# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' AA8 - COLORLESS PRISM' _shelx_refln_list_code 4 _shelx_F_calc_maximum 381.76 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.7708 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.7360 _cell_length_b 12.2010 _cell_length_c 19.5030 _cell_angle_alpha 72.674 _cell_angle_beta 73.357 _cell_angle_gamma 73.937 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 99768.22 97207.55 1787.09 o 4 0 0 60347.18 59745.47 2062.91 o 5 0 0 435.47 417.95 78.84 o 6 0 0 5068.84 5006.15 94.15 o 7 0 0 62663.63 63070.29 1317.81 o 8 0 0 5563.65 5507.68 185.39 o 9 0 0 25.19 52.35 53.43 o 10 0 0 13272.83 13956.44 266.97 o 11 0 0 6938.29 6930.41 176.44 o 12 0 0 4.93 46.55 77.77 o 13 0 0 622.13 462.04 71.95 o 14 0 0 5612.46 5472.32 458.82 o -14 1 0 0.66 -230.56 153.70 o -13 1 0 11.22 -64.11 92.18 o -12 1 0 818.91 613.32 95.22 o -11 1 0 279.74 259.57 45.50 o -10 1 0 263.46 270.90 41.59 o -9 1 0 22.06 21.43 34.64 o -8 1 0 786.66 711.03 92.77 o -7 1 0 959.95 1066.29 35.40 o -6 1 0 1013.55 1152.94 34.19 o -5 1 0 1.24 6.64 38.12 o -4 1 0 1112.36 964.26 44.70 o -3 1 0 2.53 -9.19 18.37 o -2 1 0 109.51 137.48 31.23 o 3 1 0 9109.41 8346.68 171.77 o 4 1 0 191.26 164.06 24.65 o 5 1 0 280.06 234.31 21.37 o 6 1 0 1528.52 1534.95 82.52 o 7 1 0 2243.70 2111.24 91.09 o 8 1 0 0.82 48.68 33.61 o 9 1 0 729.73 765.88 47.61 o 10 1 0 2581.73 2548.79 80.46 o 11 1 0 30.76 18.15 47.32 o 12 1 0 119.38 30.53 53.43 o 13 1 0 1266.08 1378.80 87.72 o 14 1 0 1183.49 1122.35 128.91 o -13 2 0 459.18 527.25 150.03 o -12 2 0 2611.53 2358.76 170.08 o -11 2 0 71.05 117.22 82.06 o -10 2 0 9061.14 9619.46 239.74 o -9 2 0 73.33 51.88 30.69 o -8 2 0 3955.22 3742.76 78.87 o -7 2 0 7013.88 6925.36 120.34 o -6 2 0 213.10 234.27 23.92 o -5 2 0 17711.30 16364.41 245.12 o -4 2 0 1830.22 1967.12 46.54 o -3 2 0 3895.71 4223.64 71.12 o -2 2 0 6089.22 5779.96 233.16 o 3 2 0 4159.65 4207.72 80.84 o 4 2 0 3483.26 3287.09 78.44 o 5 2 0 18315.31 18319.23 328.32 o 6 2 0 26684.80 27919.98 574.25 o 7 2 0 493.00 500.78 25.02 o 8 2 0 46.42 81.19 38.86 o 9 2 0 17666.13 18503.33 930.80 o 10 2 0 949.72 861.95 99.36 o 11 2 0 2931.35 3218.43 107.40 o 12 2 0 4003.43 4003.00 133.27 o 13 2 0 5090.86 4934.35 176.89 o 14 2 0 42.46 353.34 123.09 o -13 3 0 49.20 366.50 137.78 o -12 3 0 321.49 324.50 