# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 225.40 _exptl_crystal_F_000 1060.00 _reflns_d_resolution_high 0.7799 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.1623 _cell_length_b 13.2460 _cell_length_c 17.4853 _cell_angle_alpha 111.712 _cell_angle_beta 100.538 _cell_angle_gamma 92.334 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6922.77 7032.75 70.61 o 3 0 0 1140.82 978.96 19.87 o 4 0 0 2.93 5.21 8.96 o 5 0 0 1360.12 1450.03 29.23 o 6 0 0 3519.89 3632.99 53.44 o 7 0 0 1845.90 1837.88 47.28 o 8 0 0 85.90 60.97 20.50 o 9 0 0 1096.45 996.75 33.61 o 10 0 0 57.34 61.16 19.40 o 11 0 0 4.66 -24.45 56.68 o 12 0 0 26.48 -7.20 31.98 o 13 0 0 0.50 8.94 41.58 o 14 0 0 100.55 39.40 46.14 o -15 1 0 5.88 3.53 112.42 o -14 1 0 217.69 145.32 65.04 o -13 1 0 518.52 552.21 125.30 o -12 1 0 170.60 112.98 38.28 o -11 1 0 265.50 293.46 79.10 o -10 1 0 1330.12 1294.01 39.30 o -9 1 0 218.67 258.09 41.14 o -8 1 0 6.69 11.58 14.99 o -7 1 0 34.55 52.31 14.04 o -6 1 0 96.27 110.10 16.53 o -5 1 0 377.72 331.03 17.50 o -4 1 0 498.12 527.19 17.88 o -3 1 0 1834.42 1969.96 28.63 o -2 1 0 2799.36 3057.69 66.28 o -1 1 0 5082.31 4592.28 78.53 o 0 1 0 63.26 15.10 4.98 o 1 1 0 1978.80 2241.64 41.52 o 2 1 0 6203.09 6645.72 109.67 o 3 1 0 77.46 51.89 18.45 o 4 1 0 173.49 122.58 22.57 o 5 1 0 617.00 517.37 19.35 o 6 1 0 26.76 18.39 11.58 o 7 1 0 2263.76 2292.41 44.14 o 8 1 0 104.76 117.74 18.83 o 9 1 0 555.32 571.01 40.75 o 10 1 0 137.27 109.56 31.03 o 11 1 0 101.10 56.94 33.63 o 12 1 0 1.16 -29.43 34.67 o 13 1 0 147.77 61.20 42.41 o 14 1 0 467.71 346.67 64.88 o -15 2 0 77.11 51.07 119.17 o -14 2 0 12.83 -83.10 104.02 o -13 2 0 20.27 8.83 57.35 o -12 2 0 415.63 461.29 79.83 o -11 2 0 0.31 -22.38 37.92 o -10 2 0 0.89 -13.12 17.14 o -9 2 0 900.86 783.09 29.89 o -8 2 0 206.62 236.48 25.89 o -7 2 0 29.62 11.05 11.93 o -6 2 0 2882.21 3158.33 47.42 o -5 2 0 124.75 156.11 13.43 o -4 2 0 157.57 217.96 13.68 o -3 2 0 93.47 85.29 9.10 o -2 2 0 10699.80 11825.90 264.35 o -1 2 0 3494.16 3655.67 68.67 o 0 2 0 16135.56 16301.94 269.77 o 1 2 0 262.44 308.57 15.52 o 2 2 0 5296.31 6038.12 104.64 o 3 2 0 2907.01 3056.02 67.11 o 4 2 0 187.94 215.66 23.88 o 5 2 0 461.62 593.53 32.86 o 6 2 0 5452.61 5140.13 112.68 o 7 2 0 4306.56 4370.75 106.09 o 8 2 0 42.85 24.24 25.33 o 9 2 0 1725.16 1606.75 