# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' NdDCE-Bipy' _shelx_refln_list_code 4 _shelx_F_calc_maximum 195.22 _exptl_crystal_F_000 662.00 _reflns_d_resolution_high 0.8038 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.8492 _cell_length_b 12.2399 _cell_length_c 12.3403 _cell_angle_alpha 109.336 _cell_angle_beta 104.427 _cell_angle_gamma 102.457 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5684.93 5295.69 141.67 o 2 0 0 8279.71 7960.81 135.80 o 3 0 0 14595.52 13505.70 123.01 o 4 0 0 1539.29 1507.76 54.47 o 5 0 0 4.51 1.19 67.43 o 6 0 0 1352.71 1335.48 60.45 o 7 0 0 4491.74 4608.74 91.37 o 8 0 0 0.69 -3.29 56.86 o 9 0 0 171.65 174.25 81.52 o -10 1 0 453.67 342.61 78.59 o -9 1 0 1917.80 2117.15 80.85 o -8 1 0 1316.32 1298.14 74.88 o -7 1 0 865.28 936.82 73.70 o -6 1 0 4950.37 4905.05 79.22 o -5 1 0 4606.55 4390.86 68.46 o -4 1 0 594.55 641.90 49.13 o -3 1 0 11944.95 11728.08 119.14 o -2 1 0 6969.51 6508.68 140.11 o -1 1 0 391.16 356.71 78.52 o 1 1 0 8872.64 8116.35 142.97 o 2 1 0 6702.50 6335.22 210.79 o 3 1 0 6092.36 5410.74 81.26 o 4 1 0 5246.65 5104.48 123.81 o 5 1 0 2400.32 2358.09 67.02 o 6 1 0 598.96 602.44 61.33 o 7 1 0 3006.57 3104.65 83.54 o 8 1 0 984.43 990.20 72.73 o 9 1 0 69.65 2.22 78.55 o -10 2 0 13.43 5.66 85.09 o -9 2 0 647.18 627.02 69.95 o -8 2 0 2667.37 2887.88 81.08 o -7 2 0 586.49 572.53 57.61 o -6 2 0 6499.57 6362.57 147.61 o -5 2 0 6205.30 6201.13 92.37 o -4 2 0 930.26 830.55 47.66 o -3 2 0 6581.96 6903.64 101.90 o -2 2 0 114.43 187.41 76.45 o -1 2 0 981.42 1178.42 98.62 o 0 2 0 932.96 964.78 83.46 o 1 2 0 9491.97 9286.66 133.10 o 2 2 0 2288.12 1922.41 84.65 o 3 2 0 216.78 245.10 50.00 o 4 2 0 6313.22 5980.58 141.89 o 5 2 0 1289.51 1180.50 54.17 o 6 2 0 644.09 618.26 69.27 o 7 2 0 2196.70 2145.10 80.51 o 8 2 0 1604.25 1509.79 74.28 o 9 2 0 265.18 328.80 95.44 o -10 3 0 436.89 383.87 87.64 o -9 3 0 95.09 59.35 68.42 o -8 3 0 2948.54 3113.60 66.10 o -7 3 0 3080.16 3127.71 58.83 o -6 3 0 105.01 68.90 51.10 o -5 3 0 7395.51 7218.39 150.04 o -4 3 0 1986.43 1992.52 56.59 o -3 3 0 221.81 271.50 52.50 o -2 3 0 8.94 -1.04 62.98 o -1 3 0 19144.81 19752.32 156.07 o 0 3 0 2633.17 2646.98 90.78 o 1 3 0 9.55 46.73 75.78 o 2 3 0 12970.61 11977.98 111.17 o 3 3 0 12.61 21.70 48.96 o 4 3 0 61.29 61.42 67.83 o 5 3 0 2023.16 2064.29 64.23 o 6 3 0 2442.01 2446.68 78.48 o 7 3 0 19.92 45.98 62.22 o 8 3 0 475.23 438.99 82.97 o 9 3 0 1021.94 849.43 74.72 o -10 4 0 1565.27 1644.83 91.42 o -9 4 0 485.94 562.33 