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The Sn atom of the monomeric title compound, [Sn(C10H13)3(C6H4NO3)], adopts a distorted SnOC3 tetra­hedral geometry.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806015662/hb2043sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806015662/hb2043Isup2.hkl
Contains datablock I

CCDC reference: 610780

Key indicators

  • Single-crystal X-ray study
  • T = 273 K
  • Mean [sigma](C-C) = 0.004 Å
  • R factor = 0.024
  • wR factor = 0.062
  • Data-to-parameter ratio = 18.1

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N1
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 2 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion

Computing details top

Data collection: SMART (Bruker, 2002); cell refinement: SAINT (Bruker, 2002); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 (Farrugia, 1997); software used to prepare material for publication: SHELXL97.

Tris(2-methyl-2-phenylpropyl)(4-nitrophenolato)tin(IV) top
Crystal data top
[Sn(C10H13)3(C6H4NO3)]Z = 2
Mr = 656.40F(000) = 680
Triclinic, P1Dx = 1.322 Mg m3
Hall symbol: -P 1Mo Kα radiation, λ = 0.71073 Å
a = 9.9002 (4) ÅCell parameters from 6938 reflections
b = 12.1230 (5) Åθ = 2.3–28.3°
c = 14.4012 (6) ŵ = 0.81 mm1
α = 86.585 (1)°T = 273 K
β = 75.938 (1)°Plate, pale yellow
γ = 79.725 (1)°0.32 × 0.25 × 0.09 mm
V = 1649.51 (12) Å3
Data collection top
Bruker SMART APEX CCD
diffractometer
6787 independent reflections
Radiation source: fine-focus sealed tube6450 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.018
φ and ω scansθmax = 26.5°, θmin = 1.5°
Absorption correction: multi-scan
(SADABS; Bruker, 2002)
h = 1212
Tmin = 0.782, Tmax = 0.931k = 1515
17940 measured reflectionsl = 1818
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.024Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.062H-atom parameters constrained
S = 1.05 w = 1/[σ2(Fo2) + (0.0359P)2 + 0.293P]
where P = (Fo2 + 2Fc2)/3
6787 reflections(Δ/σ)max = 0.001
376 parametersΔρmax = 0.33 e Å3
23 restraintsΔρmin = 0.29 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Sn10.128418 (11)0.738588 (9)0.307856 (8)0.04210 (5)
N10.4796 (2)0.7744 (2)0.68518 (15)0.0837 (7)
O10.03682 (15)0.65426 (12)0.42716 (10)0.0627 (4)
O20.4982 (3)0.8587 (3)0.7324 (2)0.1335 (10)
O30.5672 (2)0.7140 (2)0.69375 (15)0.1146 (8)
