# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' B in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 447.64 _exptl_crystal_F_000 1364.00 _reflns_d_resolution_high 0.7964 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.0919 _cell_length_b 13.9901 _cell_length_c 18.2073 _cell_angle_alpha 112.456 _cell_angle_beta 104.944 _cell_angle_gamma 90.641 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 628.18 627.37 43.71 o 2 0 0 31.26 34.35 22.55 o 3 0 0 198.64 153.15 65.41 o 4 0 0 13347.42 12951.20 534.11 o 5 0 0 2922.16 2941.06 149.39 o 6 0 0 148.59 144.44 41.16 o 7 0 0 4812.56 4935.35 243.22 o 8 0 0 2293.70 2468.58 202.15 o 9 0 0 1385.68 1486.50 197.09 o 10 0 0 2829.33 2903.16 199.41 o 11 0 0 158.98 170.05 96.38 o 12 0 0 3371.80 4576.09 551.75 o 13 0 0 72.18 -177.22 118.15 o 14 0 0 138.34 295.47 201.46 o 15 0 0 102.30 -210.17 140.11 o -15 1 0 295.85 637.84 249.95 o -14 1 0 980.85 1062.74 275.08 o -13 1 0 164.56 423.91 183.06 o -12 1 0 0.74 -68.09 75.97 o -11 1 0 4415.09 4376.84 264.86 o -10 1 0 37.65 13.83 54.34 o -9 1 0 2562.75 2762.77 184.52 o -8 1 0 1350.13 1518.39 196.82 o -7 1 0 140.46 298.49 149.81 o -6 1 0 512.02 603.34 66.65 o -5 1 0 31.59 -5.77 29.02 o -4 1 0 13067.55 13240.20 544.86 o -3 1 0 523.16 547.92 47.77 o -2 1 0 53362.62 52963.50 2080.06 o -1 1 0 1912.54 1785.55 80.60 o 0 1 0 7157.71 7157.65 286.74 o 1 1 0 32687.62 33200.55 1306.48 o 2 1 0 158.63 171.22 22.93 o 3 1 0 21566.46 22910.51 916.50 o 4 1 0 1853.63 2068.04 114.48 o 5 1 0 1270.51 1450.69 98.42 o 6 1 0 3.16 0.18 27.22 o 7 1 0 343.66 483.27 64.56 o 8 1 0 6033.98 5738.07 282.48 o 9 1 0 4974.75 4535.46 268.94 o 10 1 0 4049.00 3980.77 238.28 o 11 1 0 52.43 115.94 86.63 o 12 1 0 17.79 44.28 86.01 o 13 1 0 2206.23 2094.80 375.02 o 14 1 0 20.55 -14.64 161.09 o 15 1 0 241.93 382.15 226.60 o -15 2 0 54.00 319.22 149.61 o -13 2 0 1370.36 1585.60 216.34 o -12 2 0 225.04 382.95 121.82 o -11 2 0 22.88 37.17 54.57 o -10 2 0 719.13 733.47 125.77 o -9 2 0 0.81 -25.32 58.75 o -8 2 0 185.38 98.46 46.53 o -7 2 0 4088.28 3881.31 200.43 o -6 2 0 130.60 180.24 55.03 o -5 2 0 43114.66 43069.37 1714.31 o -4 2 0 52.28 -10.97 28.06 o -3 2 0 38821.63 39853.12 1579.29 o -2 2 0 22152.68 21877.33 871.89 o -1 2 0 56303.29 57958.40 2277.40 o 0 2 0 2410.15 2212.89 124.78 o 1 2 0 4532.02 4847.40 205.10 o 2 2 0 