84.18 o -8 4 0 78.90 79.38 63.37 o -7 4 0 4744.98 5210.27 82.86 o -6 4 0 2899.91 2698.48 60.00 o -5 4 0 340.30 364.47 49.24 o -4 4 0 4944.94 4803.23 68.79 o -3 4 0 548.85 787.00 55.99 o -2 4 0 138.10 119.62 50.73 o -1 4 0 1493.78 1541.21 62.12 o 0 4 0 12819.59 12221.27 112.29 o 1 4 0 2272.24 2158.54 61.43 o 2 4 0 281.13 216.30 46.50 o 3 4 0 6585.69 6564.17 170.57 o 4 4 0 1806.06 1857.65 68.67 o 5 4 0 159.55 217.97 58.20 o 6 4 0 1627.25 1671.21 80.75 o 7 4 0 1447.90 1408.84 80.65 o 8 4 0 135.55 56.82 95.86 o -10 5 0 469.71 401.75 69.73 o -9 5 0 677.87 726.00 61.30 o -8 5 0 42.97 -18.37 50.24 o -7 5 0 1585.40 1632.47 70.30 o -6 5 0 2832.83 3045.54 61.90 o -5 5 0 3361.47 3540.73 68.86 o -4 5 0 2425.20 2611.48 60.67 o -3 5 0 6996.73 6620.23 76.49 o -2 5 0 4752.34 4509.61 71.17 o -1 5 0 76.06 69.53 49.78 o 0 5 0 2278.76 2190.66 62.19 o 1 5 0 7590.64 7357.15 83.39 o 2 5 0 1979.49 1993.74 65.88 o 3 5 0 2267.57 2154.60 71.05 o 4 5 0 2478.62 2525.87 75.35 o 5 5 0 1502.42 1575.25 80.56 o 6 5 0 573.21 631.28 65.19 o 7 5 0 1382.49 1305.53 78.70 o 8 5 0 459.22 298.94 93.07 o -10 6 0 1.59 58.60 84.78 o -9 6 0 1165.31 1211.70 77.36 o -8 6 0 585.35 661.65 72.08 o -7 6 0 775.63 797.54 65.69 o -6 6 0 2264.11 2498.70 58.92 o -5 6 0 2446.83 2411.74 57.57 o -4 6 0 1095.93 1116.19 59.92 o -3 6 0 2818.38 2790.45 78.00 o -2 6 0 4859.83 4772.48 68.00 o -1 6 0 100.51 114.99 40.37 o 0 6 0 77.52 85.81 56.84 o 1 6 0 7614.96 7618.88 83.59 o 2 6 0 700.18 643.46 58.42 o 3 6 0 14.31 36.15 53.48 o 4 6 0 5021.26 5020.23 118.77 o 5 6 0 2533.51 2718.15 81.87 o 6 6 0 206.38 115.95 83.07 o 7 6 0 980.73 1026.15 83.75 o -10 7 0 605.88 493.19 79.41 o -9 7 0 16.38 92.03 57.40 o -8 7 0 3270.03 3433.12 70.39 o -7 7 0 2138.64 2222.39 88.51 o -6 7 0 105.66 156.66 57.68 o -5 7 0 3577.21 3502.34 70.21 o -4 7 0 1762.74 1956.32 61.83 o -3 7 0 1877.98 1934.11 62.85 o -2 7 0 1692.45 1733.27 62.72 o -1 7 0 7632.74 8178.72 92.17 o 0 7 0 1224.60 1210.47 60.94 o 1 7 0 1246.78 1310.93 71.79 o 2 7 0 5221.86 5305.21 83.86 o 3 7 0 298.88 319.09 65.89 o 4 7 0 537.20 600.45 66.27 o 5 7 0 2195.09 2245.62 91.68 o 6 7 0 605.84 609.70 60.41 o -10 8 0 1338.20 1019.77 96.30 o -9 8 0 119.44 141.76 80.75 o -8 8 0 754.01 763.22 70.29 o -7 8 0 1730.50 1824.51 64.83 o -6 8 0 2577.30 2825.83 78.14 o -5 8 0 2.65 42.33 45.64 o -4 8 0 2889.50 2963.41 57.81 o -3 8 0 5995.32 6180.07 79.68 o -2 8 0 288.16 287.26 48.48 o -1 8 0 6457.87 6616.43 93.16 o 0 8 0 5328.43 5288.90 74.32 o 1 8 0 1.88 -9.38 53.33 o 2 