Acta Cryst. (2006). E62, m426-m428  [ doi:10.1107/S1600536806003011 ]

[1,1'-Bis(diphenylphosphino)cobaltocenium-²P,P']chloro(⁵-pentamethylcyclopentadienyl)ruthenium(II) hexafluorophosphate dichloromethane hemisolvate

X.-H. Wu, Y. Ren, G.-A. Yu and S.-H. Liu

Online 3 February 2006

Key indicators

• Single-crystal X-ray study
• T = 292 K
• Mean (C-C) = 0.006 Å
• R factor = 0.049
• wR factor = 0.144
• Data-to-parameter ratio = 18.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT231_ALERT_4_C Hirshfeld Test (Solvent)   P3     -   F5      ..       5.82 su    
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for         P3     
PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor ....       2.63       
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety         C1     
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      46.00 A   3  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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