##############################################################################
### ###
### Electronic paper (Acta Crystallographica Section E) ###
### ###
##############################################################################
# #
# This CIF contains the data in a paper accepted for publication in Acta #
# Crystallographica Section E. It conforms to the requirements of Notes #
# for Authors for Section E, and has been peer reviewed under the auspices #
# of the IUCr Commission on Journals. #
# #
# Full details of the Crystallographic Information File format #
# are given in the paper "The Crystallographic Information File (CIF): #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H. #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. #
# #
# The current version of the core CIF dictionary is obtainable from #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1. #
# #
# Software is freely available for graphical display of the structure(s) in #
# this CIF. For information consult the CIF home page http://www.iucr.org/ #
# cif/home.html #
# #
# Copyright International Union of Crystallography #
# #
##############################################################################
data_I
_audit_creation_method SHELXL-97
_chemical_name_systematic
;
{(E)-2-[2-(2,3-Dimethyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrazol-4-
yliminomethyl)phenoxy]acetic acid monohydrate
;
_chemical_name_common ?
_chemical_formula_moiety 'C20 H19 N3 O4, H2 O'
_chemical_formula_sum 'C20 H21 N3 O5'
_chemical_formula_iupac 'C20 H19 N3 O4, H2 O'
_chemical_formula_weight 383.40
_chemical_melting_point '466.2-466.9'
_symmetry_cell_setting 'monoclinic'
_symmetry_space_group_name_H-M 'C 2/c'
_symmetry_space_group_name_Hall '-C 2yc'
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
_cell_length_a 18.0213(15)
_cell_length_b 6.8755(6)
_cell_length_c 30.352(3)
_cell_angle_alpha 90.00
_cell_angle_beta 94.518(2)
_cell_angle_gamma 90.00
_cell_volume 3749.1(6)
_cell_formula_units_Z 8
_cell_measurement_reflns_used 1657
_cell_measurement_theta_min 2.27
_cell_measurement_theta_max 25.00
_cell_measurement_temperature 296(2)
_exptl_crystal_description block
_exptl_crystal_colour yellow
_exptl_crystal_size_max 0.20
_exptl_crystal_size_mid 0.14
_exptl_crystal_size_min 0.08
_exptl_crystal_density_diffrn 1.359
_exptl_crystal_density_meas ?
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 1616
_exptl_absorpt_coefficient_mu 0.099
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details '(SADABS; Bruker, 2004)'
_exptl_absorpt_correction_T_min 0.98
_exptl_absorpt_correction_T_max 0.99
_exptl_special_details
;
?
;
_diffrn_ambient_temperature 296(2)
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_source 'fine-focus sealed tube'
_diffrn_radiation_monochromator graphite
_diffrn_measurement_device_type 'Bruker APEX-II area-detector'
_diffrn_measurement_method '\f and \w'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number 10093
_diffrn_reflns_av_R_equivalents 0.0675
_diffrn_reflns_av_sigmaI/netI 0.0803
_diffrn_reflns_theta_min 2.27
_diffrn_reflns_theta_max 25.00
_diffrn_reflns_theta_full 25.00
_diffrn_measured_fraction_theta_max 0.976
_diffrn_measured_fraction_theta_full 0.976
_diffrn_reflns_limit_h_min -21
_diffrn_reflns_limit_h_max 21
_diffrn_reflns_limit_k_min -8
_diffrn_reflns_limit_k_max 7
_diffrn_reflns_limit_l_min -36
_diffrn_reflns_limit_l_max 34
_diffrn_standards_number 0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time 0
_diffrn_standards_decay_% 0
_refine_special_details
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;
_reflns_number_total 3231
_reflns_number_gt 1522
_reflns_threshold_expression I>2\s(I)
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type full
_refine_ls_R_factor_all 0.1236
_refine_ls_R_factor_gt 0.0516
_refine_ls_wR_factor_gt 0.1091
_refine_ls_wR_factor_ref 0.1265
_refine_ls_goodness_of_fit_ref 1.009
_refine_ls_restrained_S_all 1.010
_refine_ls_number_reflns 3231
_refine_ls_number_parameters 265
_refine_ls_number_restraints 3
_refine_ls_hydrogen_treatment mixed
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0499P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_diff_density_max 0.184
_refine_diff_density_min -0.177
_refine_ls_extinction_method APEX2
_refine_ls_extinction_coef 0.0009(2)
_refine_ls_extinction_expression
'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
'C' 'C' 0.0033 0.0016
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'H' 'H' 0.0000 0.0000
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'N' 'N' 0.0061 0.0033
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'O' 'O' 0.0106 0.0060
'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection 'APEX2 (Bruker, 2004)'
_computing_cell_refinement 'APEX2'
_computing_data_reduction 'APEX2'
_computing_structure_solution 'APEX2'
_computing_structure_refinement 'APEX2'
_computing_molecular_graphics 'APEX2'
_computing_publication_material 'APEX2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O O1 -0.00791(11) 0.6046(3) 0.87063(7) 0.0610(6) Uani d . 1 . .