8 0 1497.67 1486.92 83.08 o 3 8 0 1154.59 1166.98 64.06 o 4 8 0 233.18 204.79 69.58 o 5 8 0 360.36 310.20 83.08 o 6 8 0 527.57 482.35 73.79 o -9 9 0 708.80 747.27 81.16 o -8 9 0 9.14 4.73 67.33 o -7 9 0 2249.03 2244.64 58.02 o -6 9 0 1513.42 1679.94 65.15 o -5 9 0 987.05 999.44 67.07 o -4 9 0 5248.80 5321.85 70.53 o -3 9 0 3500.50 3479.62 68.27 o -2 9 0 1279.26 1224.58 58.11 o -1 9 0 682.09 672.27 49.22 o 0 9 0 3207.57 3412.39 74.80 o 1 9 0 1101.03 1087.67 61.58 o 2 9 0 2.52 -11.15 71.03 o 3 9 0 2927.72 2934.56 80.28 o 4 9 0 1457.16 1439.35 79.31 o 5 9 0 323.90 249.11 87.35 o -9 10 0 1808.14 1793.49 83.33 o -8 10 0 1841.78 1702.37 73.07 o -7 10 0 321.38 223.91 83.35 o -6 10 0 5775.19 5893.61 69.28 o -5 10 0 1698.38 1837.56 69.81 o -4 10 0 99.82 157.05 52.80 o -3 10 0 1761.14 1849.09 68.30 o -2 10 0 2413.65 2567.89 71.47 o -1 10 0 983.35 1064.21 56.79 o 0 10 0 769.87 850.71 62.08 o 1 10 0 3107.81 3274.88 79.47 o 2 10 0 813.89 783.37 85.21 o 3 10 0 117.08 75.51 73.73 o 4 10 0 1743.69 1683.40 101.58 o -8 11 0 1778.30 1653.87 84.14 o -7 11 0 663.88 688.96 69.08 o -6 11 0 367.31 317.14 60.08 o -5 11 0 1374.57 1394.33 77.29 o -4 11 0 718.28 876.04 60.34 o -3 11 0 781.37 835.30 83.78 o -2 11 0 2549.43 2658.63 60.43 o -1 11 0 2368.40 2239.42 63.07 o 0 11 0 182.80 166.88 67.01 o 1 11 0 621.42 635.30 76.76 o 2 11 0 1229.45 1274.87 63.34 o 3 11 0 12.24 -15.33 78.07 o -8 12 0 633.70 428.04 77.37 o -7 12 0 575.83 632.69 80.17 o -6 12 0 456.01 461.20 82.17 o -5 12 0 958.90 905.96 69.79 o -4 12 0 529.88 498.56 68.76 o -3 12 0 352.58 324.69 59.61 o -2 12 0 285.35 224.68 59.72 o -1 12 0 1012.50 1034.03 85.35 o 0 12 0 377.74 327.78 68.48 o 1 12 0 130.82 29.51 86.62 o 2 12 0 1217.47 1042.11 77.99 o -7 13 0 799.11 592.37 76.89 o -6 13 0 685.77 474.33 80.37 o -5 13 0 62.86 -15.43 79.22 o -4 13 0 1000.01 907.23 79.14 o -3 13 0 677.09 738.00 86.87 o -2 13 0 921.67 821.71 65.88 o -1 13 0 352.18 328.42 97.15 o 0 13 0 1124.12 1131.58 82.18 o -5 14 0 1097.97 1126.02 142.57 o -4 14 0 72.65 84.44 75.80 o -3 14 0 885.18 661.37 95.47 o -2 14 0 1400.25 864.84 69.28 o 1 -14 1 5.55 41.14 91.29 o 2 -14 1 1813.92 1764.57 99.82 o 3 -14 1 1009.69 1018.41 81.60 o 4 -14 1 102.11 88.99 94.55 o 5 -14 1 604.51 484.62 79.21 o -1 -13 1 285.58 267.29 109.66 o 0 -13 1 1115.40 1107.45 83.08 o 1 -13 1 486.33 462.69 82.64 o 2 -13 1 70.55 -30.11 67.17 o 3 -13 1 804.41 718.96 75.38 o 4 -13 1 763.65 725.94 60.79 o 5 -13 1 2.56 13.58 58.93 o 6 -13 1 1063.35 1131.85 70.97 o 7 -13 1 