C10.0868 (2)0.68588 (16)0.48845 (13)0.0513 (4)
C20.1204 (2)0.78684 (19)0.53586 (17)0.0686 (6)
H2A0.05560.83580.52410.082*
C30.2490 (3)0.8158 (2)0.60038 (17)0.0723 (6)
H30.27060.88360.63210.087*
C40.3436 (2)0.7439 (2)0.61692 (14)0.0604 (5)
C50.3134 (2)0.6427 (2)0.57153 (16)0.0644 (5)
H50.37890.59420.58390.077*
C60.1853 (2)0.61386 (18)0.50773 (15)0.0607 (5)
H60.16420.54540.47710.073*
C70.05356 (19)0.81330 (16)0.25572 (15)0.0523 (4)
H7A0.04720.77760.19600.063*
H7B0.13640.79420.30100.063*
C80.0805 (2)0.94098 (16)0.23794 (15)0.0545 (4)
C90.1851 (2)0.9665 (2)0.1728 (2)0.0768 (7)
H9A0.20791.04610.16360.115*
H9B0.26980.93740.20220.115*
H9C0.14300.93190.11190.115*
C100.1474 (3)0.9985 (2)0.3338 (2)0.0861 (8)
H10A0.08020.98750.37310.129*
H10B0.22910.96680.36570.129*
H10C0.17501.07730.32290.129*
C110.0562 (2)0.98155 (16)0.18709 (15)0.0531 (4)
C120.1473 (3)0.9209 (2)0.11120 (17)0.0691 (6)
H120.12340.85640.09240.083*
C130.2726 (3)0.9542 (3)0.0628 (2)0.0927 (8)
H130.33190.91190.01240.111*
C140.3094 (4)1.0488 (3)0.0890 (3)0.1045 (10)
H140.39421.07090.05700.125*
C150.2211 (4)1.1110 (3)0.1624 (3)0.1009 (10)
H150.24551.17610.17960.121*
C160.0947 (3)1.07826 (19)0.2118 (2)0.0756 (7)
H160.03581.12160.26170.091*
C170.2438 (2)0.84692 (16)0.35988 (15)0.0527 (4)
H17A0.27110.90120.30960.063*
H17B0.17990.88820.41340.063*
C180.3779 (2)0.79017 (17)0.39257 (15)0.0564 (5)
C190.3341 (3)0.7147 (2)0.47930 (17)0.0801 (7)
H19A0.29710.65390.46040.120*
H19B0.26290.75740.52750.120*
H19C0.41480.68540.50460.120*
C200.4481 (3)0.8814 (2)0.4227 (2)0.0793 (7)
H20A0.53210.84690.44230.119*
H20B0.38370.92250.47510.119*
H20C0.47240.93170.36960.119*
C210.4839 (2)0.72585 (18)0.30927 (16)0.0574 (5)
C220.5161 (3)0.7755 (2)0.21933 (18)0.0724 (6)
H220.47520.84950.21060.087*
C230.6080 (3)0.7178 (3)0.1415 (2)0.0948 (9)
H230.62810.75360.08210.114*
C240.6685 (3)0.6094 (3)0.1522 (3)0.1001 (11)
H240.72640.56980.09980.120*
C250.6433 (3)0.5594 (3)0.2406 (3)0.0967 (10)
H250.68760.48640.24880.116*
C260.5515 (3)0.6170 (2)0.3192 (2)0.0766 (7)
H260.53570.58150.37900.092*
C270.25668 (18)0.59189 (15)0.23748 (13)0.0453 (4)
H27A0.34230.61400.19810.054*
H27B0.28440.54050.28640.054*
C280.19556 (19)0.52582 (14)0.17375 (13)0.0455 (4)
C290.3036 (3)0.41778 (17)0.14298 (16)0.0638 (5)
H29A0.27160.37720.09960.096*
H29B0.31260.37170.19850.096*
H29C0.39370.43740.11180.096*