O O2 0.18056(11) 0.8674(3) 0.94052(7) 0.0574(6) Uani d . 1 . .
O O3 0.05648(12) 1.0462(4) 0.95971(8) 0.0841(8) Uani d . 1 . .
O O4 0.12074(13) 1.2879(4) 0.99355(9) 0.0860(8) Uani d . 1 . .
H H4A 0.0792 1.3259 0.9987 0.129 Uiso calc R 1 . .
O O5 0.00245(16) 0.6615(5) 0.96328(10) 0.0902(8) Uani d D 1 . .
N N1 -0.05004(12) 0.3334(3) 0.83101(8) 0.0489(7) Uani d . 1 . .
N N2 -0.01738(13) 0.1641(4) 0.81545(8) 0.0492(6) Uani d . 1 . .
N N3 0.14185(12) 0.3618(4) 0.87651(7) 0.0487(6) Uani d . 1 . .
C C1 0.15482(16) 0.5224(5) 0.89700(9) 0.0497(8) Uani d . 1 . .
H H1 0.1150 0.6028 0.9024 0.060 Uiso calc R 1 . .
C C2 0.23058(15) 0.5836(4) 0.91218(9) 0.0449(8) Uani d . 1 . .
C C3 0.24315(16) 0.7617(5) 0.93360(9) 0.0492(8) Uani d . 1 . .
C C4 0.31477(17) 0.8228(5) 0.94696(10) 0.0574(9) Uani d . 1 . .
H H4 0.3225 0.9411 0.9615 0.069 Uiso calc R 1 . .
C C5 0.37456(18) 0.7064(6) 0.93853(11) 0.0668(10) Uani d . 1 . .
H H5 0.4227 0.7480 0.9469 0.080 Uiso calc R 1 . .
C C6 0.36338(17) 0.5296(5) 0.91789(10) 0.0672(10) Uani d . 1 . .
H H6 0.4038 0.4507 0.9129 0.081 Uiso calc R 1 . .
C C7 0.29245(16) 0.4699(5) 0.90473(10) 0.0591(9) Uani d . 1 . .
H H7 0.2854 0.3508 0.8905 0.071 Uiso calc R 1 . .
C C8 0.18960(16) 1.0448(4) 0.96428(9) 0.0531(8) Uani d . 1 . .
H H8A 0.2168 1.1374 0.9476 0.064 Uiso calc R 1 . .
H H8B 0.2176 1.0223 0.9924 0.064 Uiso calc R 1 . .
C C9 0.11482(19) 1.1230(5) 0.97158(11) 0.0601(9) Uani d . 1 . .
C C10 0.00416(16) 0.4392(5) 0.85674(9) 0.0479(8) Uani d . 1 . .
C C11 0.06979(16) 0.3183(4) 0.85914(9) 0.0437(8) Uani d . 1 . .
C C12 0.05254(16) 0.1511(4) 0.83597(9) 0.0465(8) Uani d . 1 . .
C C13 0.09902(16) -0.0241(4) 0.83191(10) 0.0640(9) Uani d . 1 . .
H H13A 0.1462 -0.0057 0.8484 0.096 Uiso calc R 1 . .
H H13B 0.1068 -0.0456 0.8014 0.096 Uiso calc R 1 . .
H H13C 0.0743 -0.1347 0.8433 0.096 Uiso calc R 1 . .
C C14 -0.06675(17) -0.0012(4) 0.80614(10) 0.0636(9) Uani d . 1 . .
H H14A -0.0792 -0.0584 0.8334 0.095 Uiso calc R 1 . .
H H14B -0.0422 -0.0960 0.7892 0.095 Uiso calc R 1 . .
H H14C -0.1114 0.0420 0.7897 0.095 Uiso calc R 1 . .
C C15 -0.10746(15) 0.4290(4) 0.80384(9) 0.0440(8) Uani d . 1 . .
C C16 -0.10647(15) 0.4333(4) 0.75853(10) 0.0492(8) Uani d . 1 . .
H H16 -0.0699 0.3658 0.7448 0.059 Uiso calc R 1 . .
C C17 -0.16005(16) 0.5383(5) 0.73342(10) 0.0560(9) Uani d . 1 . .
H H17 -0.1601 0.5393 0.7028 0.067 Uiso calc R 1 . .
