Acta Cryst. (2006). E62, o1384-o1386  [ doi:10.1107/S160053680600849X ]

(E)-1-Mercapto-1-(p-tolylsulfanyl)-N-(p-tosylmethyl) methanimine: a two-dimensional supramolecular network of S-HO and C-H interactions

M. Kakeya, T. Fujihara and A. Nagasawa

Online 15 March 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.004 Å
• R factor = 0.056
• wR factor = 0.158
• Data-to-parameter ratio = 20.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         S2     
PLAT420_ALERT_2_C D-H Without Acceptor       S3     -   H1A    ...          ?       
PLAT480_ALERT_4_C Long H...A H-Bond Reported H1A    ..  O1      ..       2.68 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H13    ..  O1      ..       2.66 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H2     ..  CG1     ..       3.02 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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