# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' A in Pc' _shelx_refln_list_code 4 _shelx_F_calc_maximum 306.24 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 7.6873 _cell_length_b 19.1020 _cell_length_c 13.8413 _cell_angle_alpha 90.000 _cell_angle_beta 118.452 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 1 -17 95.07 -12.32 121.29 o 3 1 -17 406.18 694.36 171.09 o 4 1 -17 475.86 638.67 181.04 o 5 1 -17 101.84 183.18 194.40 o 6 1 -17 17.09 28.21 111.69 o 2 2 -17 319.83 439.48 152.59 o 3 2 -17 93.33 90.15 135.59 o 4 2 -17 5.46 188.14 159.35 o 5 2 -17 498.77 658.74 238.87 o 6 2 -17 118.70 76.79 255.33 o 2 3 -17 4.39 -242.41 182.88 o 3 3 -17 1.07 -60.45 119.84 o 4 3 -17 18.78 99.73 119.96 o 5 3 -17 270.51 636.28 156.51 o 6 3 -17 168.89 477.20 153.25 o 3 4 -17 52.11 -15.23 115.55 o 4 4 -17 21.32 -0.24 126.91 o 5 4 -17 0.52 57.41 102.10 o 6 4 -17 238.14 393.59 198.54 o 3 5 -17 20.34 128.34 206.51 o 4 5 -17 56.44 308.56 139.74 o 5 5 -17 135.65 266.34 135.02 o 6 5 -17 31.71 -130.68 116.59 o 4 6 -17 175.10 449.94 149.56 o 5 6 -17 27.53 39.91 143.11 o 6 6 -17 167.58 285.19 184.78 o 4 7 -17 16.87 237.13 162.74 o 5 7 -17 63.26 46.17 162.94 o 1 0 -16 943.03 1303.01 316.90 o 2 0 -16 328.18 525.31 231.74 o 3 0 -16 144.07 0.20 181.29 o 4 0 -16 217.50 196.04 180.59 o 5 0 -16 872.80 1245.17 301.74 o 6 0 -16 385.68 560.91 222.57 o 7 0 -16 205.51 251.39 239.82 o 1 1 -16 133.23 333.47 209.26 o 2 1 -16 354.56 586.20 175.40 o 3 1 -16 644.65 507.99 163.87 o 4 1 -16 625.34 584.11 162.37 o 5 1 -16 35.62 181.15 125.76 o 6 1 -16 158.72 222.97 127.59 o 7 1 -16 66.08 81.49 288.78 o 1 2 -16 15.94 -61.03 221.57 o 2 2 -16 384.90 553.42 214.14 o 3 2 -16 274.09 253.97 136.01 o 4 2 -16 151.56 362.76 138.63 o 5 2 -16 889.51 1164.03 203.53 o 6 2 -16 346.35 462.84 158.65 o 7 2 -16 9.00 -112.92 130.28 o 1 3 -16 323.06 272.13 236.73 o 2 3 -16 84.50 241.95 201.93 o 3 3 -16 97.79 68.87 189.36 o 4 3 -16 555.33 629.28 163.65 o 5 3 -16 206.87 305.76 146.43 o 6 3 -16 82.69 265.86 148.13 o 7 3 -16 114.21 312.65 149.47 o 1 4 -16 29.07 273.82 238.72 o 2 4 -16 671.56 1107.76 296.56 o 3 4 -16 412.64 419.60 149.34 o 4 4 -16 50.66 -25.21 118.03 o 5 4 -16 6.76 262.11 128.05 o 6 4 -16 241.71 281.14 267.09 o 7 4 -16 537.30 655.66 171.40 o 1 5 -16 373.93 1010.93 325.38 o 2 5 -16 111.96 505.67 256.97 o 3 5 -16 182.68 399.28 145.95 o 4 5 -16 56.44 356.51 246.80 o 5 5 -16 321.74 735.58 179.58 o 6 5 -16 371.33 257.65 147.23 o 7 5 -16 48.05 -7.80 124.07 o 1 