69.29 o 10 2 0 5.30 -28.60 28.60 o 11 2 0 154.13 155.92 40.64 o 12 2 0 24.39 -10.43 36.13 o 13 2 0 57.56 39.71 44.95 o 14 2 0 34.64 32.44 50.09 o -15 3 0 7.93 92.03 120.78 o -14 3 0 193.20 159.35 109.36 o -13 3 0 356.49 263.47 110.66 o -12 3 0 18.53 0.99 88.65 o -11 3 0 3.26 -11.22 25.38 o -10 3 0 1631.91 1679.51 43.17 o -9 3 0 233.72 230.59 22.43 o -8 3 0 3562.89 3465.79 65.30 o -7 3 0 122.56 105.33 15.45 o -6 3 0 1555.61 1842.80 34.63 o -5 3 0 937.18 975.90 25.35 o -4 3 0 4719.19 4739.66 55.72 o -3 3 0 17.85 19.78 6.86 o -2 3 0 39.60 88.65 17.13 o -1 3 0 2585.30 2639.53 36.08 o 0 3 0 45264.27 49435.94 517.64 o 1 3 0 4685.29 4538.61 80.76 o 2 3 0 3464.01 3569.09 72.61 o 3 3 0 1265.65 1265.63 41.42 o 4 3 0 4825.24 4759.20 99.14 o 5 3 0 16.36 -3.74 16.25 o 6 3 0 498.39 545.88 36.64 o 7 3 0 2768.70 2747.71 82.63 o 8 3 0 1065.13 1061.70 55.12 o 9 3 0 954.29 943.52 56.42 o 10 3 0 367.94 333.59 49.52 o 11 3 0 925.62 962.05 61.09 o 12 3 0 229.18 158.10 46.19 o 13 3 0 7.39 -3.01 41.52 o 14 3 0 1.60 -2.70 48.95 o -15 4 0 79.01 -15.36 122.86 o -14 4 0 27.92 49.15 110.35 o -13 4 0 325.02 160.59 104.43 o -12 4 0 170.78 7.84 89.33 o -11 4 0 475.17 624.67 103.39 o -10 4 0 46.24 44.32 28.12 o -9 4 0 418.78 428.75 45.48 o -8 4 0 238.69 276.77 22.19 o -7 4 0 78.04 53.55 14.04 o -6 4 0 439.63 389.77 28.67 o -5 4 0 754.77 783.30 28.92 o -4 4 0 1383.69 1450.96 26.45 o -3 4 0 6443.23 6286.80 123.32 o -2 4 0 292.21 295.54 26.21 o -1 4 0 14900.08 15703.23 174.28 o 0 4 0 2597.19 2962.20 44.04 o 1 4 0 2646.13 2370.36 53.10 o 2 4 0 112.17 152.86 19.78 o 3 4 0 794.00 817.91 35.71 o 4 4 0 294.61 294.50 28.96 o 5 4 0 55.62 28.70 19.88 o 6 4 0 2029.65 1813.90 63.84 o 7 4 0 173.90 119.38 31.25 o 8 4 0 1635.98 1576.90 67.99 o 9 4 0 946.24 952.75 57.93 o 10 4 0 18.15 81.28 37.73 o 11 4 0 1.12 -13.65 34.36 o 12 4 0 182.21 173.72 50.45 o 13 4 0 48.93 44.07 44.69 o 14 4 0 8.54 29.17 55.43 o -15 5 0 44.75 -5.19 127.58 o -14 5 0 1.21 -92.44 95.92 o -13 5 0 60.55 47.91 94.93 o -12 5 0 55.30 26.32 88.81 o -11 5 0 107.85 -0.05 77.03 o -10 5 0 31.95 16.91 40.41 o -9 5 0 56.85 33.95 27.22 o -8 5 0 821.40 831.82 45.61 o -7 5 0 1.63 -12.56 12.56 o -6 5 0 804.01 821.81 22.90 o -5 5 0 2333.26 2275.41 34.76 o -4 5 0 2511.93 2567.75 71.37 o -3 5 0 778.55 806.44 38.98 o -2 5 0 1610.55 1510.00 51.54 o -1 5 