92.93 o -11 3 0 292.91 332.57 56.69 o -10 3 0 109.06 83.87 33.83 o -9 3 0 471.29 468.00 34.50 o -8 3 0 1135.21 1087.83 50.98 o -7 3 0 134.81 79.42 25.57 o -6 3 0 444.54 380.58 29.99 o -5 3 0 3084.27 3268.34 68.37 o -4 3 0 27.26 128.16 19.19 o -3 3 0 167.37 134.57 16.99 o -2 3 0 36.02 -25.48 16.99 o -1 3 0 1268.80 1164.00 76.39 o 1 3 0 292.64 456.21 33.07 o 2 3 0 785.46 868.43 37.66 o 3 3 0 3929.42 3820.96 69.97 o 4 3 0 174.84 118.39 33.83 o 5 3 0 198.64 232.17 30.97 o 6 3 0 161.09 288.10 37.88 o 7 3 0 446.93 439.98 83.43 o 8 3 0 494.60 450.71 29.49 o 9 3 0 321.78 522.41 66.75 o 10 3 0 942.57 937.21 65.45 o 11 3 0 378.08 316.22 53.43 o 12 3 0 314.78 208.86 62.55 o 13 3 0 71.18 143.94 85.01 o 14 3 0 112.25 130.99 122.78 o -12 4 0 4973.81 5190.42 350.89 o -11 4 0 4087.20 4158.95 243.57 o -10 4 0 0.01 13.40 38.82 o -9 4 0 2534.90 2653.38 73.79 o -8 4 0 20779.60 20931.15 348.80 o -7 4 0 1946.74 1847.65 73.79 o -6 4 0 41.33 76.79 27.12 o -5 4 0 46112.37 46265.54 686.26 o -4 4 0 29869.58 29422.70 433.23 o -3 4 0 53.11 143.37 35.52 o -2 4 0 39891.26 43087.23 807.45 o -1 4 0 72053.68 68226.91 1436.31 o 0 4 0 11348.13 11536.51 182.55 o 1 4 0 1947.29 1938.26 36.03 o 2 4 0 42137.71 40463.53 1046.23 o 3 4 0 34696.36 34892.75 1175.59 o 4 4 0 2148.52 2369.85 112.98 o 5 4 0 20438.93 21299.20 475.35 o 6 4 0 29352.59 29038.60 453.06 o 7 4 0 4523.01 4687.99 148.19 o 8 4 0 38.82 24.99 36.65 o 9 4 0 15689.97 15665.26 254.15 o 10 4 0 5887.94 5617.60 143.45 o 11 4 0 719.83 699.95 85.88 o 12 4 0 1835.10 1532.38 117.42 o 13 4 0 6295.23 5703.52 230.26 o 14 4 0 336.03 209.26 173.30 o -12 5 0 441.98 482.54 121.55 o -11 5 0 71.21 47.22 71.97 o -10 5 0 12.79 -33.51 58.02 o -9 5 0 1885.78 1638.97 92.01 o -8 5 0 110.94 214.76 33.70 o -7 5 0 45.10 88.55 30.62 o -6 5 0 580.18 662.31 32.87 o -5 5 0 909.93 848.83 30.22 o -4 5 0 1138.65 1254.63 34.49 o -3 5 0 20.23 15.39 19.27 o -2 5 0 485.79 540.48 49.30 o -1 5 0 154.84 178.00 19.81 o 1 5 0 42.05 -18.06 16.00 o 2 5 0 1681.19 1571.11 33.73 o 3 5 0 88.57 122.40 18.03 o 4 5 0 1108.73 1123.94 55.11 o 5 5 0 6420.58 6395.73 117.00 o 6 5 0 1072.77 1048.46 46.23 o 7 5 0 450.54 402.00 63.53 o 8 5 0 1928.93 1991.07 68.70 o 9 5 0 3749.00 3657.73 100.96 o 10 5 0 0.72 -53.95 78.23 o 11 5 0 143.58 183.02 52.26 o 12 5 0 2904.02 2776.33 154.47 o 13 5 0 667.44 592.29 