1459.14 1191.70 70.49 o -3 -12 1 340.06 286.96 103.92 o -2 -12 1 1331.65 1226.95 84.23 o -1 -12 1 367.56 336.11 74.20 o 0 -12 1 616.07 644.65 84.13 o 1 -12 1 1472.61 1444.38 78.91 o 2 -12 1 1228.26 1283.56 63.71 o 3 -12 1 291.52 289.57 60.24 o 4 -12 1 1433.34 1533.57 72.76 o 5 -12 1 606.21 631.07 69.41 o 6 -12 1 247.37 76.11 67.66 o 7 -12 1 668.71 865.08 87.56 o 8 -12 1 365.94 258.20 67.15 o -4 -11 1 376.28 259.94 75.89 o -3 -11 1 44.63 53.97 79.05 o -2 -11 1 1742.31 1720.21 73.54 o -1 -11 1 1343.36 1458.48 74.11 o 0 -11 1 147.92 130.14 70.69 o 1 -11 1 3470.14 3613.02 82.46 o 2 -11 1 2229.14 2367.09 78.74 o 3 -11 1 1129.93 1145.20 58.16 o 4 -11 1 2345.36 2246.37 66.40 o 5 -11 1 2844.19 3004.95 67.23 o 6 -11 1 159.97 156.01 68.88 o 7 -11 1 579.14 581.82 68.30 o 8 -11 1 1372.51 1399.60 82.40 o 9 -11 1 279.17 122.37 132.36 o -5 -10 1 822.91 600.02 85.36 o -4 -10 1 2506.99 2640.60 92.89 o -3 -10 1 46.37 101.06 73.50 o -2 -10 1 501.05 548.41 60.04 o -1 -10 1 3563.46 3470.67 77.95 o 0 -10 1 690.71 684.81 56.14 o 1 -10 1 968.50 1013.44 67.42 o 2 -10 1 5995.61 6163.93 74.66 o 3 -10 1 1822.76 1880.36 93.45 o 4 -10 1 12.78 63.33 61.77 o 5 -10 1 4534.09 4530.92 74.57 o 6 -10 1 6365.82 6364.81 78.85 o 7 -10 1 112.85 122.53 58.99 o 8 -10 1 786.15 768.04 68.92 o 9 -10 1 1370.94 1358.96 81.89 o -5 -9 1 84.71 15.09 86.62 o -4 -9 1 1548.51 1626.60 74.98 o -3 -9 1 2798.32 2997.33 76.42 o -2 -9 1 7.78 1.01 73.34 o -1 -9 1 3238.58 3312.55 77.05 o 0 -9 1 4155.36 4182.93 63.44 o 1 -9 1 311.74 354.74 55.12 o 2 -9 1 2688.03 2675.07 56.96 o 3 -9 1 421.90 425.55 55.10 o 4 -9 1 458.63 487.35 59.09 o 5 -9 1 46.67 16.48 64.40 o 6 -9 1 1830.40 1909.40 66.42 o 7 -9 1 1024.62 1076.18 73.34 o 8 -9 1 105.03 67.05 67.97 o 9 -9 1 1101.20 1130.70 82.03 o -6 -8 1 738.64 701.52 81.95 o -5 -8 1 863.78 879.02 77.77 o -4 -8 1 557.21 517.33 72.25 o -3 -8 1 1607.91 1761.72 69.56 o -2 -8 1 1052.58 1125.43 70.02 o -1 -8 1 411.34 470.04 55.98 o 0 -8 1 4279.28 4329.18 66.15 o 1 -8 1 312.24 320.67 56.23 o 2 -8 1 1092.90 1115.59 60.36 o 3 -8 1 3396.46 3263.97 60.07 o 4 -8 1 262.91 269.58 67.52 o 5 -8 1 1041.78 1070.32 57.20 o 6 -8 1 1179.20 1377.16 67.37 o 7 -8 1 1987.16 2076.99 66.35 o 8 -8 1 425.83 463.62 60.31 o 9 -8 1 183.00 180.32 72.51 o 10 -8 1 1315.46 1113.89 204.95 o -7 -7 1 76.88 115.42 84.93 o -6 -7 1 994.62 956.20 78.33 o -5 -7 1 2422.68 2447.80 75.21 o -4 -7 1 275.26 312.01 67.18 o -3 -7 1 37.97 54.74 64.28 o -2 -7 1 2788.76 2871.04 90.20 o -1 -7 1 3386.40 3591.65 