6 -16 82.18 117.07 192.16 o 2 6 -16 131.97 419.51 251.29 o 3 6 -16 58.82 273.20 133.94 o 4 6 -16 173.27 215.45 135.40 o 5 6 -16 64.36 207.65 148.48 o 6 6 -16 246.39 233.06 140.88 o 7 6 -16 471.94 429.45 172.98 o 2 7 -16 195.87 149.68 239.52 o 3 7 -16 209.95 176.70 214.49 o 4 7 -16 259.66 441.90 163.25 o 5 7 -16 109.46 312.83 152.50 o 6 7 -16 270.15 -54.74 177.85 o 7 7 -16 36.23 151.65 153.04 o 2 8 -16 305.39 656.24 285.89 o 3 8 -16 4.05 522.92 237.83 o 4 8 -16 83.40 162.99 154.05 o 5 8 -16 151.15 388.43 168.13 o 6 8 -16 176.16 9.41 131.53 o 7 8 -16 297.43 93.34 286.09 o 3 9 -16 228.14 855.48 284.00 o 4 9 -16 315.74 -346.52 287.19 o 5 9 -16 181.16 138.34 152.99 o 6 9 -16 34.40 72.53 143.70 o 4 10 -16 73.83 463.29 392.99 o 5 10 -16 393.79 371.50 169.65 o 6 10 -16 7.07 28.87 151.17 o 5 11 -16 25.91 173.51 176.50 o 0 1 -15 327.14 651.35 269.84 o 1 1 -15 235.72 509.65 187.17 o 2 1 -15 230.81 416.26 158.42 o 3 1 -15 462.01 413.15 144.84 o 4 1 -15 291.80 411.69 145.02 o 5 1 -15 26.12 -67.69 115.99 o 6 1 -15 47.07 112.59 127.68 o 7 1 -15 55.00 -36.70 163.79 o 8 1 -15 12.63 -184.41 152.73 o 0 2 -15 48.10 264.45 269.93 o 1 2 -15 630.15 634.41 180.52 o 2 2 -15 301.18 668.46 189.96 o 3 2 -15 207.40 325.19 136.32 o 4 2 -15 204.96 345.38 155.71 o 5 2 -15 329.01 456.51 151.50 o 6 2 -15 337.28 478.01 152.65 o 7 2 -15 111.27 117.39 195.25 o 8 2 -15 5.31 -123.31 151.38 o 0 3 -15 106.49 353.70 269.84 o 1 3 -15 137.45 198.24 247.20 o 2 3 -15 127.38 11.66 118.01 o 3 3 -15 323.27 361.83 148.25 o 4 3 -15 998.42 934.86 188.79 o 5 3 -15 173.38 224.37 127.82 o 6 3 -15 39.00 138.54 129.41 o 7 3 -15 349.72 360.42 139.51 o 8 3 -15 366.27 427.09 315.76 o 0 4 -15 50.06 -14.36 223.67 o 1 4 -15 429.92 316.20 221.77 o 2 4 -15 258.32 239.46 144.37 o 3 4 -15 253.66 393.96 145.60 o 4 4 -15 341.41 129.93 267.14 o 5 4 -15 257.17 217.15 131.36 o 6 4 -15 322.90 314.93 145.98 o 7 4 -15 23.48 121.30 133.71 o 8 4 -15 109.97 178.67 175.21 o 0 5 -15 215.26 538.47 266.35 o 1 5 -15 8.31 162.34 238.72 o 2 5 -15 22.43 259.42 130.33 o 3 5 -15 64.24 363.24 142.73 o 4 5 -15 48.21 166.39 124.76 o 5 5 -15 86.96 -86.25 108.89 o 6 5 -15 26.81 -23.65 110.39 o 7 5 -15 75.82 162.73 132.71 o 8 5 -15 24.69 103.85 137.41 o 0 6 -15 5.99 -278.51 185.67 o 1 6 -15 227.89 640.98 267.34 o 2 6 -15 797.30 887.29 334.25 o 3 6 -15 632.34 624.30 172.25 o 4 6 -15 60.41 19.37 119.47 o 5 6 -15 387.21 324.17 266.20 o 6 6 -15 813.85 936.92 189.98 o 7 6 -15 394.72 720.63 297.66 o 8 6 -15 7.66 -144.79 231.44 o 0 7 -15 123.32 431.38 256.87 o 1 7 -15 354.68 805.22 271.63 o 2 7 -15 73.62 99.12 222.87 o 3 7 -15 718.44 1301.49 212.61 o 4 7 -15 1499.37 1257.45 260.86 o 5 7 -15 212.24 392.65 200.23 o 6 7 -15 42.23 323.96 152.34 o 7 7 -15 37.90 117.07 133.94 o 8 7 -15 470.78 1018.41 323.98 o 1 8 -15 212.53 -156.86 197.24 o 2 8 -15 319.38 302.84 250.29 o 3 8 -15 70.78 180.49 220.67 o 4 8 -15 281.39 481.39 161.57 o 5 8 -15 236.12 336.61 159.90 o 6 8 -15 165.76 300.74 144.94 o 7 8 -15 73.92 135.84 130.96 o 1 9 -15 143.06 172.21 229.85 o 2 9 -15 87.58 108.19 217.28 o 3 9 -15 178.20 229.65 308.72 o 4 9 -15 155.82 200.33 157.13 o 5 9 -15 347.61 295.54 153.89 o 6 9 -15 223.01 308.93 153.95 o 7 9 -15 91.81 -77.29 128.90 o 2 10 -15 66.51 786.17 262.16 o 3 10 -15 45.93 -140.40 282.20 o 4 10 -15 183.24 451.22 302.94 o 5 10 -15 83.76 266.79 157.08 o 6 10 -15 15.06 18.55 144.59 o 7 10 -15 1.53 4.45 134.07 o 2 11 -15 465.15 194.45 360.38 o 3 11 -15 220.97 906.63 395.58 o 4 11 -15 128.69 7.28 321.79 o 5 11 -15 74.45 113.92 242.96 o 6 11 -15 2.07 -76.52 130.26 o 3 12 -15 20.35 139.80 357.29 o 4 12 -15 14.82 -249.99 308.63 o 5 12 -15 65.28 162.68 163.45 o 6 12 -15 105.31 121.60 199.14 o 4 13 -15 36.77 18.85 346.62 o 5 13 -15 101.79 285.69 357.09 o 0 0 -14 237.23 587.34 258.47 o 1 0 -14 129.63 207.71 198.14 o 2 0 -14 100.06 172.81 181.19 o 3 0 -14 195.89 3.29 167.13 o 4 0 -14 430.67 708.89 213.59 o 5 0 -14 13.48 -139.01 137.31 o 6 0 -14 157.79 170.72 185.37 o 7 0 -14 117.20 -249.94 166.63 o 8 0 -14 401.56 394.98 232.94 o 9 0 -14 303.05 298.45 274.32 o 0 1 -14 101.97 250.89 227.95 o 1 1 -14 130.71 397.39 148.10 o 2 1 -14 792.32 1029.37 186.88 o 3 1 -14 131.47 167.15 120.52 o 4 1 -14 438.04 223.70 116.58 o 5 1 -14 24.82 142.95 117.24 o 6 1 -14 138.26 195.55 120.82 o 7 1 -14 163.37 13.02 126.99 o 8 1 -14 184.86 324.86 269.59 o 9 1 -14 98.69 84.21 182.62 o -1 2 -14 282.77 672.69 268.84 o 0 2 -14 272.82 -27.22 208.71 o 1 2 -14 71.29 168.31 143.75 o 2 2 -14 319.36 272.58 140.17 o 3 2 -14 821.90 900.78 180.49 o 4 2 -14 844.49 1006.52 180.07 o 5 2 -14 90.48 332.28 141.75 o 6 2 -14 467.71 564.12 232.14 o 7 2 -14 43.66 -60.43 156.01 o 8 2 -14 63.78 137.18 144.57 o 9 2 -14 25.29 -73.30 175.29 o -1 3 -14 444.90 904.24 307.73 o 0 3 -14 116.27 -147.18 214.69 o 1 3 -14 143.11 286.09 141.17 o 2 3 -14 1113.82 1241.17 226.41 o 3 3 -14 443.62 587.66 157.20 o 4 3 -14 1390.69 1545.92 324.88 o 5 3 -14 1666.80 1860.25 243.76 o 6 3 -14 133.43 206.52 127.65 o 