# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title 'Trimethylammonium perchlorate at 97 K' _shelx_refln_list_code 4 _shelx_F_calc_maximum 69.32 _exptl_crystal_F_000 168.00 _reflns_d_resolution_high 0.7338 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' _cell_length_a 5.5038 _cell_length_b 8.6049 _cell_length_c 7.5798 _cell_angle_alpha 90.000 _cell_angle_beta 103.665 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 613.32 613.64 16.43 o 2 0 0 1677.13 1500.50 30.90 o 3 0 0 891.57 859.42 13.24 o 4 0 0 140.66 152.97 1.57 o 5 0 0 18.40 21.08 0.35 o 6 0 0 2.37 1.44 0.20 o 7 0 0 92.04 93.10 1.32 o 1 1 0 206.59 178.79 1.83 o 2 1 0 494.27 504.80 5.61 o 3 1 0 293.02 307.52 4.10 o 4 1 0 8.16 6.95 0.20 o 5 1 0 2.42 1.77 0.20 o 6 1 0 0.09 0.21 0.18 o 7 1 0 39.10 32.91 4.42 o 0 2 0 4805.24 4102.93 29.48 o 1 2 0 609.24 537.08 3.86 o 2 2 0 212.38 191.59 2.73 o 3 2 0 851.33 800.27 5.27 o 4 2 0 246.47 263.75 1.75 o 5 2 0 48.75 51.17 0.49 o 6 2 0 41.69 45.46 0.47 o 7 2 0 88.32 86.85 0.74 o 1 3 0 1404.22 1381.51 17.41 o 2 3 0 147.23 159.76 1.40 o 3 3 0 257.36 266.05 2.92 o 4 3 0 55.22 52.74 0.74 o 5 3 0 137.30 133.32 1.02 o 6 3 0 1.23 1.41 0.17 o 7 3 0 25.14 23.98 0.52 o 0 4 0 478.98 429.87 4.12 o 1 4 0 94.68 83.63 0.57 o 2 4 0 39.23 41.76 3.30 o 3 4 0 543.40 551.16 23.52 o 4 4 0 326.75 324.90 4.76 o 5 4 0 66.12 69.65 0.59 o 6 4 0 124.17 125.68 1.42 o 1 5 0 316.18 339.42 2.16 o 2 5 0 47.07 47.82 0.56 o 3 5 0 49.26 51.07 0.93 o 4 5 0 46.16 45.51 1.14 o 5 5 0 45.86 42.06 0.68 o 6 5 0 0.02 0.20 0.42 o 0 6 0 1850.52 1753.96 15.19 o 1 6 0 125.96 129.70 0.88 o 2 6 0 297.13 300.40 4.49 o 3 6 0 347.75 376.42 7.14 o 4 6 0 112.21 102.93 2.44 o 5 6 0 36.15 35.87 0.81 o 6 6 0 5.34 5.19 0.48 o 1 7 0 4.17 4.29 0.17 o 2 7 0 38.45 39.39 0.54 o 3 7 0 66.89 67.15 1.08 o 4 7 0 21.98 24.52 0.84 o 5 7 0 0.08 0.23 0.44 o 0 8 0 1114.30 1088.28 8.44 o 1 8 0 111.84 113.08 0.75 o 2 8 0 197.79 193.54 1.71 o 3 8 0 189.30 200.41 4.00 o 4 8 0 41.32 36.09 0.67 o 5 8 0 19.57 20.34 0.70 o 1 9 0 41.55 42.43 0.38 o 2 9 0 21.98 22.72 0.39 o 3 9 0 6.23 8.09 0.42 o 4 9 0 8.19 10.24 0.52 o 0 10 0 101.86 100.62 1.04 o 