0 914.53 916.70 21.07 o 0 5 0 2420.41 2402.19 41.55 o 1 5 0 1452.53 1352.29 31.24 o 2 5 0 6224.23 6361.90 118.91 o 3 5 0 4.70 -10.12 14.79 o 4 5 0 1562.62 1427.00 51.70 o 5 5 0 982.78 942.06 45.21 o 6 5 0 13.37 20.55 22.16 o 7 5 0 1403.35 1211.08 57.98 o 8 5 0 8.29 -17.28 26.57 o 9 5 0 100.64 114.19 37.06 o 10 5 0 53.03 43.18 36.54 o 11 5 0 355.95 299.18 53.46 o 12 5 0 59.75 5.61 41.16 o 13 5 0 13.86 44.22 48.84 o -14 6 0 8.92 -106.72 106.72 o -13 6 0 443.72 258.59 106.35 o -12 6 0 862.83 729.93 122.34 o -11 6 0 9.91 3.17 74.85 o -10 6 0 442.94 486.69 81.70 o -9 6 0 1.97 22.98 28.03 o -8 6 0 17.47 9.96 26.66 o -7 6 0 138.39 145.51 28.71 o -6 6 0 358.30 402.18 34.18 o -5 6 0 28.51 62.96 24.65 o -4 6 0 780.94 826.94 44.01 o -3 6 0 12.69 -17.23 17.23 o -2 6 0 1629.39 1721.82 59.48 o -1 6 0 607.96 543.30 23.38 o 0 6 0 8.81 4.66 9.83 o 1 6 0 1662.42 1851.13 39.12 o 2 6 0 107.28 127.61 16.28 o 3 6 0 9.27 4.00 16.71 o 4 6 0 386.32 394.68 32.86 o 5 6 0 39.74 43.44 22.99 o 6 6 0 57.75 98.57 29.17 o 7 6 0 12.42 -23.15 23.15 o 8 6 0 58.15 44.90 30.73 o 9 6 0 711.57 690.64 55.90 o 10 6 0 1.59 -35.35 35.35 o 11 6 0 252.70 233.05 51.59 o 12 6 0 92.06 60.57 46.82 o 13 6 0 0.18 -49.36 49.36 o -14 7 0 102.11 6.07 106.20 o -13 7 0 324.58 180.94 105.52 o -12 7 0 133.01 -34.57 84.40 o -11 7 0 476.04 498.85 108.43 o -10 7 0 350.15 515.57 97.97 o -9 7 0 76.86 79.83 32.70 o -8 7 0 2.63 -24.38 24.38 o -7 7 0 111.11 142.86 31.35 o -6 7 0 0.35 -13.69 29.30 o -5 7 0 4.70 -11.99 22.53 o -4 7 0 77.32 137.86 29.48 o -3 7 0 404.81 417.73 35.92 o -2 7 0 406.19 361.37 15.68 o -1 7 0 2756.75 2772.90 47.21 o 0 7 0 15.43 19.46 11.43 o 1 7 0 656.52 533.13 23.95 o 2 7 0 1365.92 1244.59 36.16 o 3 7 0 211.53 211.49 47.23 o 4 7 0 206.18 219.61 31.77 o 5 7 0 387.72 404.75 35.97 o 6 7 0 1099.09 946.94 52.73 o 7 7 0 51.08 29.95 29.79 o 8 7 0 1070.74 1146.67 64.05 o 9 7 0 49.06 -13.81 35.40 o 10 7 0 50.19 -13.13 37.01 o 11 7 0 0.61 -22.16 39.71 o 12 7 0 206.09 324.56 66.13 o -13 8 0 131.93 -1.04 100.02 o -12 8 0 1384.62 1388.02 122.55 o -11 8 0 322.18 251.48 100.49 o -10 8 0 590.22 493.40 97.22 o -9 8 0 3.75 -11.38 56.58 o -8 8 0 60.39 52.07 29.89 o -7 8 0 428.43 494.75 44.96 o -6 8 0 371.78 445.96 49.62 o -5 8 0 46.93 54.66 30.00 o -4 8 0 422.96 471.65 47.23 o -3 8 0 1521.59 1540.00 65.71 o -2 8 0 27.03 