C C18 -0.21312(16) 0.6412(4) 0.75379(11) 0.0562(9) Uani d . 1 . .
H H18 -0.2483 0.7148 0.7370 0.067 Uiso calc R 1 . .
C C19 -0.21403(16) 0.6349(4) 0.79913(11) 0.0581(9) Uani d . 1 . .
H H19 -0.2502 0.7037 0.8129 0.070 Uiso calc R 1 . .
C C20 -0.16193(16) 0.5276(4) 0.82428(10) 0.0551(9) Uani d . 1 . .
H H20 -0.1634 0.5217 0.8548 0.066 Uiso calc R 1 . .
H H5A 0.023(2) 0.779(3) 0.9636(12) 0.106(17) Uiso d D 1 . .
H H5B -0.004(3) 0.624(7) 0.9351(9) 0.25(4) Uiso d D 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O1 0.0587(14) 0.0502(16) 0.0713(15) 0.0059(12) -0.0131(11) -0.0163(12)
O2 0.0520(13) 0.0486(15) 0.0696(14) 0.0000(11) -0.0079(10) -0.0162(11)
O3 0.0553(15) 0.087(2) 0.108(2) -0.0058(14) -0.0044(13) -0.0360(15)
O4 0.0727(17) 0.078(2) 0.107(2) 0.0003(14) 0.0019(16) -0.0411(16)
O5 0.095(2) 0.090(3) 0.086(2) -0.0152(18) 0.0091(15) -0.0088(17)
N1 0.0478(15) 0.0405(17) 0.0564(16) 0.0014(13) -0.0091(12) -0.0090(13)
N2 0.0508(16) 0.0374(17) 0.0581(16) -0.0038(13) -0.0048(12) -0.0050(12)
N3 0.0510(16) 0.0434(17) 0.0497(15) -0.0025(13) -0.0082(12) -0.0025(13)
C1 0.0458(18) 0.053(2) 0.0496(19) 0.0033(16) -0.0023(14) 0.0029(16)
C2 0.0480(19) 0.048(2) 0.0379(17) -0.0027(16) -0.0024(13) -0.0020(15)
C3 0.045(2) 0.055(2) 0.0472(19) 0.0031(17) -0.0007(15) 0.0030(16)
C4 0.049(2) 0.062(2) 0.059(2) -0.0068(18) -0.0077(16) -0.0088(17)
C5 0.044(2) 0.085(3) 0.071(2) -0.008(2) -0.0032(17) -0.002(2)
C6 0.048(2) 0.081(3) 0.072(2) 0.009(2) 0.0012(17) -0.005(2)
C7 0.054(2) 0.065(3) 0.056(2) 0.0067(19) -0.0042(16) -0.0085(17)
C8 0.0546(19) 0.046(2) 0.057(2) -0.0042(16) -0.0030(15) -0.0060(16)
C9 0.060(2) 0.060(3) 0.060(2) -0.001(2) 0.0018(17) -0.0109(19)
C10 0.053(2) 0.041(2) 0.0483(19) -0.0044(17) -0.0066(14) 0.0008(16)
C11 0.0490(19) 0.038(2) 0.0428(17) -0.0013(15) -0.0047(14) 0.0026(14)
C12 0.0474(19) 0.042(2) 0.0483(18) -0.0002(16) -0.0048(14) 0.0050(15)
C13 0.069(2) 0.046(2) 0.075(2) 0.0089(18) -0.0070(17) -0.0029(17)
C14 0.065(2) 0.046(2) 0.078(2) -0.0138(18) -0.0036(17) -0.0039(18)
C15 0.0394(17) 0.041(2) 0.051(2) -0.0054(15) -0.0040(14) -0.0057(15)
C16 0.0422(18) 0.053(2) 0.052(2) 0.0021(15) 0.0044(14) -0.0056(16)
C17 0.055(2) 0.061(2) 0.0515(19) -0.0019(18) -0.0017(16) 0.0021(17)
C18 0.0464(19) 0.050(2) 0.070(3) 0.0074(17) -0.0091(17) 0.0010(17)
C19 0.049(2) 0.058(2) 0.067(2) 0.0062(17) 0.0010(16) -0.0097(18)
C20 0.0510(19) 0.058(2) 0.056(2) 0.0003(18) 0.0009(16) -0.0033(17)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
O1 C10 . 1.238(3) y
O2 C3 . 1.372(3) ?
O2 C8 . 1.420(3) ?
O3 C9 . 1.206(4) ?
O4 C9 . 1.315(4) ?
O4 H4A . 0.8200 ?
O5 H5A . 0.883(18) ?
O5 H5B . 0.892(19) ?
