Acta Cryst. (2006). E62, m535-m537  [ doi:10.1107/S1600536806004958 ]

trans-Dichlorobis(10-dodecyl-9-phospha-10-silatriptycene-P)palladium(II)

H. Tsuji, T. Inoue, S. Sase and K. Tamao

Online 17 February 2006

Key indicators

• Single-crystal X-ray study
• T = 103 K
• Mean (C-C) = 0.004 Å
• R factor = 0.034
• wR factor = 0.080
• Data-to-parameter ratio = 16.4

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          3     
            P1  -PD1 -P1  -C1     15.00  0.00   2.757   1.555   1.555   1.555   
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          6     
            P1  -PD1 -P1  -C13     3.00  0.00   2.757   1.555   1.555   1.555   
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          9     
            P1  -PD1 -P1  -C7      9.00  0.00   2.757   1.555   1.555   1.555   
PLAT732_ALERT_1_C Angle   Calc    82.77(2), Rep    82.77(5) ......       2.50 su-Rat
              CL1  -PD1  -P1      1.555   1.555   1.555                         

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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