11.42 23.15 o -1 8 0 2746.18 2690.37 49.10 o 0 8 0 44.60 55.91 15.05 o 1 8 0 684.74 768.48 34.67 o 2 8 0 34.21 18.14 15.53 o 3 8 0 945.71 826.84 33.45 o 4 8 0 20.93 7.29 22.84 o 5 8 0 350.30 457.28 47.13 o 6 8 0 1246.69 1141.32 60.36 o 7 8 0 48.07 39.34 32.23 o 8 8 0 209.34 148.71 40.49 o 9 8 0 18.76 -28.96 34.88 o 10 8 0 3.50 46.61 44.01 o 11 8 0 429.98 472.85 68.41 o 12 8 0 157.17 159.76 55.80 o -13 9 0 109.85 16.45 105.16 o -12 9 0 195.42 89.59 97.37 o -11 9 0 578.10 483.64 110.61 o -10 9 0 61.03 -45.52 73.96 o -9 9 0 4.72 19.36 33.61 o -8 9 0 4.66 3.04 28.63 o -7 9 0 480.27 577.95 91.48 o -6 9 0 0.88 -1.87 30.52 o -5 9 0 680.02 713.11 53.05 o -4 9 0 827.50 891.82 55.80 o -3 9 0 40.34 49.62 29.43 o -2 9 0 57.06 58.29 29.64 o -1 9 0 382.83 422.97 48.12 o 0 9 0 40.18 36.27 25.85 o 1 9 0 965.06 846.49 32.91 o 2 9 0 376.21 395.94 71.21 o 3 9 0 297.32 276.93 36.36 o 4 9 0 466.48 393.10 35.66 o 5 9 0 44.61 6.86 21.64 o 6 9 0 13.74 34.88 30.36 o 7 9 0 2.35 25.48 34.05 o 8 9 0 9.05 -24.71 33.01 o 9 9 0 254.12 315.73 54.81 o 10 9 0 261.85 385.03 59.48 o 11 9 0 67.68 35.50 51.70 o -12 10 0 1.10 -76.09 93.22 o -11 10 0 0.26 -62.54 82.99 o -10 10 0 329.86 387.15 102.25 o -9 10 0 564.14 731.03 59.45 o -8 10 0 5.55 -19.14 29.65 o -7 10 0 198.69 333.74 52.73 o -6 10 0 603.50 593.84 54.19 o -5 10 0 46.45 20.87 33.06 o -4 10 0 945.41 1170.08 67.42 o -3 10 0 852.25 832.91 57.30 o -2 10 0 294.13 343.29 49.05 o -1 10 0 1125.19 1052.36 64.36 o 0 10 0 1.69 -6.80 28.50 o 1 10 0 33.31 -2.08 28.44 o 2 10 0 162.14 206.54 27.35 o 3 10 0 562.67 624.56 34.11 o 4 10 0 19.51 41.17 21.71 o 5 10 0 5.67 2.56 23.21 o 6 10 0 245.09 231.36 33.61 o 7 10 0 106.40 75.78 31.22 o 8 10 0 942.07 945.99 48.56 o 9 10 0 279.81 340.86 78.40 o 10 10 0 26.82 -14.97 36.52 o -12 11 0 162.84 208.81 111.65 o -11 11 0 779.66 960.33 137.70 o -10 11 0 63.81 55.59 84.71 o -9 11 0 914.62 927.69 56.94 o -8 11 0 1083.77 1205.46 63.89 o -7 11 0 713.96 710.88 62.65 o -6 11 0 101.07 122.96 40.69 o -5 11 0 1346.91 1358.54 75.57 o -4 11 0 1971.38 1730.38 82.63 o -3 11 0 700.11 688.56 58.13 o -2 11 0 730.96 738.96 59.17 o -1 11 0 46.36 7.06 34.52 o 0 11 0 358.05 321.13 50.45 o 1 11 0 165.69 163.97 45.05 o 2 11 0 867.82 760.29 61.20 o 3 11 0 393.47 524.13 63.74 o 4 11 0 93.55 74.43 29.77 o 5 11 0 220.49 258.17 69.84 o 6 