148.65 o 14 5 0 8.54 -74.59 89.22 o -11 6 0 1562.93 1541.23 114.77 o -10 6 0 683.72 744.36 115.12 o -9 6 0 3509.45 3484.46 139.93 o -8 6 0 459.04 523.29 38.49 o -7 6 0 24.29 57.53 25.01 o -6 6 0 12852.38 12857.62 226.12 o -5 6 0 345.48 346.13 73.33 o -4 6 0 2314.03 2464.29 52.71 o -3 6 0 12480.66 12917.24 267.57 o -2 6 0 17511.77 16607.10 329.76 o -1 6 0 1293.55 1141.47 34.49 o 0 6 0 6314.21 6700.71 228.72 o 1 6 0 55915.15 56719.32 764.14 o 2 6 0 10929.01 11432.87 426.36 o 3 6 0 1468.02 1609.65 44.40 o 4 6 0 18375.48 17643.32 250.15 o 5 6 0 31983.33 32472.94 425.74 o 6 6 0 707.29 701.13 43.62 o 7 6 0 82.37 86.72 44.24 o 8 6 0 21669.84 23414.39 402.48 o 9 6 0 3939.95 3935.79 220.76 o 10 6 0 28.43 37.52 41.93 o 11 6 0 7304.27 7288.54 410.59 o 12 6 0 9155.71 9303.18 349.39 o 13 6 0 2.03 -72.46 86.03 o 14 6 0 625.83 417.33 173.76 o -11 7 0 108.32 12.25 82.06 o -10 7 0 327.54 367.60 119.11 o -9 7 0 255.07 319.40 180.65 o -8 7 0 59.02 80.97 32.37 o -7 7 0 278.94 294.72 40.42 o -6 7 0 11.98 91.85 94.46 o -5 7 0 65.52 139.86 27.28 o -4 7 0 78.40 59.15 25.87 o -3 7 0 7.62 -7.58 33.37 o -2 7 0 81.48 78.33 21.43 o -1 7 0 93.54 110.29 19.27 o 1 7 0 196.09 232.11 24.25 o 2 7 0 176.38 244.75 21.53 o 3 7 0 37.77 41.27 47.46 o 4 7 0 1842.23 1860.20 48.84 o 5 7 0 89.72 87.92 79.45 o 6 7 0 595.77 654.19 27.88 o 7 7 0 523.40 480.04 69.04 o 8 7 0 1134.04 1170.48 59.81 o 9 7 0 273.71 359.71 47.31 o 10 7 0 0.64 15.92 50.10 o 11 7 0 1403.24 1440.98 306.95 o 12 7 0 197.53 240.76 125.23 o 13 7 0 13.07 -68.62 86.08 o 14 7 0 380.45 204.35 111.73 o -10 8 0 811.23 643.68 82.68 o -9 8 0 6799.34 6548.12 279.24 o -8 8 0 608.15 465.94 36.09 o -7 8 0 7.91 128.60 27.68 o -6 8 0 8616.49 8627.65 178.78 o -5 8 0 11509.85 12048.15 247.70 o -4 8 0 91.55 62.78 24.85 o -3 8 0 2001.86 1972.62 66.75 o -2 8 0 18335.60 18736.63 319.50 o -1 8 0 474.47 524.72 25.53 o 0 8 0 258.56 334.88 37.97 o 1 8 0 18817.49 19516.06 730.25 o 2 8 0 28286.04 29478.81 373.30 o 3 8 0 307.54 281.55 35.67 o 4 8 0 1921.33 1780.91 98.44 o 5 8 0 22915.54 23283.54 532.15 o 6 8 0 357.01 357.48 59.55 o 7 8 0 461.88 453.93 43.91 o 8 8 0 8806.06 8978.74 575.47 o 9 8 0 4735.21 4666.30 97.29 o 10 8 0 701.34 683.51 44.08 o 11 8 0 382.86 294.10 85.75 o 12 8 0 4590.73 4719.53 241.93 o 13 8 0 2.33 -169.20 112.80 o -9 9 0 14.13 29.61 60.03 o -8 9 0 