1 10 0 61.23 58.52 0.60 o 2 10 0 14.02 13.17 0.41 o 3 10 0 119.82 124.32 1.72 o 1 11 0 65.05 66.04 0.69 o 2 11 0 2.91 3.68 0.44 o -7 0 1 18.59 17.78 0.48 o -6 0 1 1.32 0.99 0.25 o -5 0 1 1.02 0.88 0.22 o -4 0 1 81.59 91.32 2.37 o -3 0 1 382.73 415.35 19.90 o -2 0 1 1052.19 1047.65 9.63 o -1 0 1 124.81 132.36 3.54 o 1 0 1 106.65 102.40 0.90 o 2 0 1 46.43 56.75 0.95 o 3 0 1 6.55 11.42 0.25 o 4 0 1 29.78 29.42 0.42 o 5 0 1 97.75 99.72 1.32 o 6 0 1 8.72 9.61 0.45 o 7 0 1 81.61 81.96 1.24 o -7 1 1 1.16 1.30 0.20 o -6 1 1 55.48 59.62 0.54 o -5 1 1 1.47 1.98 0.16 o -4 1 1 255.69 268.04 2.82 o -3 1 1 319.48 312.09 5.12 o -2 1 1 348.66 314.17 2.16 o -1 1 1 4110.20 3745.65 56.46 o 0 1 1 674.84 683.81 3.92 o 1 1 1 4240.76 3916.70 24.41 o 2 1 1 216.85 200.92 2.35 o 3 1 1 520.67 526.59 3.21 o 4 1 1 249.35 259.68 1.82 o 5 1 1 0.02 0.33 0.18 o 6 1 1 74.04 77.89 0.80 o 7 1 1 11.04 12.06 0.33 o -7 2 1 18.37 17.73 0.31 o -6 2 1 28.59 25.94 0.35 o -5 2 1 10.67 6.98 1.55 o -4 2 1 46.62 43.69 0.73 o -3 2 1 163.82 186.43 4.89 o -2 2 1 0.89 1.29 0.14 o -1 2 1 388.02 364.58 2.19 o 0 2 1 313.09 308.59 1.73 o 1 2 1 471.29 472.07 2.84 o 2 2 1 488.08 475.21 2.61 o 3 2 1 12.64 12.44 0.21 o 4 2 1 322.55 329.58 2.66 o 5 2 1 61.10 58.58 0.54 o 6 2 1 18.80 20.30 0.33 o -7 3 1 79.82 78.23 1.11 o -6 3 1 64.88 64.92 0.63 o -5 3 1 109.46 112.81 1.28 o -4 3 1 161.87 169.78 3.42 o -3 3 1 66.59 69.63 2.48 o -2 3 1 12.91 11.18 0.66 o -1 3 1 0.15 1.89 0.11 o 0 3 1 450.10 393.89 2.19 o 1 3 1 68.61 62.58 0.99 o 2 3 1 271.91 254.48 3.62 o 3 3 1 447.44 445.98 6.02 o 4 3 1 506.22 509.93 5.42 o 5 3 1 112.70 114.53 0.90 o 6 3 1 89.98 91.89 0.97 o -6 4 1 51.00 48.26 0.86 o -5 4 1 15.37 13.45 0.65 o -4 4 1 232.65 225.55 2.87 o -3 4 1 44.51 45.85 0.88 o -2 4 1 268.13 298.55 3.18 o -1 4 1 249.16 261.87 1.51 o 0 4 1 348.04 348.45 2.95 o 1 4 1 519.02 506.25 3.02 o 2 4 1 1080.23 1069.40 8.23 o 3 4 1 23.74 25.32 0.62 o 4 4 1 530.40 532.25 6.70 o 5 4 1 32.36 30.58 0.50 o 6 4 1 18.87 18.07 0.56 o -6 5 1 70.39 70.08 0.94 o -5 5 1 72.92 70.39 1.24 o -4 5 1 146.18 148.43 5.68 o -3 5 1 114.14 109.78 1.94 o -2 5 1 30.59 27.01 0.57 o -1 5 1 