Acta Cryst. (2006). E62, m469-m471  [ doi:10.1107/S1600536806003904 ]

catena-Poly[tributyltin(IV)--acetato]

M. A. Saeed, A. Badshah, M. K. Rauf, D. C. Craig and S. Ali

Online 8 February 2006

Key indicators

• Single-crystal X-ray study
• T = 294 K
• Mean (C-C) = 0.016 Å
• Disorder in main residue
• R factor = 0.053
• wR factor = 0.060
• Data-to-parameter ratio = 19.0

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT241_ALERT_2_A Check High      Ueq as Compared to Neighbors for        C16     

PLAT241_ALERT_2_A Check High      Ueq as Compared to Neighbors for       C16'     

Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.90 Ratio 
PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for         C4     

PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for        C4'     

PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for        C20     

PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for       C20'     

PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        C15     
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for       C15'     
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        C19     

Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT150_ALERT_1_C Volume as Calculated Differs from that Given ...    3599.00 Ang-3 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.78 Ratio 
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Sn1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Sn2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for      C1AC1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C3     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for      C1AC2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C10     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C13     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      13.00 Perc. 
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         16       
PLAT360_ALERT_2_C Short  C(sp3)-C(sp3) Bond  C11    -   C12    ...       1.43 Ang.  
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety      C2AC1     
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety      C2AC2     
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........         90       
PLAT731_ALERT_1_C Bond    Calc     1.43(3), Rep   1.430(12) ......       2.50 su-Rat
              C11  -C12     1.555   1.555                                       
PLAT731_ALERT_1_C Bond    Calc     1.50(2), Rep    1.501(9) ......       2.22 su-Rat
              C23  -C24     1.555   1.555                                       

   2 ALERT level A = In general: serious problem
   8 ALERT level B = Potentially serious problem
  20 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  18 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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