604.15 617.44 138.70 o -7 9 0 1078.69 921.90 132.58 o -6 9 0 73.39 151.99 23.52 o -5 9 0 1085.53 1081.48 89.41 o -4 9 0 2595.32 2756.37 116.66 o -3 9 0 41.23 30.50 25.02 o -2 9 0 9.75 60.20 33.68 o -1 9 0 403.10 549.84 102.11 o 1 9 0 343.29 303.36 29.04 o 2 9 0 409.90 396.95 31.12 o 3 9 0 200.56 199.47 28.14 o 4 9 0 1249.65 1193.04 49.53 o 5 9 0 6.00 -51.62 34.41 o 6 9 0 1.00 -22.37 34.03 o 7 9 0 107.09 173.84 41.42 o 8 9 0 452.48 360.68 56.66 o 9 9 0 1.19 95.91 60.63 o 10 9 0 29.84 94.97 60.98 o 11 9 0 1320.56 1317.72 322.87 o 12 9 0 467.57 414.15 99.87 o 13 9 0 293.60 124.42 146.97 o -8 10 0 37.22 46.94 47.92 o -7 10 0 4987.94 5388.98 657.99 o -6 10 0 320.39 347.80 33.77 o -5 10 0 533.54 521.52 70.27 o -4 10 0 7485.90 7447.51 123.65 o -3 10 0 10029.33 10371.61 265.61 o -2 10 0 1.69 15.92 23.04 o -1 10 0 1702.50 1763.24 93.08 o 0 10 0 24247.28 25694.73 521.74 o 1 10 0 919.11 904.21 59.40 o 2 10 0 294.01 358.08 82.52 o 3 10 0 12917.87 13337.72 219.91 o 4 10 0 15969.05 16388.03 446.41 o 5 10 0 95.65 58.53 33.60 o 6 10 0 1854.91 1769.30 104.41 o 7 10 0 20305.96 20654.70 385.00 o 8 10 0 3491.17 3353.59 124.46 o 9 10 0 396.58 307.04 116.66 o 10 10 0 7130.37 7575.53 280.94 o 11 10 0 6137.99 5833.24 280.12 o 12 10 0 131.55 113.87 95.26 o -7 11 0 146.41 -12.25 109.92 o -6 11 0 35.83 -51.74 180.04 o -5 11 0 3.52 -12.95 20.24 o -4 11 0 56.99 57.10 28.78 o -3 11 0 16.61 47.29 21.33 o -2 11 0 291.64 288.47 25.75 o -1 11 0 221.38 261.51 26.47 o 1 11 0 765.10 752.68 40.53 o 2 11 0 53.18 70.24 33.83 o 3 11 0 1921.39 1717.38 55.27 o 4 11 0 5.67 -3.65 33.68 o 5 11 0 1051.23 994.67 49.13 o 6 11 0 773.80 810.03 61.03 o 7 11 0 529.82 643.83 60.50 o 8 11 0 424.13 383.73 66.78 o 9 11 0 31.02 -82.00 102.88 o 10 11 0 1487.27 1236.36 137.92 o 11 11 0 4.37 72.63 163.50 o -5 12 0 74.23 248.62 157.07 o -4 12 0 264.47 64.30 94.92 o -3 12 0 4998.67 5080.17 623.08 o -2 12 0 366.61 272.73 30.36 o -1 12 0 138.40 159.40 37.84 o 0 12 0 6868.94 7075.85 136.37 o 1 12 0 4620.96 4668.22 101.78 o 2 12 0 1048.55 1079.15 52.82 o 3 12 0 61.45 103.32 39.68 o 4 12 0 5125.99 5216.21 134.22 o 5 12 0 19.40 18.71 39.82 o 6 12 0 951.61 989.16 63.41 o 7 12 0 3774.19 3753.33 129.14 o 8 12 0 1305.20 1215.24 160.90 o 9 12 0 666.49 440.48 137.17 o 10 12 0 86.77 196.73 226.73 o 11 12 0 559.55 351.15 108.22 o -4 13 0 6.28 -245.25 218.31 o -3 13 0 1.70 351.80 218.00 o -2 13 0 676.24 613.34 59.25 o -1 13 0 14.62 -16.38 51.63 o 1 13 0 333.09 344.33 48.62 o 2 13 0 396.12 350.39 50.98 o 3 13 0 215.81 279.46 58.74 o 4 13 0 40.44 -74.00 50.58 o 5 13 0 955.25 981.22 190.91 o 6 13 0 162.77 223.10 52.35 o 7 13 0 939.90 1131.96 134.11 o 8 13 0 139.95 160.46 73.59 o 9 13 0 107.32 85.93 161.82 o -2 14 0 1217.64 1142.98 224.43 o -1 14 0 4021.73 3483.19 182.36 o 0 14 0 1689.69 1562.04 111.16 o 1 14 0 816.52 833.86 164.57 o 2 14 0 6808.25 7007.98 308.51 o 3 14 0 6242.12 6077.16 285.85 o 4 14 0 410.12 418.43 123.09 o 5 14 0 2768.56 2704.19 165.96 o 6 14 0 7744.65 8001.31 379.13 o 7 14 0 2326.90 2624.74 199.79 o 2 15 0 251.48 279.24 85.12 o 3 15 0 15.77 -141.46 94.30 o 4 15 0 359.65 379.36 118.49 o -7 -14 1 371.53 482.05 119.54 o -6 -14 1 1.38 35.84 78.18 o -5 -14 1 278.89 -1.77 162.12 o -4 -14 1 134.54 220.71 99.30 o -3 -14 1 457.60 425.58 99.14 o -2 -14 1 347.14 253.61 83.49 o -1 -14 1 48.34 29.87 55.27 o 0 -14 1 259.78 352.16 81.89 o 1 -14 1 52.74 155.33 63.32 o -9 -13 1 4168.38 3855.63 371.09 o -8 -13 1 52.39 -2.32 70.34 o -7 -13 1 599.62 486.24 80.41 o -6 -13 1 6627.78 6649.49 724.58 o -5 -13 1 3105.32 3138.61 141.42 o -4 -13 1 1.14 1.91 61.10 o -3 -13 1 3261.53 3079.81 394.67 o -2 -13 1 4758.93 4991.70 212.03 o -1 -13 1 0.06 26.56 183.40 o 0 -13 1 481.05 450.36 52.72 o 1 -13 1 4599.99 4588.94 285.82 o 2 -13 1 270.61 312.58 88.79 o 3 -13 1 252.70 268.91 128.75 o 4 -13 1 1615.23 1964.47 240.35 o -10 -12 1 562.04 445.35 86.79 o -9 -12 1 5.96 108.79 139.31 o -8 -12 1 2.82 -56.52 64.27 o -7 -12 1 538.11 513.23 68.02 o -6 -12 1 536.60 409.40 80.61 o -5 -12 1 562.17 650.24 82.98 o -4 -12 1 198.27 233.96 46.08 o -3 -12 1 659.76 683.59 120.64 o -2 -12 1 511.40 503.98 43.08 o -1 -12 1 419.10 395.09 66.14 o 0 -12 1 155.00 142.93 31.12 o 1 -12 1 67.20 -5.45 45.77 o 2 -12 1 460.68 472.35 81.44 o 3 -12 1 12.95 -21.56 45.67 o 4 -12 1 0.17 10.11 37.81 o 5 -12 1 281.78 103.80 205.14 o -11 -11 1 3325.06 3106.02 193.85 o -10 -11 1 1965.54 1919.81 275.56 o -9 -11 1 152.38 135.03 69.49 o -8 -11 1 4681.40 4746.56 169.24 o -7 -11 1 11164.23 10963.25 261.83 o -6 -11 1 18.02 -60.00 139.01 o -5 -11 1 1980.00 1872.61 67.52 o -4 -11 1 15688.29 15674.95 380.13 o -3 -11 1 5178.36 5247.60 104.69 o -2 -11 1 293.47 250.18 33.03 