7 3 -14 157.21 200.72 141.11 o 8 3 -14 68.63 241.92 156.47 o 9 3 -14 127.45 -2.19 258.07 o -1 4 -14 270.45 645.07 312.61 o 0 4 -14 686.03 670.60 297.86 o 1 4 -14 2425.38 2607.21 474.55 o 2 4 -14 1120.26 1043.83 188.87 o 3 4 -14 987.85 1406.46 265.55 o 4 4 -14 188.80 309.73 157.40 o 5 4 -14 1550.64 1686.79 228.89 o 6 4 -14 870.47 716.20 162.46 o 7 4 -14 19.70 108.30 119.90 o 8 4 -14 206.07 338.33 165.88 o 9 4 -14 252.46 170.02 256.47 o -1 5 -14 623.54 414.82 255.97 o 0 5 -14 1009.60 759.05 309.32 o 1 5 -14 176.55 -34.70 219.78 o 2 5 -14 561.99 459.00 157.13 o 3 5 -14 1211.38 1127.52 191.74 o 4 5 -14 1472.55 1792.04 242.32 o 5 5 -14 201.08 91.94 117.10 o 6 5 -14 1006.24 1072.14 357.39 o 7 5 -14 1871.38 1753.42 244.55 o 8 5 -14 804.13 731.07 197.97 o -1 6 -14 39.43 384.31 250.69 o 0 6 -14 384.41 646.17 299.35 o 1 6 -14 1042.83 1155.62 338.34 o 2 6 -14 292.37 365.57 140.71 o 3 6 -14 357.56 162.14 173.01 o 4 6 -14 105.26 218.40 135.54 o 5 6 -14 1318.07 1423.74 221.90 o 6 6 -14 711.36 1065.49 189.90 o 7 6 -14 29.23 -20.93 123.95 o 8 6 -14 132.44 63.64 120.18 o -1 7 -14 199.55 178.39 222.47 o 0 7 -14 119.33 -87.75 206.61 o 1 7 -14 191.61 -23.13 227.75 o 2 7 -14 214.79 308.72 251.39 o 3 7 -14 73.19 59.69 121.12 o 4 7 -14 182.79 125.09 119.12 o 5 7 -14 831.72 1067.09 187.87 o 6 7 -14 173.08 187.05 139.69 o 7 7 -14 46.90 32.06 154.01 o 8 7 -14 113.17 176.48 129.44 o -1 8 -14 2.40 207.31 256.57 o 0 8 -14 132.93 184.18 210.70 o 1 8 -14 299.72 428.98 266.84 o 2 8 -14 78.06 441.15 243.71 o 3 8 -14 1682.60 1655.66 235.29 o 4 8 -14 283.33 383.64 199.48 o 5 8 -14 305.70 377.82 152.85 o 6 8 -14 42.74 170.82 132.51 o 7 8 -14 34.01 81.40 125.63 o 8 8 -14 53.94 200.11 148.19 o 0 9 -14 56.72 -65.12 186.17 o 1 9 -14 37.94 284.59 249.29 o 2 9 -14 319.75 286.39 252.58 o 3 9 -14 171.47 495.10 315.41 o 4 9 -14 70.33 270.16 144.77 o 5 9 -14 46.76 2.85 135.62 o 6 9 -14 115.42 238.78 378.88 o 7 9 -14 48.89 117.02 135.17 o 8 9 -14 99.67 -67.01 224.26 o 0 10 -14 1.31 -280.60 187.07 o 1 10 -14 32.07 176.90 222.27 o 2 10 -14 38.79 477.85 324.78 o 3 10 -14 145.95 270.23 275.12 o 4 10 -14 185.60 365.84 148.48 o 5 10 -14 28.97 250.92 155.45 o 6 10 -14 4.32 -186.99 124.66 o 7 10 -14 195.84 168.18 134.60 o 1 11 -14 7.81 324.98 237.53 o 2 11 -14 89.09 79.77 275.82 o 3 11 -14 109.82 279.81 293.97 o 4 11 -14 273.01 38.60 218.93 o 5 11 -14 106.47 -60.87 311.67 o 6 11 -14 102.58 54.98 131.56 o 7 11 -14 0.99 243.47 135.69 o 1 12 -14 279.10 5.78 216.69 o 2 12 -14 