235.71 237.94 1.54 o 0 5 1 154.78 150.20 1.18 o 1 5 1 312.73 312.28 2.82 o 2 5 1 113.73 112.93 0.95 o 3 5 1 338.79 343.12 2.53 o 4 5 1 298.58 306.84 2.71 o 5 5 1 47.97 46.72 0.72 o 6 5 1 63.25 65.10 1.24 o -6 6 1 3.33 3.81 0.46 o -5 6 1 6.79 7.52 0.44 o -4 6 1 2.00 4.19 0.49 o -3 6 1 21.01 19.95 0.59 o -2 6 1 28.70 27.43 1.99 o -1 6 1 17.83 18.49 0.25 o 0 6 1 49.69 57.11 1.04 o 1 6 1 81.76 90.78 0.64 o 2 6 1 22.78 26.17 0.39 o 3 6 1 3.44 5.14 0.40 o 4 6 1 46.97 46.60 0.87 o 5 6 1 61.89 60.94 1.21 o 6 6 1 4.73 4.59 0.67 o -5 7 1 4.39 3.33 0.50 o -4 7 1 143.27 146.69 2.49 o -3 7 1 171.77 159.06 3.09 o -2 7 1 147.22 148.95 5.51 o -1 7 1 856.26 830.12 5.00 o 0 7 1 165.71 172.03 1.23 o 1 7 1 761.12 746.09 4.12 o 2 7 1 42.88 44.12 0.51 o 3 7 1 144.67 141.87 1.67 o 4 7 1 91.91 95.64 1.19 o 5 7 1 2.11 3.26 0.53 o -5 8 1 0.48 1.66 0.50 o -4 8 1 4.77 5.21 0.47 o -3 8 1 20.65 19.98 0.75 o -2 8 1 29.58 27.74 1.24 o -1 8 1 8.62 9.79 0.47 o 0 8 1 5.36 7.02 0.20 o 1 8 1 7.40 8.80 0.18 o 2 8 1 1.79 2.76 0.45 o 3 8 1 0.14 0.62 0.38 o 4 8 1 27.24 27.76 0.70 o 5 8 1 46.32 48.62 1.30 o -4 9 1 75.66 75.31 1.09 o -3 9 1 74.36 69.25 1.06 o -2 9 1 90.26 90.45 1.22 o -1 9 1 152.10 152.62 1.00 o 0 9 1 107.63 107.41 0.76 o 1 9 1 158.74 159.35 1.03 o 2 9 1 47.67 47.60 0.56 o 3 9 1 51.67 51.64 0.92 o 4 9 1 76.03 81.57 1.35 o -3 10 1 10.95 10.47 0.45 o -2 10 1 24.04 26.44 0.54 o -1 10 1 21.87 21.89 0.51 o 0 10 1 8.58 9.24 0.37 o 1 10 1 18.64 20.02 0.43 o 2 10 1 129.74 137.89 1.90 o 3 10 1 0.89 2.00 0.64 o -2 11 1 33.21 32.61 0.61 o -1 11 1 9.56 10.10 0.32 o 0 11 1 41.57 40.10 1.18 o 1 11 1 24.28 24.37 0.44 o 2 11 1 41.83 41.80 0.72 o -7 0 2 205.94 201.20 2.46 o -6 0 2 7.07 7.17 0.43 o -5 0 2 218.51 218.59 4.60 o -4 0 2 351.90 353.59 9.11 o -3 0 2 231.57 220.63 3.48 o -2 0 2 1005.47 928.04 13.42 o -1 0 2 758.24 738.00 6.83 o 0 0 2 4229.62 3877.66 35.13 o 1 0 2 438.13 460.42 4.46 o 2 0 2 511.71 499.45 3.95 o 3 0 2 29.89 32.68 0.55 o 4 0 2 15.74 15.71 1.55 o 5 0 2 15.74 16.08 0.33 o 6 0 2 0.22 0.07 0.59 o -7 1 2 0.03 0.22 0.21 o -6 1 2 0.03 0.10 0.20 o -5 1 2 45.02 40.56 0.47 o -4 1 2 25.45 28.36 1.05 o -3 1 2 237.02 