o -1 -11 1 6801.69 7094.57 232.09 o 0 -11 1 16990.85 17495.53 284.09 o 1 -11 1 704.84 655.52 70.73 o 2 -11 1 1955.11 2029.83 137.32 o 3 -11 1 11951.08 12056.13 608.85 o 4 -11 1 3197.52 3244.30 88.85 o 5 -11 1 19.46 -21.74 41.44 o 6 -11 1 2293.35 1989.38 209.74 o 7 -11 1 6274.95 5975.47 470.60 o -12 -10 1 354.11 583.93 117.75 o -11 -10 1 487.00 583.80 106.67 o -10 -10 1 735.22 899.85 330.98 o -9 -10 1 8.09 -23.27 58.72 o -8 -10 1 651.08 624.04 71.65 o -7 -10 1 336.98 370.90 125.54 o -6 -10 1 1254.89 1288.32 120.64 o -5 -10 1 1514.59 1418.40 58.74 o -4 -10 1 661.07 684.27 44.84 o -3 -10 1 2160.61 2058.82 119.11 o -2 -10 1 0.65 29.44 42.56 o -1 -10 1 1026.79 1067.56 80.07 o 0 -10 1 667.62 719.63 49.14 o 1 -10 1 103.04 120.33 52.36 o 2 -10 1 179.17 145.77 26.56 o 3 -10 1 47.64 62.69 22.78 o 4 -10 1 290.45 280.31 30.37 o 5 -10 1 168.73 197.96 28.98 o 6 -10 1 21.20 -18.06 45.62 o 7 -10 1 287.37 245.25 58.79 o 8 -10 1 380.00 400.74 66.54 o -12 -9 1 128.67 108.85 118.86 o -11 -9 1 1670.92 1827.95 310.01 o -10 -9 1 7242.72 7932.72 457.13 o -9 -9 1 73.90 92.52 56.52 o -8 -9 1 752.38 810.10 63.87 o -7 -9 1 11551.93 11512.54 233.87 o -6 -9 1 1602.44 1705.41 64.38 o -5 -9 1 60.58 108.58 33.37 o -4 -9 1 219.52 302.11 36.02 o -3 -9 1 7258.92 7226.78 326.08 o -2 -9 1 99.78 15.23 25.98 o -1 -9 1 76.36 84.99 27.98 o 0 -9 1 7193.65 7223.31 178.05 o 1 -9 1 10.40 12.32 23.92 o 2 -9 1 3310.40 3481.13 110.84 o 3 -9 1 1940.69 1992.78 139.16 o 4 -9 1 4206.98 4071.66 133.96 o 5 -9 1 3267.46 3269.60 91.96 o 6 -9 1 476.08 459.36 38.58 o 7 -9 1 2489.32 2407.90 298.53 o 8 -9 1 117.05 -4.44 93.23 o 9 -9 1 2174.39 2058.44 132.73 o -13 -8 1 1.53 -2.38 97.67 o -12 -8 1 241.30 343.43 100.88 o -11 -8 1 2286.60 2281.87 145.15 o -10 -8 1 42.11 40.31 73.18 o -9 -8 1 49.64 12.25 45.58 o -8 -8 1 2578.54 2576.66 98.59 o -7 -8 1 154.09 164.99 44.56 o -6 -8 1 156.35 253.31 39.75 o -5 -8 1 2.85 -53.54 35.69 o -4 -8 1 2448.79 2460.20 82.52 o -3 -8 1 324.35 368.93 26.47 o -2 -8 1 572.28 624.60 31.12 o -1 -8 1 1389.51 1463.15 73.64 o 0 -8 1 16.43 -32.37 30.62 o 1 -8 1 468.22 438.44 47.15 o 2 -8 1 5.59 44.16 24.83 o 3 -8 1 310.56 308.87 25.87 o 4 -8 1 628.92 627.15 34.17 o 5 -8 1 196.70 230.26 99.36 o 6 -8 1 126.03 179.19 29.09 o 7 -8 1 1070.94 1047.77 42.95 o 8 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