# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' DG17 STOE IPDS MEASUREMENT P2/C' _shelx_refln_list_code 4 _shelx_F_calc_maximum 344.32 _exptl_crystal_F_000 828.00 _reflns_d_resolution_high 0.8148 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 9.8887 _cell_length_b 11.3492 _cell_length_c 14.6304 _cell_angle_alpha 90.000 _cell_angle_beta 119.701 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 1 -17 1146.28 937.21 169.72 o 4 1 -17 918.33 765.19 149.31 o 5 1 -17 1272.13 1150.05 201.97 o 6 1 -17 2089.06 1748.85 250.21 o 7 1 -17 514.93 383.69 309.67 o 8 1 -17 1539.86 1078.88 260.43 o 9 1 -17 574.22 352.18 309.67 o 3 2 -17 432.14 240.55 180.36 o 4 2 -17 492.49 456.64 152.40 o 5 2 -17 800.95 630.82 172.28 o 6 2 -17 1118.40 1007.36 178.23 o 7 2 -17 416.98 400.45 207.74 o 8 2 -17 460.46 564.57 261.53 o 4 3 -17 70.16 143.15 148.84 o 5 3 -17 203.72 191.82 175.33 o 6 3 -17 179.60 185.30 204.61 o 7 3 -17 41.20 -19.71 256.41 o 8 3 -17 238.36 132.57 311.70 o 5 4 -17 870.49 612.27 176.40 o 6 4 -17 1316.37 1358.67 252.94 o 7 4 -17 631.41 652.74 304.61 o 1 0 -16 2361.37 1781.94 221.09 o 2 0 -16 6004.35 5989.35 204.52 o 3 0 -16 2753.99 2678.69 257.90 o 4 0 -16 1343.16 1334.83 315.74 o 5 0 -16 369.11 459.45 278.30 o 6 0 -16 1248.78 895.62 286.40 o 7 0 -16 218.22 529.28 229.72 o 8 0 -16 3456.97 2419.69 263.12 o 9 0 -16 3248.29 2705.08 271.22 o 10 0 -16 2619.52 2209.20 332.95 o 1 1 -16 54.08 227.52 189.35 o 2 1 -16 75.34 111.90 146.03 o 3 1 -16 59.44 48.76 145.24 o 4 1 -16 2.78 -37.31 149.14 o 5 1 -16 119.80 57.33 159.46 o 6 1 -16 626.22 358.57 197.41 o 7 1 -16 198.24 75.30 197.78 o 8 1 -16 582.16 477.61 284.88 o 9 1 -16 50.00 118.92 254.22 o 10 1 -16 54.93 -80.96 457.42 o 1 2 -16 76.27 86.79 173.34 o 2 2 -16 275.60 269.34 145.30 o 3 2 -16 64.20 233.20 159.56 o 4 2 -16 256.12 329.05 191.93 o 5 2 -16 524.36 570.04 191.65 o 6 2 -16 1306.21 1045.00 226.46 o 7 2 -16 175.25 303.77 202.23 o 8 2 -16 435.46 580.26 274.76 o 9 2 -16 70.35 133.44 264.41 o 2 3 -16 1196.12 1078.95 145.53 o 3 3 -16 344.70 343.21 177.46 o 4 3 -16 118.81 29.29 196.51 o 5 3 -16 89.09 345.55 240.62 o 6 3 -16 197.58 225.02 201.70 o 7 3 -16 4.00 -45.89 249.71 o 8 3 -16 366.23 -39.70 277.29 o 9 3 -16 470.77 254.37 220.53 o 2 4 -16 98.33 102.96 169.13 o 3 4 -16 1.52 -183.43 183.43 o 4 4 -16 111.08 235.35 199.03 o 5 4 -16 0.60 -41.69 172.88 o 6 4 -16 75.84 -31.96 204.36 o 7 4 -16 0.09 -186.76 253.17 o 8 4 -16 147.17 102.88 185.27 o 3 5 -16 861.96 688.94 159.93 o 4 5 -16 1030.26 728.33 148.19 o 5 5 -16 627.90 464.16 221.99 o 6 5 -16 1059.09 849.00 255.39 o 7 5 -16 336.68 235.67 257.91 o 8 5 -16 954.75 930.81 310.98 o 4 6 -16 337.23 45.91 247.44 o 5 6 -16 450.25 413.43 225.12 o 6 6 -16 1022.12 930.07 184.16 o 0 1 -15 28.97 33.86 156.77 o 1 1 -15 429.01 375.40 156.30 o 2 1 -15 60.00 -27.30 114.97 o 3 1 -15 107.03 158.61 115.48 o 4 1 -15 98.70 -4.92 194.06 o 5 1 -15 10.06 -59.60 157.26 o 6 1 -15 168.42 1.69 159.16 o 7 1 -15 1461.16 1520.52 203.93 o 8 1 -15 16.99 -194.57 205.24 o 9 1 -15 680.43 445.75 306.64 o 10 1 -15 47.37 -8.90 218.57 o 0 2 -15 22.72 -29.71 132.90 o 1 2 -15 126.82 129.59 155.07 o 2 2 -15 162.79 168.53 117.28 o 3 2 -15 14.50 -115.35 115.35 o 4 2 -15 244.76 150.99 120.76 o 5 2 -15 106.79 168.34 157.63 o 6 2 -15 201.25 113.68 161.00 o 7 2 -15 335.07 78.04 203.59 o 8 2 -15 60.77 72.09 169.21 o 9 2 -15 129.39 218.43 255.44 o 10 2 -15 23.42 -181.44 222.49 o 0 3 -15 41.16 150.09 131.47 o 1 3 -15 148.84 190.01 139.91 o 2 3 -15 16.02 75.98 136.81 o 3 3 -15 92.20 98.24 115.68 o 4 3 -15 150.98 89.96 123.37 o 5 3 -15 87.25 52.64 159.86 o 6 3 -15 73.98 -14.05 164.37 o 7 3 -15 69.34 137.40 166.42 o 8 3 -15 89.04 71.76 178.88 o 9 3 -15 4.79 10.84 260.83 o 10 3 -15 18.55 36.36 228.54 o 1 4 -15 149.47 176.68 154.48 o 2 4 -15 127.38 178.67 140.28 o 3 4 -15 58.67 -14.69 136.75 o 4 4 -15 5.29 18.85 125.96 o 5 4 -15 43.05 52.56 161.54 o 6 4 -15 15.89 -60.94 204.60 o 7 4 -15 118.10 29.09 197.60 o 8 4 -15 8.44 67.06 255.39 o 9 4 -15 49.55 -16.97 218.59 o 1 5 -15 298.84 204.97 183.11 o 2 5 -15 289.36 318.25 147.17 o 3 5 -15 138.51 177.56 158.58 o 4 5 -15 206.47 105.97 173.20 o 5 5 -15 87.26 181.88 170.98 o 6 5 -15 113.79 13.38 199.56 o 7 5 -15 143.39 64.92 255.02 o 8 5 -15 278.06 180.57 210.16 o 9 5 -15 227.62 199.74 209.99 o 2 6 -15 168.46 97.72 179.87 o 3 6 -15 26.84 161.91 159.57 o 4 6 -15 140.94 175.20 198.42 o 5 6 -15 152.10 47.81 173.57 o 6 6 -15 63.82 18.07 246.01 o 7 6 -15 507.58 367.53 253.34 o 8 6 -15 190.89 -91.21 260.77 o 3 7 -15 17.36 76.02 169.99 o 4 7 -15 304.06 330.83 153.89 o 5 7 -15 147.64 71.70 199.41 o 6 7 -15 339.07 397.14 172.06 o 7 7 -15 117.69 185.72 292.88 o -1 0 -14 730.21 794.42 240.44 o 0 0 -14 416.08 306.92 140.61 o 1 0 -14 1984.15 1895.83 249.96 o 2 0 -14 371.62 376.16 161.90 o 3 0 -14 3595.17 3882.05 181.15 o 4 0 -14 660.23 541.42 220.62 o 5 0 -14 2957.53 2923.67 241.87 o 6 0 -14 250.55 248.95 245.92 o 7 0 -14 2322.80 2142.40 210.50 o 8 0 -14 53.13 181.15 285.38 o 9 0 -14 1247.67 675.00 225.68 o 10 0 -14 609.56 687.15 376.46 o 11 0 -14 1060.02 1242.74 400.75 o -1 1 -14 158.10 172.88 137.03 o 0 1 -14 105.88 -16.49 126.62 o 1 1 -14 147.35 101.29 112.66 o 2 1 -14 63.43 -17.24 104.33 o 3 1 -14 393.43 373.32 157.48 o 4 1 -14 179.54 110.23 156.64 o 5 1 -14 433.02 312.42 113.67 o 6 1 -14 119.78 76.90 193.54 o 7 1 -14 300.32 205.18 163.99 o 8 1 -14 89.62 126.69 165.70 o 9 1 -14 325.35 163.24 173.15 o 10 1 -14 180.19 133.82 278.30 o 11 1 -14 358.67 288.24 259.66 o -1 2 -14 270.07 178.62 126.67 o 0 2 -14 219.78 157.19 124.56 o 1 2 -14 562.47 513.13 122.84 o 2 2 -14 230.00 250.41 120.22 o 3 2 -14 871.62 868.59 121.80 o 4 2 -14 472.25 331.73 137.44 o 5 2 -14 957.08 926.46 197.78 o 6 2 -14 179.95 151.61 140.95 o 7 2 -14 1170.70 1087.66 169.02 o 8 2 -14 85.43 23.06 170.03 o 9 2 -14 803.84 874.41 213.90 o 10 2 -14 197.79 387.50 259.73 o 11 2 -14 652.56 1137.49 466.53 o -1 3 -14 388.06 440.22 150.51 o 0 3 -14 319.60 380.90 124.54 o 1 3 -14 921.09 793.14 113.26 o 2 3 -14 414.11 439.86 114.76 o 3 3 -14 1468.26 1355.75 140.39 o 4 3 -14 886.13 812.10 197.03 o 5 3 -14 1164.41 1004.04 163.80 o 6 3 -14 790.51 814.40 165.68 o 7 3 -14 1383.38 1219.19 149.92 o 8 3 -14 383.46 194.68 149.88 o 9 3 -14 1002.36 947.43 187.08 o 10 3 -14 624.74 834.64 268.70 o -1 4 -14 91.76 189.21 168.12 o 0 4 -14 90.24 74.55 149.33 o 1 4 -14 50.46 74.72 116.36 o 2 4 -14 124.77 163.50 105.11 o 3 4 -14 36.87 23.13 123.06 o 4 4 -14 168.14 169.23 124.22 o 5 4 -14 44.79 -61.61 197.84 o 6 4 -14 105.90 89.26 164.01 o 7 4 -14 93.14 35.13 144.19 o 8 4 -14 66.98 144.57 208.95 o 9 4 -14 55.47 102.71 257.91 o 10 4 -14 45.12 54.80 220.11 o 0 5 -14 267.36 194.08 153.61 o 1 5 -14 1013.52 952.01 131.38 o 2 5 -14 376.61 364.16 117.57 o 3 5 -14 1151.82 1073.17 164.89 o 4 5 -14 984.40 1032.94 163.19 o 5 5 -14 866.63 786.24 164.75 o 6 5 -14 737.51 543.09 204.94 o 7 5 -14 836.60 786.10 172.88 o 8 5 -14 379.84 103.74 206.31 o 9 5 -14 663.47 536.15 262.44 o 0 6 -14 202.74 6.07 203.49 o 1 6 -14 661.30 428.12 156.10 o 2 6 -14 188.55 297.32 153.32 o 3 6 -14 1089.11 1067.55 164.29 o 4 6 -14 353.90 233.62 162.39 o 5 6 -14 893.24 837.47 127.96 o 6 6 -14 403.68 311.62 167.71 o 7 6 -14 744.45 805.96 247.40 o 8 6 -14 264.29 239.88 180.84 o 9 6 -14 533.36 635.31 217.48 o 1 7 -14 306.04 268.91 176.73 o 2 7 -14 56.34 152.88 155.39 o 3 7 -14 554.45 395.23 150.21 o 4 7 -14 288.82 316.35 166.51 o 5 7 -14 508.98 476.67 152.28 o 6 7 -14 66.96 4.01 168.61 o 7 7 -14 125.36 159.99 