266.41 3.78 o -2 1 2 30.92 33.94 0.55 o -1 1 2 19.09 19.32 0.96 o 0 1 2 564.73 550.86 3.66 o 1 1 2 114.96 113.02 0.88 o 2 1 2 8.20 13.34 0.25 o 3 1 2 299.37 311.83 2.24 o 4 1 2 294.39 302.45 2.25 o 5 1 2 89.13 87.26 0.64 o 6 1 2 154.22 160.41 1.37 o -7 2 2 175.19 168.30 1.83 o -6 2 2 14.98 14.93 0.31 o -5 2 2 152.42 151.17 2.24 o -4 2 2 305.21 313.29 10.81 o -3 2 2 33.21 36.04 0.56 o -2 2 2 0.21 0.77 0.51 o -1 2 2 424.43 404.97 2.79 o 0 2 2 218.48 200.05 1.36 o 2 2 2 160.04 167.55 1.16 o 3 2 2 299.51 303.68 2.37 o 4 2 2 8.33 10.55 0.28 o 5 2 2 66.99 67.08 0.54 o 6 2 2 32.45 33.51 0.54 o -7 3 2 0.71 1.17 0.35 o -6 3 2 5.14 4.64 0.22 o -5 3 2 330.01 329.02 3.75 o -4 3 2 0.62 1.95 0.54 o -3 3 2 75.15 80.82 0.95 o -2 3 2 49.85 47.94 0.45 o -1 3 2 17.34 24.89 0.28 o 0 3 2 1526.31 1502.44 12.60 o 1 3 2 1342.53 1305.65 6.90 o 2 3 2 144.99 148.31 1.05 o 3 3 2 1223.44 1171.18 6.92 o 4 3 2 140.91 143.81 1.19 o 5 3 2 172.31 172.71 1.19 o 6 3 2 38.70 39.23 0.74 o -7 4 2 147.68 146.12 2.82 o -6 4 2 61.72 61.61 1.87 o -5 4 2 98.75 97.84 1.38 o -4 4 2 294.89 301.53 4.69 o -2 4 2 64.39 71.44 2.00 o -1 4 2 39.58 32.31 0.32 o 0 4 2 0.09 0.62 0.14 o 1 4 2 0.05 0.95 0.35 o 2 4 2 137.05 134.64 1.25 o 3 4 2 415.67 425.86 4.02 o 4 4 2 65.79 63.18 1.12 o 5 4 2 98.12 96.98 1.42 o 6 4 2 73.36 67.07 5.13 o -6 5 2 2.66 2.78 0.67 o -5 5 2 127.31 124.86 1.97 o -4 5 2 1.34 2.51 1.31 o -3 5 2 0.11 0.85 0.67 o -2 5 2 9.28 9.29 0.20 o -1 5 2 0.87 0.59 0.30 o 0 5 2 506.68 539.60 3.30 o 1 5 2 442.97 471.94 2.90 o 2 5 2 51.88 57.33 0.50 o 3 5 2 508.66 521.87 9.02 o 4 5 2 100.40 96.14 2.92 o 5 5 2 71.33 70.47 0.93 o 6 5 2 47.15 52.02 1.07 o -6 6 2 0.33 0.72 0.53 o -5 6 2 144.41 147.28 1.87 o -4 6 2 202.22 199.68 2.61 o -3 6 2 83.27 92.81 1.25 o -2 6 2 143.81 134.85 2.70 o -1 6 2 157.36 161.99 1.12 o 0 6 2 526.38 527.80 3.28 o 1 6 2 0.92 1.14 0.15 o 2 6 2 228.07 218.75 5.56 o 3 6 2 68.33 67.34 0.83 o 4 6 2 1.20 0.91 0.39 o 5 6 2 26.24 25.96 0.63 o -6 7 2 0.35 0.38 0.57 o -5 7 2 1.64 1.87 0.54 o -4 7 2 9.38 9.24 0.57 o -3 7 2 139.78 139.79 1.75 o -2 7 2 1.90 1.84 0.11 o -1 7 2 12.96 14.79 0.74 o 0 7 2 47.53 51.39 0.50 