C300.0574 (2)0.4917 (2)0.23224 (16)0.0645 (5)
H30A0.01290.55750.24870.097*
H30B0.07350.45290.28970.097*
H30C0.02520.44330.19500.097*
C310.17821 (18)0.59336 (14)0.08306 (12)0.0444 (4)
C320.2944 (2)0.63137 (17)0.02252 (14)0.0569 (5)
H320.38100.61720.03910.068*
C330.2833 (3)0.6896 (2)0.06150 (16)0.0720 (6)
H330.36240.71320.10110.086*
C340.1563 (3)0.7127 (2)0.08674 (17)0.0784 (7)
H340.14880.75200.14320.094*
C350.0408 (3)0.6775 (2)0.02833 (19)0.0758 (7)
H350.04580.69380.04490.091*
C360.0511 (2)0.61767 (18)0.05555 (16)0.0592 (5)
H360.02860.59350.09400.071*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Sn10.03973 (7)0.04147 (7)0.04277 (8)0.00435 (5)0.00626 (5)0.00444 (5)
N10.0561 (12)0.1186 (19)0.0593 (12)0.0065 (12)0.0012 (9)0.0180 (12)
O10.0603 (8)0.0576 (8)0.0547 (8)0.0004 (6)0.0066 (6)0.0071 (6)
O20.0933 (16)0.148 (2)0.1207 (19)0.0149 (15)0.0300 (14)0.0350 (18)
O30.0626 (11)0.186 (2)0.0842 (14)0.0280 (14)0.0033 (10)0.0177 (14)
C10.0535 (10)0.0514 (10)0.0418 (9)0.0016 (8)0.0043 (8)0.0072 (8)
C20.0663 (13)0.0611 (13)0.0704 (14)0.0173 (10)0.0056 (11)0.0077 (10)
C30.0755 (15)0.0639 (13)0.0648 (13)0.0039 (11)0.0042 (11)0.0108 (11)
C40.0505 (10)0.0780 (14)0.0427 (10)0.0040 (10)0.0054 (8)0.0119 (9)
C50.0557 (11)0.0742 (14)0.0631 (12)0.0168 (10)0.0140 (10)0.0182 (11)
C60.0667 (12)0.0546 (11)0.0581 (11)0.0102 (9)0.0108 (10)0.0028 (9)
C70.0440 (9)0.0485 (10)0.0641 (11)0.0073 (8)0.0126 (8)0.0002 (8)
C80.0488 (10)0.0464 (10)0.0651 (12)0.0015 (8)0.0132 (9)0.0061 (9)
C90.0598 (13)0.0658 (14)0.1077 (19)0.0015 (11)0.0365 (13)0.0075 (13)
C100.0825 (17)0.0735 (16)0.0855 (17)0.0062 (13)0.0032 (14)0.0237 (13)
C110.0582 (11)0.0434 (9)0.0604 (11)0.0064 (8)0.0223 (9)0.0048 (8)
C120.0670 (13)0.0752 (15)0.0653 (13)0.0202 (11)0.0099 (11)0.0024 (11)
C130.0774 (17)0.117 (2)0.0805 (18)0.0340 (17)0.0023 (14)0.0085 (16)
C140.090 (2)0.117 (3)0.112 (2)0.0499 (19)0.0200 (18)0.038 (2)
C150.123 (3)0.0718 (17)0.132 (3)0.0499 (18)0.060 (2)0.0266 (18)
C160.0946 (18)0.0495 (12)0.0921 (17)0.0174 (12)0.0379 (14)0.0056 (11)
C170.0506 (10)0.0483 (10)0.0596 (11)0.0052 (8)0.0132 (8)0.0131 (8)
C180.0571 (11)0.0586 (11)0.0583 (11)0.0084 (9)0.0211 (9)0.0112 (9)
C190.0848 (17)0.0990 (19)0.0608 (13)0.0146 (14)0.0276 (12)0.0044 (13)
C200.0748 (15)0.0820 (17)0.0920 (18)0.0138 (13)0.0322 (14)0.0334 (14)
C210.0424 (9)0.0608 (11)0.0743 (13)0.0078 (8)0.0211 (9)0.0171 (10)