2216.31 2472.70 119.60 o 3 2 0 7386.40 6476.01 276.84 o 4 2 0 7124.00 6887.35 300.07 o 5 2 0 18824.18 19075.72 783.60 o 6 2 0 472.16 567.11 65.91 o 7 2 0 5458.28 5230.51 255.70 o 8 2 0 1134.44 1197.97 111.35 o 9 2 0 2974.55 3004.53 283.65 o 10 2 0 3142.64 3013.20 410.35 o 11 2 0 1693.91 1695.39 242.23 o 12 2 0 10.42 42.38 90.36 o 13 2 0 379.90 258.26 195.13 o 14 2 0 15.23 11.08 166.44 o 15 2 0 0.58 -71.44 174.35 o -15 3 0 291.16 386.90 173.76 o -14 3 0 83.12 122.50 129.43 o -13 3 0 35.42 123.51 94.50 o -12 3 0 1456.78 1504.69 199.08 o -11 3 0 945.55 1111.64 162.38 o -10 3 0 1.61 23.55 65.75 o -9 3 0 1312.18 1389.13 149.93 o -8 3 0 2230.88 2363.88 160.65 o -7 3 0 1077.78 1080.93 98.45 o -6 3 0 19981.63 19066.02 790.75 o -5 3 0 2042.46 2147.37 127.74 o -4 3 0 22323.91 21986.35 892.52 o -3 3 0 1156.53 1525.19 94.36 o -2 3 0 16740.63 16641.21 675.49 o -1 3 0 19107.30 20491.21 822.68 o 0 3 0 19047.75 20065.21 805.47 o 1 3 0 10391.40 9701.56 402.64 o 2 3 0 3164.68 2942.08 141.58 o 3 3 0 3823.88 4151.99 191.43 o 4 3 0 1953.93 2326.64 172.94 o 5 3 0 461.26 685.04 66.90 o 6 3 0 11520.89 10953.78 473.20 o 7 3 0 418.95 410.64 62.05 o 8 3 0 10042.66 9134.81 725.71 o 9 3 0 580.89 496.89 109.47 o 10 3 0 386.24 542.69 118.35 o 11 3 0 681.77 374.23 146.15 o 12 3 0 513.31 617.48 139.32 o 13 3 0 263.22 35.23 167.03 o 14 3 0 23.12 -207.80 162.28 o 15 3 0 99.83 -246.98 200.67 o -15 4 0 772.31 736.99 212.94 o -14 4 0 5.82 129.83 217.79 o -13 4 0 294.93 600.86 147.25 o -12 4 0 144.15 168.49 96.18 o -11 4 0 20.66 -14.49 101.13 o -10 4 0 207.22 55.11 74.89 o -9 4 0 35.82 56.08 53.25 o -8 4 0 10128.99 10086.02 456.12 o -7 4 0 5214.71 4833.22 243.92 o -6 4 0 9878.23 9630.59 423.99 o -5 4 0 2720.88 2662.54 151.59 o -4 4 0 3437.93 3475.77 173.33 o -3 4 0 15809.69 16230.58 667.28 o -2 4 0 10972.66 10294.73 433.84 o -1 4 0 790.01 1052.65 78.71 o 0 4 0 7254.90 7353.14 318.24 o 1 4 0 723.76 786.79 110.81 o 2 4 0 970.33 885.77 71.98 o 3 4 0 3191.26 2972.00 290.44 o 4 4 0 43185.02 44026.55 1757.19 o 5 4 0 27945.00 27356.70 1110.39 o 6 4 0 3264.03 3406.63 186.36 o 7 4 0 3429.49 3957.42 299.65 o 8 4 0 1079.01 851.60 307.74 o 9 4 0 2828.05 3489.21 407.08 o 10 4 0 82.65 59.34 79.39 o 11 4 0 250.71 210.74 202.75 o 12 4 0 243.94 312.89 126.29 o 13 4 0 57.00 274.67 126.04 o 14 4 0 100.29 -47.69 174.95 o -15 