81.16 o 0 -7 1 15.27 28.34 60.84 o 1 -7 1 6442.19 6588.09 75.14 o 2 -7 1 2569.43 2430.48 76.40 o 3 -7 1 245.36 217.02 68.71 o 4 -7 1 2484.67 2794.85 75.85 o 5 -7 1 2200.04 2199.01 55.02 o 6 -7 1 500.45 446.39 65.01 o 7 -7 1 847.81 929.10 76.68 o 8 -7 1 2638.21 2705.73 66.89 o 9 -7 1 50.04 45.31 57.56 o 10 -7 1 296.02 274.00 94.38 o -7 -6 1 755.08 693.16 83.52 o -6 -6 1 93.67 57.86 75.18 o -5 -6 1 1956.07 1835.51 74.45 o -4 -6 1 3614.09 3699.31 80.42 o -3 -6 1 158.19 158.30 55.46 o -2 -6 1 377.18 401.67 79.63 o -1 -6 1 11178.66 11329.79 108.48 o 0 -6 1 2685.47 2618.89 62.03 o 1 -6 1 6125.61 5909.90 81.07 o 2 -6 1 2525.70 2747.26 61.18 o 3 -6 1 887.86 820.61 73.02 o 4 -6 1 5.32 2.58 55.54 o 5 -6 1 1088.11 1146.06 55.29 o 6 -6 1 6865.80 7103.44 76.97 o 7 -6 1 412.16 374.87 62.80 o 8 -6 1 1276.95 1291.38 58.54 o 9 -6 1 1749.86 1754.83 72.38 o 10 -6 1 10.60 4.20 94.01 o -8 -5 1 370.05 440.20 86.32 o -7 -5 1 1004.63 933.32 78.07 o -6 -5 1 1381.82 1251.05 76.60 o -5 -5 1 1657.37 1450.01 77.61 o -4 -5 1 1165.68 1080.43 65.77 o -3 -5 1 1112.36 1167.74 73.84 o -2 -5 1 3703.39 3988.52 79.31 o -1 -5 1 2731.14 2520.78 73.04 o 0 -5 1 7749.25 7734.85 90.07 o 1 -5 1 5763.15 5718.53 79.98 o 2 -5 1 8954.67 9005.43 98.94 o 3 -5 1 7091.41 7179.40 78.20 o 4 -5 1 8780.70 9152.68 112.26 o 5 -5 1 3514.70 3606.62 70.30 o 6 -5 1 3077.39 2872.29 60.96 o 7 -5 1 3099.87 3230.90 66.27 o 8 -5 1 125.57 112.83 57.76 o 9 -5 1 1955.59 1950.19 64.32 o 10 -5 1 609.76 632.23 80.46 o -8 -4 1 259.57 231.96 81.48 o -7 -4 1 1452.45 1570.74 101.31 o -6 -4 1 3385.42 3242.92 101.81 o -5 -4 1 861.02 826.52 62.75 o -4 -4 1 500.92 436.71 63.04 o -3 -4 1 4038.69 3852.20 88.05 o -2 -4 1 2810.69 2518.57 76.13 o -1 -4 1 2398.65 2245.37 80.12 o 0 -4 1 6902.83 6629.23 101.79 o 1 -4 1 26264.32 26333.90 222.23 o 2 -4 1 663.69 631.30 61.57 o 3 -4 1 15960.46 14749.28 174.20 o 4 -4 1 2983.46 2875.37 57.45 o 5 -4 1 1170.70 1395.54 72.28 o 6 -4 1 3296.19 3273.54 59.80 o 7 -4 1 2883.21 2948.17 86.99 o 8 -4 1 140.85 173.13 54.07 o 9 -4 1 835.50 835.53 84.28 o 10 -4 1 1698.12 1643.78 84.54 o -9 -3 1 1529.27 1498.28 85.19 o -8 -3 1 660.25 681.32 70.27 o -7 -3 1 66.79 44.73 70.61 o -6 -3 1 4393.60 4247.24 145.81 o -5 -3 1 4873.86 4566.89 107.80 o -4 -3 1 470.26 460.18 70.93 o -3 -3 1 1084.21 972.34 60.62 o -2 -3 1 18292.52 16724.62 191.48 o -1 -3 1 6270.67 6062.73 112.86 o 0 -3 1 896.02 810.00 77.29 o 1 -3 1 33957.80 36160.71 283.80 o 2 -3 1 217.97 188.19 67.59 o 3 -3 1 3614.31 3263.79 64.16 