198.81 o 8 7 -14 78.00 75.69 254.07 o 3 8 -14 1368.66 1470.51 197.29 o 4 8 -14 284.45 182.52 193.53 o 5 8 -14 1240.70 1184.49 197.93 o 6 8 -14 196.29 169.91 195.92 o 7 8 -14 965.27 1084.86 288.33 o -2 1 -13 1063.56 1087.46 136.82 o -1 1 -13 1315.24 1480.11 123.78 o 0 1 -13 1161.86 1181.87 122.09 o 1 1 -13 3131.08 3275.19 104.90 o 2 1 -13 2568.95 2498.53 125.62 o 3 1 -13 4906.90 4684.47 522.19 o 4 1 -13 2200.48 1890.28 171.53 o 5 1 -13 5870.06 5582.32 155.85 o 6 1 -13 979.35 858.48 120.21 o 7 1 -13 3690.49 3302.35 260.08 o 8 1 -13 1574.04 1423.48 173.33 o 9 1 -13 2212.13 1984.17 223.70 o 10 1 -13 1710.54 1608.06 217.61 o 11 1 -13 1616.60 1518.62 280.44 o -2 2 -13 511.88 535.02 146.74 o -1 2 -13 756.71 779.59 120.35 o 0 2 -13 552.32 430.92 110.24 o 1 2 -13 1349.81 1466.17 136.30 o 2 2 -13 1550.63 1707.10 116.13 o 3 2 -13 2489.11 2523.55 134.10 o 4 2 -13 1614.75 1442.40 121.59 o 5 2 -13 3017.61 2792.65 130.81 o 6 2 -13 738.07 759.69 167.06 o 7 2 -13 1898.39 1832.51 147.22 o 8 2 -13 404.08 389.83 147.04 o 9 2 -13 1380.68 1179.35 217.31 o 10 2 -13 331.59 102.20 215.28 o 11 2 -13 1021.45 982.48 238.33 o -2 3 -13 242.16 107.17 116.11 o -1 3 -13 288.90 250.56 141.47 o 0 3 -13 165.29 198.63 98.30 o 1 3 -13 302.33 260.82 121.15 o 2 3 -13 183.61 123.61 107.85 o 3 3 -13 414.45 434.11 111.94 o 4 3 -13 280.06 271.29 113.93 o 5 3 -13 770.67 587.48 119.48 o 6 3 -13 242.51 188.33 166.36 o 7 3 -13 625.85 560.23 168.47 o 8 3 -13 246.51 158.52 207.16 o 9 3 -13 93.04 32.65 211.80 o 10 3 -13 86.22 70.19 259.65 o 11 3 -13 81.53 123.92 189.87 o -2 4 -13 1093.95 1137.54 149.99 o -1 4 -13 2146.02 2274.24 150.35 o 0 4 -13 1640.27 1669.23 139.86 o 1 4 -13 2840.11 3010.04 120.49 o 2 4 -13 2863.54 2885.49 128.17 o 3 4 -13 2554.78 2776.80 239.69 o 4 4 -13 2677.95 2584.75 146.19 o 5 4 -13 3667.86 3524.51 153.97 o 6 4 -13 1481.99 1488.20 173.62 o 7 4 -13 3946.69 3535.10 201.89 o 8 4 -13 1285.86 1390.66 212.87 o 9 4 -13 3109.77 2866.98 167.80 o 10 4 -13 663.14 408.47 219.76 o -1 5 -13 631.12 553.81 136.07 o 0 5 -13 462.13 317.18 142.89 o 1 5 -13 512.01 611.84 137.84 o 2 5 -13 683.88 567.61 130.07 o 3 5 -13 506.23 409.86 137.27 o 4 5 -13 617.69 548.36 140.48 o 5 5 -13 721.61 611.86 198.12 o 6 5 -13 821.21 890.22 165.44 o 7 5 -13 809.56 755.74 206.43 o 8 5 -13 421.17 469.22 373.93 o 9 5 -13 645.41 660.77 183.09 o 10 5 -13 91.29 -13.22 218.61 o -1 6 -13 717.15 706.89 133.81 o 0 6 -13 211.63 183.33 145.71 o 1 6 -13 1368.73 1314.73 140.85 o 2 6 -13 996.89 863.45 