o 1 7 2 6.29 7.60 0.19 o 2 7 2 0.21 1.09 0.26 o 3 7 2 48.77 51.76 0.71 o 4 7 2 108.47 110.50 1.69 o 5 7 2 23.38 23.54 0.71 o -5 8 2 103.27 106.96 1.38 o -4 8 2 131.29 127.66 1.91 o -3 8 2 95.79 101.84 1.53 o -2 8 2 185.20 179.24 2.44 o -1 8 2 171.71 175.61 1.22 o 0 8 2 381.40 399.27 2.60 o 1 8 2 0.14 0.27 0.13 o 2 8 2 115.88 115.19 0.96 o 3 8 2 21.77 22.78 0.53 o 4 8 2 2.66 3.48 0.66 o -4 9 2 19.02 17.03 0.57 o -3 9 2 3.26 2.88 0.49 o -2 9 2 7.48 9.26 0.53 o -1 9 2 0.37 0.31 0.15 o 0 9 2 71.68 75.35 0.88 o 1 9 2 45.33 47.90 0.42 o 2 9 2 2.73 3.52 0.21 o 3 9 2 152.61 164.12 2.60 o 4 9 2 42.42 44.73 0.81 o -3 10 2 21.65 23.76 0.76 o -2 10 2 9.04 8.52 0.60 o -1 10 2 86.57 84.26 1.09 o 0 10 2 16.29 16.15 0.24 o 1 10 2 15.18 13.90 0.50 o 2 10 2 28.65 29.48 0.64 o 3 10 2 74.11 74.92 1.18 o -2 11 2 14.01 14.38 0.47 o -1 11 2 0.16 -0.05 0.32 o 0 11 2 95.22 96.99 1.25 o 1 11 2 92.56 93.83 1.30 o -7 0 3 7.82 7.55 1.05 o -6 0 3 26.83 27.21 0.55 o -5 0 3 9.86 9.25 0.46 o -4 0 3 66.75 70.63 2.68 o -3 0 3 101.90 111.46 3.95 o -2 0 3 1.49 0.59 0.36 o -1 0 3 570.88 586.40 5.56 o 0 0 3 38.96 30.35 0.53 o 1 0 3 30.38 46.29 2.99 o 2 0 3 10.25 12.91 0.32 o 3 0 3 107.31 103.69 1.08 o 4 0 3 291.93 299.11 3.22 o 5 0 3 172.26 169.11 2.10 o 6 0 3 101.38 99.00 1.09 o -7 1 3 37.71 37.56 0.90 o -6 1 3 240.16 240.92 3.01 o -5 1 3 109.32 105.31 2.20 o -4 1 3 759.69 738.46 5.68 o -3 1 3 607.86 606.67 11.30 o -2 1 3 87.71 76.72 0.67 o -1 1 3 2046.27 1947.32 14.37 o 0 1 3 67.32 66.37 0.63 o 1 1 3 33.34 33.23 0.35 o 2 1 3 104.36 116.98 0.90 o 3 1 3 23.85 27.77 0.66 o 4 1 3 23.17 22.61 0.38 o 5 1 3 75.19 71.56 0.74 o 6 1 3 32.84 29.90 0.41 o -7 2 3 0.07 0.37 0.27 o -6 2 3 0.04 0.17 0.13 o -5 2 3 0.60 0.79 0.23 o -4 2 3 23.66 24.11 0.65 o -3 2 3 184.86 193.22 4.07 o -2 2 3 57.46 66.88 0.60 o -1 2 3 0.40 1.18 0.66 o 0 2 3 380.84 359.41 4.17 o 1 2 3 182.74 189.81 1.28 o 2 2 3 131.86 138.56 1.02 o 3 2 3 127.87 129.20 1.02 o 4 2 3 495.97 518.21 3.69 o 5 2 3 47.68 46.10 0.52 o 6 2 3 77.66 79.54 0.72 o -7 3 3 155.25 152.04 2.56 o -6 3 3 121.48 119.55 1.25 o -5 3 3 168.42 168.48 4.98 o -4 3 3 191.88 194.99 1.99 o -3 3 3 