5 0 2.54 -115.18 184.25 o -14 5 0 31.02 85.73 108.05 o -13 5 0 63.04 112.18 120.72 o -12 5 0 608.41 852.72 156.67 o -11 5 0 1223.97 1417.80 191.47 o -10 5 0 889.72 919.39 153.17 o -9 5 0 1086.47 1106.25 119.24 o -8 5 0 924.12 1137.88 114.56 o -7 5 0 14847.09 14987.92 644.73 o -6 5 0 9481.67 9973.75 443.74 o -5 5 0 8018.41 8434.28 376.94 o -4 5 0 3.56 -13.00 30.86 o -3 5 0 4440.61 4368.40 211.72 o -2 5 0 24416.02 25132.90 1020.06 o -1 5 0 2601.64 2363.24 132.16 o 0 5 0 2897.14 2968.88 155.64 o 1 5 0 15036.44 14941.71 762.80 o 2 5 0 3712.08 3348.11 222.55 o 3 5 0 1132.00 1192.39 104.20 o 4 5 0 4311.28 4410.29 296.15 o 5 5 0 11218.79 11210.67 486.17 o 6 5 0 2577.48 2577.48 574.71 o 7 5 0 6904.64 6986.99 479.42 o 8 5 0 364.07 236.24 89.13 o 9 5 0 18.71 74.75 77.30 o 10 5 0 748.74 717.24 244.31 o 11 5 0 32.97 215.46 100.83 o 12 5 0 186.65 135.50 102.46 o 13 5 0 850.54 972.87 201.17 o 14 5 0 65.06 -150.80 189.00 o -15 6 0 151.39 173.96 243.42 o -14 6 0 58.45 101.92 191.17 o -13 6 0 567.23 485.06 223.04 o -12 6 0 36.95 22.26 99.34 o -11 6 0 7.30 100.97 83.87 o -10 6 0 2559.77 2744.88 268.55 o -9 6 0 2208.25 2871.30 277.39 o -8 6 0 3844.08 3982.28 238.17 o -7 6 0 1917.12 2252.51 164.69 o -6 6 0 4979.63 5118.37 399.71 o -5 6 0 0.31 16.09 39.40 o -4 6 0 8609.68 8480.29 381.66 o -3 6 0 10052.60 10652.51 464.50 o -2 6 0 548.41 751.15 85.80 o -1 6 0 2781.61 2691.38 154.38 o 0 6 0 3852.67 4385.69 217.23 o 1 6 0 341.80 457.69 62.90 o 2 6 0 28051.82 26513.12 1081.39 o 3 6 0 5162.79 5405.77 260.96 o 4 6 0 3639.74 3894.63 211.44 o 5 6 0 2981.85 3266.81 263.36 o 6 6 0 4485.16 3672.37 662.77 o 7 6 0 699.44 670.60 194.44 o 8 6 0 2596.51 3433.21 417.38 o 9 6 0 878.97 800.59 147.47 o 10 6 0 71.63 0.90 83.11 o 11 6 0 203.29 99.32 102.90 o 12 6 0 2.15 7.63 104.05 o 13 6 0 43.41 12.78 104.13 o -15 7 0 4.99 -33.05 220.86 o -14 7 0 186.11 -185.83 173.76 o -13 7 0 133.49 -40.57 153.37 o -12 7 0 1945.58 3111.22 466.85 o -11 7 0 106.78 104.29 156.34 o -10 7 0 736.38 719.08 140.09 o -9 7 0 639.24 684.55 105.35 o -8 7 0 2837.37 3295.59 218.06 o -7 7 0 4644.58 4654.14 283.64 o -6 7 0 8.25 -1.92 46.06 o -5 7 0 19.78 -19.71 42.54 o -4 7 0 1152.64 1146.59 107.58 o -3 7 0 172.12 148.00 49.42 o -2 7 0 2235.87 2349.33 251.34 o -1 7 0 3676.89 3814.89 229.93 o 0 7 0 21747.86 22276.61 923.11 o 1 7 0 371.14 