11 0 23.70 17.81 28.60 o 7 11 0 438.12 381.04 51.96 o 8 11 0 98.89 140.16 36.60 o 9 11 0 133.25 151.02 42.63 o -11 12 0 80.03 82.22 102.10 o -10 12 0 29.61 -13.75 89.28 o -9 12 0 1277.94 1182.92 65.52 o -8 12 0 116.61 190.23 44.07 o -7 12 0 659.01 635.46 73.81 o -6 12 0 114.77 165.57 47.18 o -5 12 0 98.12 54.50 43.70 o -4 12 0 363.75 333.54 55.07 o -3 12 0 895.74 840.95 65.24 o -2 12 0 23.84 -18.69 35.45 o -1 12 0 1.27 43.60 36.70 o 0 12 0 94.93 133.50 42.30 o 1 12 0 28.55 1.61 40.80 o 2 12 0 432.33 478.87 64.10 o 3 12 0 915.32 990.59 72.61 o 4 12 0 36.80 41.78 43.44 o 5 12 0 16.21 -13.29 45.68 o 6 12 0 279.42 213.38 57.30 o 7 12 0 9.13 -18.27 31.89 o 8 12 0 105.87 172.64 40.92 o -9 13 0 3.13 -8.45 51.57 o -8 13 0 29.52 44.89 65.24 o -7 13 0 24.54 -9.91 44.17 o -6 13 0 10.12 -22.37 41.47 o -5 13 0 95.53 29.27 42.77 o -4 13 0 208.28 148.50 49.21 o -3 13 0 31.35 7.94 38.98 o -2 13 0 443.76 448.56 66.85 o -1 13 0 25.00 -5.29 40.38 o 0 13 0 22.81 40.38 49.88 o 1 13 0 160.69 178.19 53.25 o 2 13 0 575.71 728.11 80.14 o 3 13 0 16.98 22.42 44.74 o 4 13 0 132.35 105.37 52.37 o 5 13 0 2.61 2.70 47.86 o 6 13 0 4.38 12.46 54.03 o 7 13 0 119.04 87.20 63.43 o -8 14 0 6.87 6.13 45.54 o -7 14 0 193.02 184.68 59.53 o -6 14 0 27.20 -47.75 47.75 o -5 14 0 101.79 31.56 47.70 o -4 14 0 339.78 445.70 67.99 o -3 14 0 82.44 57.77 45.57 o -2 14 0 9.50 -6.49 46.51 o -1 14 0 487.50 518.47 71.94 o 0 14 0 326.96 340.28 64.31 o 1 14 0 30.40 57.51 51.28 o 2 14 0 259.25 252.41 65.76 o 3 14 0 191.40 183.33 59.64 o 4 14 0 0.28 -50.24 51.39 o 5 14 0 156.10 169.52 66.39 o -6 15 0 8.70 -33.69 52.37 o -5 15 0 44.41 89.12 63.58 o -4 15 0 0.21 -30.36 48.12 o -3 15 0 217.45 193.65 62.03 o -2 15 0 274.18 124.31 61.35 o -1 15 0 10.06 28.91 52.06 o 0 15 0 123.49 21.54 51.90 o 1 15 0 28.07 -19.78 54.03 o 2 15 0 0.22 -5.61 59.22 o -3 -15 1 46.51 60.73 61.92 o -2 -15 1 12.33 40.49 57.61 o -1 -15 1 122.05 174.24 62.65 o 0 -15 1 4.05 -45.83 46.71 o 1 -15 1 1.46 -45.31 45.31 o 2 -15 1 159.13 178.03 59.59 o 3 -15 1 109.57 102.87 54.24 o 4 -15 1 19.26 87.72 55.59 o 5 -15 1 5.18 -46.61 50.97 o 6 -15 1 15.53 -48.79 48.79 o -5 -14 1 107.02 37.22 55.85 o -4 -14 1 13.56 -12.56 52.89 o -3 -14 1 167.47 237.51 61.56 o -2 -14 1 287.88 313.81 63.89 o -1 -14 1 309.34 228.85 56.84 o 0 -14 1 257.05 197.50 56.94 o 1 -14 1 