C220.0635 (13)0.0740 (15)0.0775 (15)0.0200 (11)0.0037 (11)0.0119 (12)
C230.0713 (16)0.122 (3)0.0881 (19)0.0361 (17)0.0088 (14)0.0301 (18)
C240.0529 (14)0.124 (3)0.121 (3)0.0183 (16)0.0011 (15)0.056 (2)
C250.0596 (15)0.0800 (18)0.153 (3)0.0135 (13)0.0366 (18)0.047 (2)
C260.0636 (13)0.0712 (15)0.1017 (19)0.0007 (11)0.0372 (13)0.0163 (13)
C270.0413 (8)0.0485 (9)0.0455 (9)0.0018 (7)0.0116 (7)0.0084 (7)
C280.0485 (9)0.0425 (9)0.0461 (9)0.0079 (7)0.0113 (7)0.0046 (7)
C290.0841 (15)0.0434 (10)0.0614 (12)0.0043 (10)0.0214 (11)0.0082 (9)
C300.0700 (13)0.0679 (13)0.0613 (12)0.0305 (11)0.0136 (10)0.0010 (10)
C310.0486 (9)0.0406 (8)0.0441 (9)0.0048 (7)0.0111 (7)0.0091 (7)
C320.0534 (11)0.0584 (11)0.0528 (11)0.0039 (9)0.0045 (8)0.0032 (9)
C330.0858 (16)0.0698 (14)0.0509 (12)0.0105 (12)0.0005 (11)0.0010 (10)
C340.120 (2)0.0617 (14)0.0541 (12)0.0022 (14)0.0324 (14)0.0003 (10)
C350.0876 (17)0.0736 (15)0.0780 (16)0.0031 (13)0.0490 (14)0.0056 (12)
C360.0583 (11)0.0627 (12)0.0636 (12)0.0131 (9)0.0243 (10)0.0060 (10)
Geometric parameters (Å, º) top
Sn1—O12.0454 (13)C18—C191.525 (3)
Sn1—C272.1415 (17)C18—C211.535 (3)
Sn1—C72.1504 (18)C18—C201.541 (3)
Sn1—C172.1584 (18)C19—H19A0.9600
N1—O31.211 (3)C19—H19B0.9600
N1—O21.223 (4)C19—H19C0.9600
N1—C41.462 (3)C20—H20A0.9600
O1—C11.331 (2)C20—H20B0.9600
C1—C21.385 (3)C20—H20C0.9600
C1—C61.390 (3)C21—C221.385 (3)
C2—C31.383 (3)C21—C261.385 (3)
C2—H2A0.9300C22—C231.395 (4)
C3—C41.361 (3)C22—H220.9300
C3—H30.9300C23—C241.359 (4)
C4—C51.375 (3)C23—H230.9300
C5—C61.374 (3)C24—C251.363 (4)
C5—H50.9300C24—H240.9300
C6—H60.9300C25—C261.401 (4)
C7—C81.540 (3)C25—H250.9300
C7—H7A0.9700C26—H260.9300
C7—H7B0.9700C27—C281.543 (2)
C8—C111.524 (3)C27—H27A0.9700
C8—C101.529 (3)C27—H27B0.9700
C8—C91.541 (3)C28—C311.529 (2)
C9—H9A0.9600C28—C301.534 (3)
C9—H9B0.9600C28—C291.548 (3)
C9—H9C0.9600C29—H29A0.9600
C10—H10A0.9600C29—H29B0.9600
C10—H10B0.9600C29—H29C0.9600
C10—H10C0.9600C30—H30A0.9600
C11—C161.386 (3)C30—H30B0.9600
C11—C121.388 (3)C30—H30C0.9600
C12—C131.383 (3)C31—C361.387 (3)
C12—H120.9300C31—C321.396 (3)
C13—C141.363 (4)C32—C331.382 (3)
C13—H130.9300C32—H320.9300
C14—C151.364 (4)C33—C341.369 (4)
C14—H140.9300C33—H330.9300
C15—C161.393 (4)C34—C351.364 (4)
C15—H150.9300C34—H340.9300
C16—H160.9300C35—C361.387 (3)
C17—C181.548 (3)C35—H350.9300
C17—H17A0.9700C36—H360.9300
C17—H17B0.9700
