Acta Cryst. (2006). E62, i64-i65  [ doi:10.1107/S1600536806005666 ]

Partial Pd occupancy in uranium palladium diantimonide, UPd_0.603(6)Sb₂

S. Bobev, D. J. Mixson, E. D. Bauer and J. L. Sarrao

Online 22 February 2006

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean () = 0.000 Å
• Disorder in main residue
• R factor = 0.020
• wR factor = 0.047
• Data-to-parameter ratio = 11.5

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT301_ALERT_3_B Main Residue  Disorder .........................      32.00 Perc. 

Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)...          ?
PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms ..          ?

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   4 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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