401.48 76.07 o 2 7 0 22.22 41.11 42.88 o 3 7 0 10016.17 10468.33 467.79 o 4 7 0 2713.48 2291.83 229.76 o 5 7 0 6656.28 6782.56 997.92 o 6 7 0 129.72 148.74 74.21 o 7 7 0 13.93 117.29 95.69 o 8 7 0 212.83 220.33 99.62 o 9 7 0 36.88 35.15 105.09 o 10 7 0 1045.23 1479.01 214.75 o 11 7 0 20.34 52.08 289.23 o 12 7 0 1272.08 1367.85 245.00 o 13 7 0 7.10 193.37 120.60 o -14 8 0 56.30 -129.82 203.64 o -13 8 0 39.12 112.21 189.79 o -12 8 0 63.12 77.58 169.01 o -11 8 0 2324.67 2983.97 451.81 o -10 8 0 617.23 589.55 218.09 o -9 8 0 1007.59 1067.88 212.25 o -8 8 0 218.45 219.94 92.59 o -7 8 0 2126.24 2027.85 201.87 o -6 8 0 1085.41 1207.86 121.86 o -5 8 0 168.33 168.12 64.95 o -4 8 0 2071.90 2140.84 157.96 o -3 8 0 9751.24 9098.77 504.78 o -2 8 0 2836.22 2564.94 178.81 o -1 8 0 799.73 910.12 97.23 o 0 8 0 1606.55 1759.92 180.00 o 1 8 0 16839.04 16633.72 727.59 o 2 8 0 200.82 209.99 61.33 o 3 8 0 3372.29 3354.24 204.29 o 4 8 0 1683.62 1845.45 201.75 o 5 8 0 2973.57 2751.66 384.82 o 6 8 0 1647.64 1590.47 198.82 o 7 8 0 396.79 330.26 109.78 o 8 8 0 712.01 998.49 400.75 o 9 8 0 409.08 783.56 160.54 o 10 8 0 377.30 266.43 120.86 o 11 8 0 80.96 43.94 217.30 o 12 8 0 22.37 67.33 113.63 o -14 9 0 605.36 896.10 332.87 o -13 9 0 766.92 907.58 302.20 o -12 9 0 196.59 285.38 217.89 o -11 9 0 1.62 -9.70 162.68 o -10 9 0 1409.59 1919.26 361.17 o -9 9 0 6.64 -144.57 96.38 o -8 9 0 2436.01 2568.20 270.63 o -7 9 0 150.97 300.63 93.55 o -6 9 0 484.77 390.72 168.32 o -5 9 0 610.32 468.67 84.85 o -4 9 0 1160.10 852.75 122.70 o -3 9 0 1397.94 1518.97 134.43 o -2 9 0 11820.17 11934.80 534.05 o -1 9 0 3615.57 3917.38 230.42 o 0 9 0 898.73 1089.16 142.90 o 1 9 0 364.23 343.89 75.91 o 2 9 0 8840.19 8738.57 413.15 o 3 9 0 379.03 414.14 108.02 o 4 9 0 869.71 947.97 271.92 o 5 9 0 305.26 394.65 114.68 o 6 9 0 451.65 466.72 125.17 o 7 9 0 265.60 302.85 115.84 o 8 9 0 223.03 126.76 168.91 o 9 9 0 807.81 865.39 282.01 o 10 9 0 1265.30 1322.88 214.84 o 11 9 0 185.37 162.42 417.18 o 12 9 0 23.92 -3.91 110.49 o -13 10 0 492.56 627.15 283.99 o -12 10 0 597.48 481.10 269.94 o -11 10 0 381.80 514.94 234.12 o -10 10 0 50.95 -25.53 161.29 o -9 10 0 97.78 174.95 138.73 o -8 10 0 406.71 281.41 160.10 o -7 10 0 358.89 535.21 121.67 o -6 10 0 1742.24 1656.02 214.82 o -5 10 0 0.30 54.42 114.19 o -4 10 0 4353.56 3517.75 711.76 