142.58 o 3 6 -13 1384.66 1444.98 139.49 o 4 6 -13 1563.77 1465.33 162.97 o 5 6 -13 1378.79 1320.35 200.65 o 6 6 -13 610.70 674.39 162.43 o 7 6 -13 1171.37 892.72 210.15 o 8 6 -13 581.88 232.59 283.87 o 9 6 -13 819.12 698.46 210.92 o 0 7 -13 572.43 483.49 144.63 o 1 7 -13 2123.00 2185.28 130.95 o 2 7 -13 1163.44 1083.95 168.12 o 3 7 -13 2255.31 2344.76 165.48 o 4 7 -13 1626.73 1574.61 142.55 o 5 7 -13 2175.98 2192.45 148.02 o 6 7 -13 1189.56 938.08 203.81 o 7 7 -13 1583.66 1306.03 179.66 o 8 7 -13 940.23 765.61 180.13 o 9 7 -13 1152.49 1229.25 215.65 o 1 8 -13 28.41 -14.20 144.88 o 2 8 -13 22.15 41.25 163.35 o 3 8 -13 18.32 95.26 159.23 o 4 8 -13 113.94 70.89 161.09 o 5 8 -13 31.45 -54.93 186.44 o 6 8 -13 27.08 52.16 161.56 o 7 8 -13 2.98 209.35 238.99 o 8 8 -13 15.73 57.90 222.13 o 2 9 -13 689.83 624.22 219.05 o 3 9 -13 1852.10 1915.96 150.41 o 4 9 -13 877.24 788.75 162.27 o 5 9 -13 1293.29 1360.02 189.64 o 6 9 -13 434.33 372.48 161.70 o -3 0 -12 2584.35 2878.44 195.89 o -2 0 -12 2689.59 3226.95 206.95 o -1 0 -12 7599.78 8406.12 616.81 o 0 0 -12 2752.59 3194.10 175.08 o 1 0 -12 15595.19 17460.55 372.42 o 2 0 -12 4439.76 4809.54 192.28 o 3 0 -12 7037.81 6420.13 206.45 o 4 0 -12 2575.99 3084.58 236.81 o 5 0 -12 8558.13 9399.46 286.40 o 6 0 -12 2117.24 2066.50 177.10 o 7 0 -12 9568.86 9669.66 298.54 o 8 0 -12 5674.53 5035.71 222.64 o 9 0 -12 3990.49 3791.97 331.94 o 10 0 -12 2497.06 2506.72 319.79 o 11 0 -12 2090.27 2211.22 389.62 o -3 1 -12 775.25 512.68 122.77 o -2 1 -12 1439.97 1136.68 132.56 o -1 1 -12 1851.56 1804.42 113.50 o 0 1 -12 152.87 170.51 106.32 o 1 1 -12 73.65 93.80 88.88 o 2 1 -12 274.02 284.36 99.41 o 3 1 -12 50.32 75.76 126.48 o 4 1 -12 540.18 529.06 132.63 o 5 1 -12 2017.65 1908.39 291.46 o 6 1 -12 2207.58 2063.52 173.56 o 7 1 -12 1202.79 866.06 171.96 o 8 1 -12 378.10 221.10 168.47 o 9 1 -12 133.90 213.06 207.09 o 10 1 -12 126.25 -50.42 174.62 o 11 1 -12 2.22 -72.36 267.63 o -3 2 -12 1213.00 1076.98 133.08 o -2 2 -12 1285.03 1173.38 102.07 o -1 2 -12 2284.83 2442.86 123.82 o 0 2 -12 209.53 177.51 80.65 o 1 2 -12 1823.18 1973.28 103.18 o 2 2 -12 122.50 119.51 97.58 o 3 2 -12 896.80 833.16 135.44 o 4 2 -12 1460.35 1602.78 138.66 o 5 2 -12 3589.79 3827.98 182.41 o 6 2 -12 889.36 874.11 144.05 o 7 2 -12 2217.40 2049.16 147.90 o 8 2 -12 372.49 330.92 120.56 o 9 2 -12 168.87 195.03 269.19 o 10 2 -12 36.91 114.14 210.87 o 11 2 -12 548.75 658.39 216.23 o -3 3 -12 450.59 473.30 113.79 o -2 3 -12 508.19 559.94 124.71 o -1 3 -12 1356.44 1390.53 108.63 o 0 3 -12 519.13 535.14 116.28 o 1 3 -12 2859.24 2894.58 148.70 o 2 3 -12 1370.10 1430.07 133.11 o 3 3 -12 676.90 771.91 114.52 o 4 3 -12 1080.08 963.72 167.75 o 5 3 -12 1425.90 1345.83 125.13 o 6 3 -12 115.99 170.36 117.70 o 7 3 -12 1729.93 1458.06 253.51 o 8 3 -12 741.15 556.03 173.82 o 9 3 -12 1018.03 1280.67 211.68 o 10 3 -12 136.48 359.95 232.17 o 11 3 -12 852.37 956.14 262.72 o -3 4 -12 33.87 98.22 133.56 o -2 4 -12 16.97 -139.79 139.79 o -1 4 -12 19.50 4.16 114.87 o 0 4 -12 63.11 17.39 130.60 o 1 4 -12 27.81 52.62 89.94 o 2 4 -12 104.48 130.12 98.13 o 3 4 -12 13.09 51.51 129.02 o 4 4 -12 318.66 350.92 162.36 o 5 4 -12 7.73 -36.61 163.11 o 6 4 -12 285.52 287.83 165.26 o 7 4 -12 53.81 59.75 140.04 o 8 4 -12 212.85 118.98 169.36 o 9 4 -12 24.65 39.25 148.12 o 10 4 -12 100.40 -35.41 255.11 o 11 4 -12 9.07 -19.93 275.03 o -2 5 -12 1304.59 1350.20 142.96 o -1 5 -12 2698.67 2732.36 138.67 o 0 5 -12 1696.37 1588.42 122.41 o 1 5 -12 4293.94 4620.07 284.54 o 2 5 -12 3811.67 3562.13 119.32 o 3 5 -12 1594.61 1657.40 135.64 o 4 5 -12 3986.37 3850.77 153.68 o 5 5 -12 2108.67 2168.75 173.34 o 6 5 -12 1950.00 1922.07 126.23 o 7 5 -12 3035.69 2797.46 178.94 o 8 5 -12 1822.43 1686.81 213.19 o 9 5 -12 1991.05 1708.29 217.58 o 10 5 -12 753.91 595.38 215.50 o -2 6 -12 855.48 818.37 131.73 o -1 6 -12 1660.88 1451.22 143.96 o 0 6 -12 407.79 368.80 117.06 o 1 6 -12 1059.07 1047.64 113.00 o 2 6 -12 430.53 388.03 135.39 o 3 6 -12 615.64 596.05 155.53 o 4 6 -12 1389.24 1129.17 141.20 o 5 6 -12 2356.84 2352.90 172.80 o 6 6 -12 994.78 843.47 201.49 o 7 6 -12 1543.06 1411.12 146.99 o 8 6 -12 425.27 258.51 205.85 o 9 6 -12 368.58 107.64 251.64 o 10 6 -12 36.01 -207.72 207.72 o -1 7 -12 933.07 788.47 141.38 o 0 7 -12 223.61 324.90 137.80 o 1 7 -12 61.36 -11.35 117.06 o 2 7 -12 459.82 411.05 111.02 o 3 7 -12 46.39 -29.26 131.63 o 4 7 -12 675.54 658.66 121.03 o 5 7 -12 654.47 634.21 137.93 o 6 7 -12 927.39 787.19 163.58 o 7 7 -12 907.58 678.58 170.82 o 8 7 -12 95.98 92.61 200.26 o 9 7 -12 90.21 -96.20 177.03 o 0 8 -12 178.19 189.22 157.18 o 1 8 -12 1894.05 1918.39 142.21 o 2 8 -12 185.93 56.98 126.97 o 3 8 -12 349.72 370.20 129.65 o 4 8 -12 87.52 54.15 150.39 o 5 8 -12 336.78 240.67 134.49 o 6 8 -12 79.09 65.33 200.85 o 7 8 -12 743.73 617.60 239.41 o 8 8 -12 585.99 570.36 242.49 o 1 9 -12 97.55 80.69 134.68 o 2 9 -12 23.38 -10.54 162.04 o 3 9 -12 110.21 102.77 175.67 o 4 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