81.28 83.29 0.88 o -2 3 3 6.31 7.88 0.28 o -1 3 3 43.19 37.92 0.38 o 0 3 3 91.07 81.96 0.65 o 1 3 3 30.68 36.12 0.47 o 2 3 3 110.51 98.97 0.81 o 3 3 3 112.17 112.28 0.90 o 4 3 3 38.47 37.26 0.43 o 5 3 3 0.29 0.53 0.21 o 6 3 3 30.62 29.17 0.63 o -7 4 3 2.23 3.36 0.66 o -6 4 3 6.25 5.69 0.56 o -5 4 3 0.07 1.58 0.80 o -4 4 3 125.14 129.36 1.98 o -3 4 3 189.58 191.64 1.53 o -2 4 3 51.75 61.28 0.74 o -1 4 3 193.22 203.80 2.02 o 0 4 3 647.77 646.35 3.95 o 1 4 3 382.41 409.18 4.55 o 2 4 3 373.11 409.38 4.67 o 3 4 3 81.82 89.63 1.48 o 4 4 3 510.55 500.80 5.85 o 5 4 3 3.92 5.08 0.30 o 6 4 3 43.86 44.92 1.34 o -6 5 3 129.81 131.25 1.89 o -5 5 3 94.03 85.99 4.71 o -4 5 3 185.64 191.08 3.15 o -3 5 3 137.39 142.47 1.25 o -2 5 3 1.50 2.05 0.26 o -1 5 3 224.47 221.77 1.47 o 0 5 3 44.09 42.11 0.48 o 1 5 3 14.00 11.68 0.35 o 2 5 3 32.77 31.70 0.40 o 3 5 3 109.03 104.10 0.90 o 4 5 3 9.25 9.55 0.64 o 5 5 3 5.82 6.07 0.53 o -6 6 3 8.63 10.20 0.73 o -5 6 3 2.05 2.36 0.54 o -4 6 3 8.61 10.21 1.74 o -3 6 3 48.57 45.78 0.53 o -2 6 3 19.03 20.37 0.67 o -1 6 3 0.04 6.73 1.22 o 0 6 3 117.28 127.80 1.14 o 1 6 3 35.22 43.86 0.61 o 2 6 3 15.12 17.82 0.28 o 3 6 3 69.12 71.33 0.90 o 4 6 3 158.44 161.10 1.74 o 5 6 3 56.20 54.58 9.02 o -5 7 3 24.76 23.88 1.20 o -4 7 3 299.20 308.74 6.74 o -3 7 3 246.25 233.68 2.31 o -2 7 3 74.27 81.81 0.68 o -1 7 3 553.50 554.45 3.49 o 0 7 3 27.66 27.23 0.44 o 1 7 3 83.34 80.80 1.37 o 2 7 3 15.07 16.02 0.29 o 3 7 3 23.37 19.95 0.35 o 4 7 3 6.40 7.11 0.54 o -5 8 3 11.52 11.87 0.73 o -4 8 3 12.49 12.21 0.65 o -3 8 3 44.90 44.78 1.32 o -2 8 3 16.09 18.74 0.51 o -1 8 3 1.45 0.91 0.19 o 0 8 3 36.83 38.29 0.64 o 1 8 3 14.46 17.27 0.30 o 2 8 3 8.84 9.77 0.28 o 3 8 3 53.79 59.33 0.88 o 4 8 3 135.16 137.98 1.35 o -4 9 3 108.84 110.22 1.78 o -3 9 3 94.69 93.22 1.36 o -2 9 3 29.39 31.00 0.77 o -1 9 3 106.99 105.09 0.82 o 0 9 3 40.86 39.56 0.42 o 1 9 3 7.45 6.77 0.25 o 2 9 3 2.32 2.25 0.28 o 3 9 3 12.54 12.34 0.47 o -3 10 3 79.76 80.33 1.72 o -2 10 3 0.61 0.50 0.50 o -1 10 3 46.39 46.61 1.29 o 0 10 3 74.26 73.04 2.73 o 1 10 3 76.23 78.99 0.93 o 2 10 3 105.90 110.23 1.26 o -1 11 3 11.39 10.06 