48 o -7 13 1 2053.59 2306.40 317.08 o -5 13 1 4740.72 5772.50 555.91 o -3 13 1 3274.06 3671.21 277.56 o -1 13 1 8581.39 8575.39 559.88 o 1 13 1 2887.88 3698.48 414.89 o 3 13 1 5229.29 5633.97 388.45 o 5 13 1 77.24 0.00 106.06 o 7 13 1 594.33 887.48 133.25 o 9 13 1 5469.88 5757.02 551.89 o -6 14 1 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