198.08 22.84 286.79 o 3 12 -14 294.88 1019.81 366.26 o 4 12 -14 299.27 476.25 305.53 o 5 12 -14 72.71 293.86 148.71 o 6 12 -14 34.03 203.06 145.94 o 7 12 -14 18.46 -68.80 129.48 o 2 13 -14 350.47 233.94 357.79 o 3 13 -14 233.50 37.19 324.58 o 4 13 -14 294.50 185.77 292.27 o 5 13 -14 109.14 133.98 155.28 o 6 13 -14 10.43 129.71 147.90 o 2 14 -14 122.92 343.83 391.49 o 3 14 -14 41.01 14.66 364.37 o 4 14 -14 74.60 290.78 314.11 o 5 14 -14 297.79 589.03 338.54 o 6 14 -14 301.42 623.71 189.87 o 3 15 -14 50.80 -136.61 329.77 o 4 15 -14 203.64 78.48 340.24 o 5 15 -14 32.43 470.97 346.62 o -1 1 -13 312.05 752.47 274.52 o 0 1 -13 162.92 253.14 139.82 o 1 1 -13 220.37 88.05 119.18 o 2 1 -13 54.47 -18.26 112.45 o 3 1 -13 559.92 504.58 136.91 o 4 1 -13 593.29 320.43 155.16 o 5 1 -13 501.60 328.55 138.01 o 6 1 -13 176.25 153.70 120.41 o 7 1 -13 98.54 82.14 119.86 o 8 1 -13 411.33 321.60 149.42 o 9 1 -13 13.92 48.03 220.18 o -1 2 -13 530.42 590.13 279.81 o 0 2 -13 290.37 744.08 173.30 o 1 2 -13 495.51 568.41 209.31 o 2 2 -13 1042.18 943.26 178.05 o 3 2 -13 445.39 557.27 147.07 o 4 2 -13 740.53 791.81 159.15 o 5 2 -13 481.74 627.69 150.02 o 6 2 -13 112.34 205.67 116.13 o 7 2 -13 505.10 355.84 145.55 o 8 2 -13 288.33 294.72 212.35 o 9 2 -13 424.53 533.32 191.54 o -2 3 -13 376.07 481.24 217.68 o -1 3 -13 234.15 322.46 145.89 o 0 3 -13 65.69 -13.66 197.34 o 1 3 -13 460.82 334.68 135.21 o 2 3 -13 577.94 715.19 159.64 o 3 3 -13 884.66 901.92 209.95 o 4 3 -13 1030.18 1151.37 178.49 o 5 3 -13 211.44 231.61 120.90 o 6 3 -13 921.00 826.76 168.00 o 7 3 -13 680.22 394.61 143.39 o 8 3 -13 113.74 400.17 150.92 o 9 3 -13 59.50 94.60 159.11 o -2 4 -13 20.48 104.17 139.41 o -1 4 -13 258.66 298.52 195.84 o 0 4 -13 729.62 975.83 321.19 o 1 4 -13 615.76 638.91 161.57 o 2 4 -13 829.88 788.09 164.48 o 3 4 -13 192.89 185.33 113.09 o 4 4 -13 334.84 378.77 172.06 o 5 4 -13 73.70 103.57 114.38 o 6 4 -13 62.06 79.43 110.85 o 7 4 -13 257.53 287.15 136.72 o 8 4 -13 142.94 261.27 150.68 o 9 4 -13 119.67 124.07 163.72 o -2 5 -13 56.49 119.41 152.47 o -1 5 -13 100.00 269.14 242.31 o 0 5 -13 175.78 68.80 223.07 o 1 5 -13 97.82 545.85 263.85 o 2 5 -13 12.85 9.63 228.95 o 3 5 -13 320.71 167.15 110.75 o 4 5 -13 153.30 -18.03 164.13 o 5 5 -13 117.26 40.89 169.02 o 6 5 -13 253.93 391.56 177.50 o 7 5 -13 293.78 742.34 322.19 o 8 5 -13 64.11 180.22 168.57 o 9 5 -13 3.90 -25.97 164.26 o -2 6 -13 150.65 136.88 168.97 o -1 6 -13 161.54 171.31 251.89 o 0 6 -13 1505.71 1480.60 