0.38 o 0 11 3 39.76 38.27 0.90 o -7 0 4 97.89 96.17 2.48 o -6 0 4 3.57 3.95 0.28 o -5 0 4 718.90 749.24 7.46 o -4 0 4 323.27 348.52 3.72 o -3 0 4 366.95 368.48 3.93 o -2 0 4 2063.63 2109.07 19.22 o -1 0 4 264.37 273.52 2.79 o 0 0 4 510.33 534.87 5.25 o 1 0 4 92.30 101.28 1.49 o 2 0 4 93.77 100.05 1.07 o 3 0 4 114.58 119.87 1.42 o 4 0 4 82.00 75.08 1.74 o 5 0 4 2.94 3.03 0.43 o 6 0 4 37.72 37.73 1.04 o -7 1 4 76.14 73.67 0.93 o -6 1 4 25.57 24.80 0.78 o -5 1 4 74.58 76.20 1.86 o -4 1 4 367.52 380.61 10.33 o -3 1 4 72.75 70.25 1.33 o -2 1 4 3.04 4.01 0.58 o -1 1 4 127.00 128.52 1.05 o 0 1 4 2.24 1.27 0.26 o 1 1 4 0.06 0.57 0.25 o 2 1 4 8.56 7.10 0.27 o 3 1 4 194.10 196.86 1.26 o 4 1 4 105.58 98.39 0.92 o 5 1 4 83.25 84.26 0.83 o 6 1 4 123.94 117.04 1.24 o -7 2 4 51.12 48.25 0.68 o -6 2 4 36.38 35.68 0.77 o -5 2 4 358.51 359.60 2.91 o -4 2 4 176.42 181.67 1.48 o -3 2 4 76.88 83.24 0.78 o -2 2 4 530.28 557.67 4.68 o -1 2 4 272.62 277.29 2.01 o 0 2 4 91.49 96.38 0.84 o 1 2 4 21.79 14.89 0.35 o 2 2 4 85.00 91.09 0.79 o 3 2 4 6.35 5.88 0.40 o 4 2 4 15.32 14.24 0.35 o 5 2 4 0.99 1.01 0.20 o -7 3 4 40.00 39.02 1.62 o -6 3 4 1.04 1.68 0.25 o -5 3 4 1.52 1.66 0.26 o -4 3 4 429.02 447.61 5.05 o -2 3 4 343.23 345.82 2.51 o -1 3 4 304.38 315.24 2.30 o 0 3 4 597.00 580.77 6.37 o 1 3 4 248.68 263.60 1.80 o 2 3 4 87.81 89.28 0.76 o 3 3 4 387.31 411.42 3.70 o 4 3 4 4.10 3.63 0.24 o 5 3 4 79.64 77.94 0.96 o -6 4 4 64.94 60.07 1.68 o -5 4 4 151.18 149.97 1.79 o -4 4 4 100.16 100.44 0.99 o -2 4 4 136.17 137.60 1.08 o -1 4 4 128.57 123.53 0.97 o 0 4 4 41.55 34.12 0.48 o 1 4 4 114.59 108.64 0.85 o 2 4 4 108.77 105.12 0.88 o 3 4 4 81.98 79.02 0.84 o 4 4 4 0.03 0.05 0.19 o 5 4 4 3.92 3.52 0.52 o -6 5 4 0.87 1.01 0.52 o -5 5 4 4.30 4.03 0.45 o -4 5 4 248.49 253.61 2.75 o -3 5 4 8.61 12.30 0.40 o -2 5 4 128.94 129.65 1.18 o -1 5 4 216.90 228.29 2.05 o 0 5 4 238.84 258.49 1.76 o 1 5 4 136.26 144.46 1.09 o 2 5 4 44.02 46.58 0.78 o 3 5 4 193.87 201.73 1.59 o 4 5 4 12.84 12.43 0.63 o 5 5 4 49.25 47.06 1.00 o -6 6 4 5.86 5.79 0.64 o -5 6 4 297.24 299.68 3.37 o 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