o -3 10 0 1064.04 1060.48 119.38 o -2 10 0 1111.62 1314.46 132.66 o -1 10 0 4077.49 4458.02 252.61 o 0 10 0 6093.62 6210.14 322.84 o 1 10 0 2968.01 3170.17 229.12 o 2 10 0 582.64 867.77 150.39 o 3 10 0 322.55 148.61 188.01 o 4 10 0 195.01 196.30 185.93 o 5 10 0 450.58 434.36 195.43 o 6 10 0 1341.63 1118.89 177.35 o 7 10 0 30.84 -15.79 88.06 o 8 10 0 1437.47 1561.68 393.53 o 9 10 0 211.71 362.73 134.66 o 10 10 0 165.38 155.59 209.68 o 11 10 0 601.88 857.19 210.27 o -12 11 0 7.19 139.52 250.94 o -11 11 0 424.46 471.60 251.93 o -10 11 0 211.81 67.29 164.06 o -9 11 0 297.09 153.18 154.96 o -8 11 0 131.61 38.00 132.20 o -7 11 0 1150.26 1293.09 254.30 o -6 11 0 2.33 14.37 85.81 o -5 11 0 983.76 888.83 274.39 o -4 11 0 77.39 -4.78 80.84 o -3 11 0 6227.55 6125.28 417.83 o -2 11 0 601.28 556.83 129.72 o -1 11 0 40.98 117.16 70.71 o 0 11 0 1073.66 1278.93 137.62 o 1 11 0 1760.43 1941.61 222.34 o 2 11 0 2.43 155.86 94.14 o 3 11 0 1.49 40.80 123.69 o 4 11 0 290.82 236.28 114.14 o 5 11 0 651.17 823.15 163.76 o 6 11 0 82.36 74.13 248.57 o 7 11 0 1125.21 1107.35 194.87 o 8 11 0 89.62 69.86 221.85 o 9 11 0 939.88 1506.28 232.16 o 10 11 0 0.08 -29.04 117.46 o -8 12 0 272.42 121.31 160.10 o -7 12 0 1316.81 1131.76 368.99 o -6 12 0 1631.07 1548.35 206.02 o -5 12 0 557.85 703.77 146.55 o -4 12 0 247.21 183.72 103.62 o -3 12 0 160.16 77.64 96.73 o -2 12 0 4904.65 4619.59 368.26 o -1 12 0 96.10 48.27 185.53 o 0 12 0 119.30 -127.84 140.71 o 1 12 0 573.68 717.42 146.86 o 2 12 0 696.87 903.80 276.37 o 3 12 0 0.24 -64.15 90.32 o 4 12 0 412.56 224.39 124.07 o 5 12 0 971.85 1221.49 381.46 o 6 12 0 906.46 945.00 188.80 o 7 12 0 340.57 595.29 155.67 o 8 12 0 42.63 173.01 129.23 o 9 12 0 22.09 42.01 121.78 o -11 13 0 14.32 -34.04 207.80 o -10 13 0 880.63 878.49 296.66 o -9 13 0 9.41 -70.26 165.84 o -8 13 0 558.98 1012.67 280.82 o -7 13 0 101.69 198.50 179.30 o -6 13 0 1297.30 1032.41 184.64 o -5 13 0 415.00 370.97 131.59 o -4 13 0 1307.23 1329.69 199.26 o -3 13 0 79.43 42.22 113.43 o -2 13 0 89.67 24.12 109.39 o -1 13 0 407.92 192.56 182.27 o 0 13 0 43.83 -217.30 144.86 o 1 13 0 36.51 81.73 189.99 o 2 13 0 1584.64 1755.20 380.37 o 3 13 0 16.11 -32.06 199.09 o 4 13 0 313.49 180.37 142.29 o 5 13 0 213.79 167.75 125.69 o 6 13 0 658.44 534.87 177.32 o 7 13 0 329.54 516.39 155.53 o -9 14 0 677.73 1010.88 