368.66 o 1 6 -13 1731.37 1379.89 360.68 o 2 6 -13 466.55 355.81 135.37 o 3 6 -13 153.31 125.03 110.38 o 4 6 -13 281.69 389.26 255.33 o 5 6 -13 950.98 1016.68 180.63 o 6 6 -13 169.54 265.98 135.07 o 7 6 -13 448.85 613.07 155.49 o 8 6 -13 395.26 354.08 156.72 o -2 7 -13 255.13 492.91 171.81 o -1 7 -13 801.38 937.54 307.93 o 0 7 -13 767.68 722.75 296.66 o 1 7 -13 172.64 689.65 278.21 o 2 7 -13 2446.27 2360.44 265.11 o 3 7 -13 562.88 806.30 166.86 o 4 7 -13 317.65 423.30 139.58 o 5 7 -13 100.94 72.94 121.77 o 6 7 -13 788.55 1295.57 200.66 o 7 7 -13 911.15 1236.87 380.62 o 8 7 -13 199.86 272.98 176.05 o -1 8 -13 122.69 242.51 261.16 o 0 8 -13 1127.25 1092.20 336.05 o 1 8 -13 339.77 571.98 259.66 o 2 8 -13 469.37 885.29 293.77 o 3 8 -13 1061.68 1138.76 467.18 o 4 8 -13 951.93 1144.30 225.01 o 5 8 -13 659.88 667.12 160.23 o 6 8 -13 626.44 485.09 310.87 o 7 8 -13 31.93 123.48 126.59 o 8 8 -13 154.75 -23.41 186.87 o -1 9 -13 114.38 188.07 245.01 o 0 9 -13 163.77 215.19 250.19 o 1 9 -13 113.07 432.27 277.81 o 2 9 -13 47.44 -151.27 207.81 o 3 9 -13 264.40 422.58 144.22 o 4 9 -13 388.58 323.70 144.13 o 5 9 -13 397.23 504.07 154.49 o 6 9 -13 0.47 -89.82 117.83 o 7 9 -13 282.32 260.10 133.40 o 8 9 -13 181.54 356.79 180.39 o -1 10 -13 84.67 217.38 216.29 o 0 10 -13 100.64 106.60 212.30 o 1 10 -13 31.69 462.89 257.57 o 2 10 -13 4.48 -132.03 254.98 o 3 10 -13 44.75 2.09 222.67 o 4 10 -13 71.34 37.07 149.13 o 5 10 -13 42.45 199.09 163.69 o 6 10 -13 217.71 403.93 153.62 o 7 10 -13 174.19 366.69 144.75 o 8 10 -13 25.64 -153.56 159.75 o -1 11 -13 3.44 691.04 289.88 o 0 11 -13 3.50 -139.50 189.66 o 1 11 -13 129.40 157.75 220.57 o 2 11 -13 129.97 429.48 300.45 o 3 11 -13 16.18 64.52 230.65 o 4 11 -13 239.18 323.56 143.26 o 5 11 -13 283.60 550.45 159.51 o 6 11 -13 136.99 241.45 136.83 o 7 11 -13 43.41 31.22 127.53 o 0 12 -13 52.40 44.47 206.81 o 1 12 -13 60.09 296.46 304.14 o 2 12 -13 167.70 586.54 319.79 o 3 12 -13 134.74 402.06 280.80 o 4 12 -13 29.98 -114.55 121.56 o 5 12 -13 98.42 40.43 157.95 o 6 12 -13 62.87 199.76 300.20 o 7 12 -13 64.62 -0.10 156.06 o 0 13 -13 9.89 -39.69 227.75 o 1 13 -13 185.45 91.44 308.72 o 2 13 -13 81.02 -176.00 250.09 o 3 13 -13 702.96 712.98 335.65 o 4 13 -13 831.02 1270.10 371.15 o 5 13 -13 272.23 383.50 166.25 o 6 13 -13 46.21 330.65 163.54 o 7 13 -13 80.37 135.52 173.01 o 1 14 -13 117.48 -243.31 328.57 o 2 14 -13 223.31 540.17 344.52 o 3 14 -13 298.15 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