o 4 -3 1 4095.59 3732.32 68.85 o 5 -3 1 2520.03 2711.11 66.75 o 6 -3 1 0.67 -2.66 54.13 o 7 -3 1 719.75 767.92 58.34 o 8 -3 1 1953.05 2065.55 65.77 o 9 -3 1 35.52 34.80 81.88 o 10 -3 1 394.09 294.52 85.82 o -9 -2 1 336.70 291.38 97.25 o -8 -2 1 1289.65 1386.28 88.31 o -7 -2 1 2776.07 2787.82 74.00 o -6 -2 1 1562.65 1529.77 71.83 o -5 -2 1 2709.62 2684.31 91.45 o -4 -2 1 9111.53 8512.31 244.24 o -3 -2 1 1677.77 1575.18 72.91 o -2 -2 1 2497.14 2217.48 98.25 o -1 -2 1 6144.50 6077.56 147.46 o 0 -2 1 2950.58 3170.06 108.73 o 1 -2 1 6047.30 6426.93 116.40 o 2 -2 1 4936.06 4778.61 98.89 o 3 -2 1 3860.98 3360.64 82.49 o 4 -2 1 6819.51 6359.57 77.08 o 5 -2 1 2217.81 2382.91 65.47 o 6 -2 1 3689.74 3700.12 68.74 o 7 -2 1 78.11 141.90 69.80 o 8 -2 1 1859.72 1801.49 69.75 o 9 -2 1 798.95 810.37 69.84 o 10 -2 1 0.47 40.78 91.13 o -9 -1 1 26.10 32.46 66.68 o -8 -1 1 784.01 832.38 73.06 o -7 -1 1 3565.40 3668.48 78.58 o -6 -1 1 2172.29 2083.61 65.26 o -5 -1 1 2856.87 2728.26 100.15 o -4 -1 1 8271.71 7612.27 173.20 o -3 -1 1 1556.26 1462.53 73.91 o -2 -1 1 38112.35 38915.97 931.18 o -1 -1 1 10918.52 10740.05 609.07 o 0 -1 1 7304.14 7102.11 246.33 o 1 -1 1 225.25 238.93 75.46 o 2 -1 1 8034.07 8293.73 136.49 o 3 -1 1 8550.06 7990.23 99.66 o 4 -1 1 401.93 343.01 45.17 o 5 -1 1 3121.62 2974.33 67.92 o 6 -1 1 3029.60 3103.90 66.50 o 7 -1 1 1701.29 1628.06 60.31 o 8 -1 1 1152.67 1083.77 73.22 o 9 -1 1 2326.18 2203.75 75.23 o -10 0 1 1717.51 1525.79 100.34 o -9 0 1 268.12 271.13 67.60 o -8 0 1 160.81 204.31 63.29 o -7 0 1 4391.34 4562.14 110.31 o -6 0 1 4915.69 5008.52 78.28 o -5 0 1 729.01 695.71 65.19 o -4 0 1 10064.54 9519.80 101.60 o -3 0 1 17838.39 18505.31 251.52 o -2 0 1 119.08 120.41 82.84 o -1 0 1 1302.15 1555.63 119.02 o 1 0 1 4198.65 4086.01 98.19 o 2 0 1 43.12 126.98 86.31 o 3 0 1 12852.91 11783.51 137.33 o 4 0 1 6768.66 6211.00 169.16 o 5 0 1 166.42 180.69 55.74 o 6 0 1 1456.81 1508.19 59.92 o 7 0 1 2636.28 2776.52 82.44 o 8 0 1 14.77 25.83 83.11 o 9 0 1 414.69 329.89 97.14 o -10 1 1 597.48 572.58 97.19 o -9 1 1 2525.64 2484.59 77.29 o -8 1 1 650.37 696.79 66.14 o -7 1 1 754.20 748.39 60.73 o -6 1 1 4354.02 4383.89 74.72 o -5 1 1 3163.75 2909.64 79.13 o -4 1 1 410.20 333.89 51.54 o -3 1 1 4855.83 5497.00 99.42 o -2 1 1 8546.74 8933.73 125.76 o -1 1 1 163.22 145.02 83.26 o 0 1 1 450.68 422.30 68.88 o 1 1 1 8152.02 7805.07 113.06 o 2 1 1 441.74 500.01 57.18 o 3 1 1 7831.03 7563.27 87.14 o 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