309.52 o -8 14 0 9.32 13.46 175.74 o -7 14 0 751.89 767.07 244.21 o -6 14 0 52.95 -2.52 106.22 o -5 14 0 251.04 256.78 127.76 o -4 14 0 6.23 -43.07 111.60 o -3 14 0 729.04 533.33 148.30 o -2 14 0 255.04 522.86 234.91 o -1 14 0 309.81 109.64 195.33 o 0 14 0 321.31 172.77 212.94 o 1 14 0 172.17 95.98 208.00 o 2 14 0 17.36 -31.66 197.51 o 3 14 0 1375.69 1973.09 430.44 o 4 14 0 71.33 -82.53 215.71 o 5 14 0 1021.14 1203.25 372.65 o 6 14 0 8.40 189.39 202.45 o -7 15 0 144.30 150.80 189.79 o -6 15 0 543.89 244.21 188.40 o -5 15 0 12.85 -9.05 114.40 o -4 15 0 55.22 -66.25 119.97 o -3 15 0 194.23 598.26 244.61 o -2 15 0 354.43 534.14 247.58 o -1 15 0 79.16 142.69 208.00 o 0 15 0 371.15 290.52 237.88 o 1 15 0 1136.92 1473.38 378.98 o 2 15 0 98.47 -35.62 232.14 o 3 15 0 81.36 -120.52 261.23 o 4 15 0 532.19 1204.63 412.23 o -4 16 0 29.04 -81.93 188.40 o -3 16 0 6.59 201.07 225.21 o -2 16 0 764.71 660.00 297.45 o -1 16 0 30.12 -18.01 233.13 o 0 16 0 54.00 -98.16 237.88 o -2 -16 1 24.28 -23.55 264.00 o -1 -16 1 2.47 220.07 291.71 o 0 -16 1 998.03 929.74 326.54 o 1 -16 1 34.71 98.75 230.36 o 2 -16 1 32.00 -60.56 201.46 o 3 -16 1 267.18 483.67 250.54 o 4 -16 1 371.15 476.94 239.46 o 5 -16 1 239.11 387.29 223.04 o -5 -15 1 35.30 -7.12 308.53 o -4 -15 1 186.41 -59.96 247.18 o -3 -15 1 555.69 954.88 355.43 o -2 -15 1 121.61 66.10 240.85 o -1 -15 1 129.90 504.65 259.05 o 0 -15 1 41.57 294.28 229.17 o 1 -15 1 2103.67 2028.30 408.47 o 2 -15 1 23.44 -247.58 165.05 o 3 -15 1 690.51 493.96 226.00 o 4 -15 1 32.24 -148.91 99.27 o 5 -15 1 588.62 402.71 141.97 o 6 -15 1 66.53 116.76 182.27 o 7 -15 1 14.14 -119.53 164.65 o 8 -15 1 48.44 170.99 207.80 o -6 -14 1 32.26 22.22 134.18 o -5 -14 1 358.98 179.48 151.29 o -4 -14 1 1.00 46.31 245.99 o -3 -14 1 173.72 237.88 231.55 o -2 -14 1 1278.56 1671.09 378.39 o -1 -14 1 1332.20 983.18 318.62 o 0 -14 1 59.20 42.55 187.81 o 1 -14 1 7.62 82.72 169.60 o 2 -14 1 1020.88 717.00 250.35 o 3 -14 1 47.78 25.61 111.07 o 4 -14 1 498.78 353.39 134.50 o 5 -14 1 60.15 134.38 114.23 o 6 -14 1 74.49 110.83 159.91 o 7 -14 1 167.80 111.81 161.88 o 8 -14 1 4.09 -47.69 155.35 o 9 -14 1 106.80 259.45 212.35 o -8 -13 1 69.14 347.03 144.70 o -7 -13 1 99.74 100.21 124.58 o -6 -13 1 344.44 283.24 138.75 o -5 -13 1 160.76 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