O1—Sn1—C2795.05 (6)C19—C18—C20108.49 (19)
O1—Sn1—C7101.12 (7)C21—C18—C20108.07 (18)
C27—Sn1—C7117.47 (7)C19—C18—C17108.64 (18)
O1—Sn1—C17104.58 (7)C21—C18—C17109.99 (16)
C27—Sn1—C17114.52 (7)C20—C18—C17109.00 (18)
C7—Sn1—C17118.62 (7)C18—C19—H19A109.5
O3—N1—O2123.1 (2)C18—C19—H19B109.5
O3—N1—C4118.6 (3)H19A—C19—H19B109.5
O2—N1—C4118.2 (3)C18—C19—H19C109.5
C1—O1—Sn1127.98 (12)H19A—C19—H19C109.5
O1—C1—C2122.63 (19)H19B—C19—H19C109.5
O1—C1—C6118.97 (19)C18—C20—H20A109.5
C2—C1—C6118.38 (19)C18—C20—H20B109.5
C3—C2—C1120.9 (2)H20A—C20—H20B109.5
C3—C2—H2A119.6C18—C20—H20C109.5
C1—C2—H2A119.6H20A—C20—H20C109.5
C4—C3—C2119.3 (2)H20B—C20—H20C109.5
C4—C3—H3120.4C22—C21—C26116.7 (2)
C2—C3—H3120.4C22—C21—C18120.6 (2)
C3—C4—C5121.37 (19)C26—C21—C18122.7 (2)
C3—C4—N1119.2 (2)C21—C22—C23121.8 (3)
C5—C4—N1119.4 (2)C21—C22—H22119.1
C6—C5—C4119.3 (2)C23—C22—H22119.1
C6—C5—H5120.3C24—C23—C22120.3 (3)
C4—C5—H5120.3C24—C23—H23119.9
C5—C6—C1120.8 (2)C22—C23—H23119.9
C5—C6—H6119.6C23—C24—C25119.4 (3)
C1—C6—H6119.6C23—C24—H24120.3
C8—C7—Sn1119.11 (13)C25—C24—H24120.3
C8—C7—H7A107.5C24—C25—C26120.7 (3)
Sn1—C7—H7A107.5C24—C25—H25119.7
C8—C7—H7B107.5C26—C25—H25119.7
Sn1—C7—H7B107.5C21—C26—C25121.0 (3)
H7A—C7—H7B107.0C21—C26—H26119.5
C11—C8—C10112.02 (19)C25—C26—H26119.5
C11—C8—C7110.64 (15)C28—C27—Sn1119.13 (11)
C10—C8—C7108.70 (19)C28—C27—H27A107.5
C11—C8—C9108.48 (18)Sn1—C27—H27A107.5
C10—C8—C9109.03 (19)C28—C27—H27B107.5
C7—C8—C9107.88 (17)Sn1—C27—H27B107.5
C8—C9—H9A109.5H27A—C27—H27B107.0
C8—C9—H9B109.5C31—C28—C30113.08 (16)
H9A—C9—H9B109.5C31—C28—C27110.62 (14)
C8—C9—H9C109.5C30—C28—C27109.49 (15)
H9A—C9—H9C109.5C31—C28—C29107.77 (15)
H9B—C9—H9C109.5C30—C28—C29108.23 (17)
C8—C10—H10A109.5C27—C28—C29107.45 (15)
C8—C10—H10B109.5C28—C29—H29A109.5
H10A—C10—H10B109.5C28—C29—H29B109.5
C8—C10—H10C109.5H29A—C29—H29B109.5
H10A—C10—H10C109.5C28—C29—H29C109.5
H10B—C10—H10C109.5H29A—C29—H29C109.5
C16—C11—C12117.3 (2)H29B—C29—H29C109.5
C16—C11—C8123.2 (2)C28—C30—H30A109.5
C12—C11—C8119.47 (18)C28—C30—H30B109.5
C13—C12—C11121.7 (2)H30A—C30—H30B109.5
C13—C12—H12119.2C28—C30—H30C109.5
C11—C12—H12119.2H30A—C30—H30C109.5
C14—C13—C12120.1 (3)H30B—C30—H30C109.5
C14—C13—H13119.9C36—C31—C32117.01 (18)
C12—C13—H13119.9C36—C31—C28123.02 (17)
C13—C14—C15119.5 (3)C32—C31—C28119.95 (16)
C13—C14—H14120.2C33—C32—C31121.4 (2)
C15—C14—H14120.2C33—C32—H32119.3