755.19 718.87 67.99 o 2 -14 1 0.28 -25.90 41.78 o 3 -14 1 253.35 271.46 55.23 o 4 -14 1 600.34 836.54 83.98 o 5 -14 1 191.14 224.54 60.88 o 6 -14 1 2.34 -41.47 44.27 o 7 -14 1 38.77 79.05 51.54 o 8 -14 1 16.03 8.77 44.35 o -7 -13 1 28.47 -19.83 53.46 o -6 -13 1 1.79 7.84 50.09 o -5 -13 1 18.34 -32.49 46.56 o -4 -13 1 64.88 102.04 50.76 o -3 -13 1 1.11 -6.49 42.61 o -2 -13 1 191.22 198.22 54.34 o -1 -13 1 694.28 651.40 64.52 o 0 -13 1 0.31 -26.89 35.92 o 1 -13 1 167.34 105.26 44.90 o 2 -13 1 47.34 60.05 39.29 o 3 -13 1 29.41 74.90 43.18 o 4 -13 1 24.62 15.31 38.36 o 5 -13 1 1.54 -10.48 40.33 o 6 -13 1 40.87 12.35 42.67 o 7 -13 1 57.04 82.94 46.51 o 8 -13 1 68.50 77.66 44.10 o 9 -13 1 21.90 -83.98 83.98 o 10 -13 1 83.12 60.73 95.24 o -8 -12 1 4.92 9.98 34.47 o -7 -12 1 5.32 -30.75 30.75 o -6 -12 1 331.49 367.35 98.93 o -5 -12 1 172.65 216.91 55.28 o -4 -12 1 0.76 15.52 38.77 o -3 -12 1 161.73 149.64 49.52 o -2 -12 1 214.49 279.71 52.63 o -1 -12 1 55.20 26.99 34.98 o 0 -12 1 67.94 94.83 39.19 o 1 -12 1 64.12 37.47 37.32 o 2 -12 1 305.04 342.88 53.36 o 3 -12 1 1539.52 1562.78 81.90 o 4 -12 1 244.22 316.93 51.54 o 5 -12 1 48.72 82.01 40.90 o 6 -12 1 704.13 678.39 61.92 o 7 -12 1 218.44 218.57 52.99 o 8 -12 1 76.08 134.52 42.08 o 9 -12 1 302.01 447.26 107.91 o 10 -12 1 135.48 215.40 95.82 o 11 -12 1 4.22 -15.73 98.15 o -9 -11 1 155.92 140.17 38.62 o -8 -11 1 356.78 355.31 88.50 o -7 -11 1 506.68 595.39 61.69 o -6 -11 1 19.11 -16.59 25.79 o -5 -11 1 239.79 291.84 35.22 o -4 -11 1 225.82 322.29 86.73 o -3 -11 1 116.79 105.98 31.74 o -2 -11 1 78.61 87.15 37.73 o -1 -11 1 781.59 784.33 59.27 o 0 -11 1 155.09 140.25 38.36 o 1 -11 1 2725.60 2587.27 98.00 o 2 -11 1 519.99 513.70 49.72 o 3 -11 1 40.40 88.81 37.99 o 4 -11 1 1640.57 1655.12 78.58 o 5 -11 1 1763.94 1863.78 84.76 o 6 -11 1 588.43 547.75 53.72 o 7 -11 1 838.13 720.53 61.82 o 8 -11 1 1249.11 1254.49 61.36 o 9 -11 1 104.05 61.30 78.06 o 10 -11 1 286.05 244.05 99.19 o 11 -11 1 1.45 5.55 86.84 o 12 -11 1 1.58 1.66 104.85 o -10 -10 1 2.84 76.30 49.41 o -9 -10 1 654.27 642.47 59.59 o -8 -10 1 389.96 477.00 60.05 o -7 -10 1 7.82 -29.84 33.74 o -6 -10 1 28.34 52.32 31.30 o -5 -10 1 5.45 -3.31 20.02 o -4 -10 1 122.78 95.14 23.71 o -3 -10 1 110.49 112.54 23.76 o -2 -10 1 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