C14—C15—C16120.9 (3)C31—C32—H32119.3
C14—C15—H15119.5C34—C33—C32120.3 (2)
C16—C15—H15119.5C34—C33—H33119.8
C11—C16—C15120.4 (3)C32—C33—H33119.8
C11—C16—H16119.8C35—C34—C33119.4 (2)
C15—C16—H16119.8C35—C34—H34120.3
C18—C17—Sn1116.96 (13)C33—C34—H34120.3
C18—C17—H17A108.1C34—C35—C36120.7 (2)
Sn1—C17—H17A108.1C34—C35—H35119.6
C18—C17—H17B108.1C36—C35—H35119.6
Sn1—C17—H17B108.1C35—C36—C31121.1 (2)
H17A—C17—H17B107.3C35—C36—H36119.5
C19—C18—C21112.57 (19)C31—C36—H36119.5
C27—Sn1—O1—C1155.95 (18)C27—Sn1—C17—C1831.65 (17)
C7—Sn1—O1—C136.66 (19)C7—Sn1—C17—C18177.37 (14)
C17—Sn1—O1—C187.08 (18)Sn1—C17—C18—C1964.4 (2)
Sn1—O1—C1—C255.7 (3)Sn1—C17—C18—C2159.2 (2)
Sn1—O1—C1—C6125.93 (18)Sn1—C17—C18—C20177.54 (16)
O1—C1—C2—C3178.8 (2)C19—C18—C21—C22168.3 (2)
C6—C1—C2—C30.4 (3)C20—C18—C21—C2271.9 (2)
C1—C2—C3—C40.2 (4)C17—C18—C21—C2247.0 (2)
C2—C3—C4—C50.7 (4)C19—C18—C21—C2611.5 (3)
C2—C3—C4—N1180.0 (2)C20—C18—C21—C26108.3 (2)
O3—N1—C4—C3174.3 (2)C17—C18—C21—C26132.8 (2)
O2—N1—C4—C37.2 (3)C26—C21—C22—C232.2 (3)
O3—N1—C4—C56.4 (3)C18—C21—C22—C23177.6 (2)
O2—N1—C4—C5172.1 (2)C21—C22—C23—C240.4 (4)
C3—C4—C5—C60.4 (3)C22—C23—C24—C252.9 (4)
N1—C4—C5—C6179.69 (19)C23—C24—C25—C262.7 (4)
C4—C5—C6—C10.3 (3)C22—C21—C26—C252.4 (3)
O1—C1—C6—C5179.10 (18)C18—C21—C26—C25177.4 (2)
C2—C1—C6—C50.7 (3)C24—C25—C26—C210.0 (4)
O1—Sn1—C7—C8125.50 (15)O1—Sn1—C27—C2888.13 (14)
C27—Sn1—C7—C8132.77 (15)C7—Sn1—C27—C2817.19 (16)
C17—Sn1—C7—C811.95 (18)C17—Sn1—C27—C28163.32 (13)
Sn1—C7—C8—C1143.9 (2)Sn1—C27—C28—C3169.36 (17)
Sn1—C7—C8—C1079.5 (2)Sn1—C27—C28—C3055.91 (19)
Sn1—C7—C8—C9162.39 (15)Sn1—C27—C28—C29173.25 (13)
C10—C8—C11—C1615.8 (3)C30—C28—C31—C362.0 (2)
C7—C8—C11—C16137.3 (2)C27—C28—C31—C36125.21 (18)
C9—C8—C11—C16104.6 (2)C29—C28—C31—C36117.6 (2)
C10—C8—C11—C12165.2 (2)C30—C28—C31—C32179.51 (17)
C7—C8—C11—C1243.7 (3)C27—C28—C31—C3256.3 (2)
C9—C8—C11—C1274.5 (2)C29—C28—C31—C3260.9 (2)
C16—C11—C12—C131.0 (4)C36—C31—C32—C330.6 (3)
C8—C11—C12—C13179.9 (2)C28—C31—C32—C33177.95 (18)
C11—C12—C13—C140.2 (5)C31—C32—C33—C340.8 (3)
C12—C13—C14—C150.7 (5)C32—C33—C34—C350.1 (4)
C13—C14—C15—C160.9 (5)C33—C34—C35—C360.7 (4)
C12—C11—C16—C150.8 (3)C34—C35—C36—C310.9 (4)
C8—C11—C16—C15179.9 (2)C32—C31—C36—C350.2 (3)
C14—C15—C16—C110.1 (4)C28—C31—C36—C35178.77 (19)
O1—Sn1—C17—C1870.98 (15)
 

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