N1 N2 . 1.403(3) y
N1 C10 . 1.405(3) y
N1 C15 . 1.432(3) y
N2 C12 . 1.364(3) y
N2 C14 . 1.457(3) y
N3 C1 . 1.280(3) y
N3 C11 . 1.395(3) y
C1 C2 . 1.468(4) y
C1 H1 . 0.9300 ?
C2 C7 . 1.395(4) ?
C2 C3 . 1.396(4) ?
C3 C4 . 1.387(4) ?
C4 C5 . 1.382(4) ?
C4 H4 . 0.9300 ?
C5 C6 . 1.375(4) ?
C5 H5 . 0.9300 ?
C6 C7 . 1.372(4) ?
C6 H6 . 0.9300 ?
C7 H7 . 0.9300 ?
C8 C9 . 1.484(4) ?
C8 H8A . 0.9700 ?
C8 H8B . 0.9700 ?
C10 C11 . 1.443(4) ?
C11 C12 . 1.370(4) y
C12 C13 . 1.478(4) ?
C13 H13A . 0.9600 ?
C13 H13B . 0.9600 ?
C13 H13C . 0.9600 ?
C14 H14A . 0.9600 ?
C14 H14B . 0.9600 ?
C14 H14C . 0.9600 ?
C15 C16 . 1.377(4) ?
C15 C20 . 1.380(4) ?
C16 C17 . 1.385(4) ?
C16 H16 . 0.9300 ?
C17 C18 . 1.375(4) ?
C17 H17 . 0.9300 ?
C18 C19 . 1.378(4) ?
C18 H18 . 0.9300 ?
C19 C20 . 1.377(4) ?
C19 H19 . 0.9300 ?
C20 H20 . 0.9300 ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C3 O2 C8 . . 118.0(2) ?
C9 O4 H4A . . 109.5 ?
H5A O5 H5B . . 108(3) ?
N2 N1 C10 . . 109.0(2) y
N2 N1 C15 . . 119.4(2) y
C10 N1 C15 . . 121.4(2) y
C12 N2 N1 . . 107.3(2) y
C12 N2 C14 . . 124.5(3) y
N1 N2 C14 . . 116.5(2) y
C1 N3 C11 . . 119.9(3) y
N3 C1 C2 . . 122.0(3) y
N3 C1 H1 . . 119.0 ?
C2 C1 H1 . . 119.0 ?
C7 C2 C3 . . 117.7(3) ?
C7 C2 C1 . . 121.6(3) ?
C3 C2 C1 . . 120.7(3) ?
O2 C3 C4 . . 123.5(3) ?
O2 C3 C2 . . 115.5(3) ?
C4 C3 C2 . . 121.0(3) ?
C5 C4 C3 . . 119.4(3) ?
C5 C4 H4 . . 120.3 ?
C3 C4 H4 . . 120.3 ?
C6 C5 C4 . . 120.5(3) ?
C6 C5 H5 . . 119.7 ?
C4 C5 H5 . . 119.7 ?
C7 C6 C5 . . 119.8(3) ?
C7 C6 H6 . . 120.1 ?
C5 C6 H6 . . 120.1 ?
C6 C7 C2 . . 121.6(3) ?
C6 C7 H7 . . 119.2 ?
C2 C7 H7 . . 119.2 ?
O2 C8 C9 . . 108.6(3) ?
O2 C8 H8A . . 110.0 ?
C9 C8 H8A . . 110.0 ?
O2 C8 H8B . . 110.0 ?
C9 C8 H8B . . 110.0 ?
H8A C8 H8B . . 108.4 ?
O3 C9 O4 . . 124.3(3) ?
O3 C9 C8 . . 125.2(3) ?
O4 C9 C8 . . 110.5(3) ?
O1 C10 N1 . . 122.1(3) y
O1 C10 C11 . . 132.6(3) y
N1 C10 C11 . . 105.1(3) ?
C12 C11 N3 . . 122.7(3) ?
C12 C11 C10 . . 107.8(3) ?
N3 C11 C10 . . 129.1(3) ?
N2 C12 C11 . . 110.1(3) ?
N2 C12 C13 . . 121.6(3) ?
C11 C12 C13 . . 128.3(3) ?
C12 C13 H13A . . 109.5 ?
C12 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C12 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
N2 C14 H14A . . 109.5 ?
N2 C14 H14B . . 109.5 ?
H14A C14 H14B . . 109.5 ?
N2 C14 H14C . . 109.5 ?
H14A C14 H14C . . 109.5 ?
H14B C14 H14C . . 109.5 ?
C16 C15 C20 . . 120.3(3) ?
C16 C15 N1 . . 121.3(3) ?
C20 C15 N1 . . 118.3(3) ?
C15 C16 C17 . . 119.8(3) ?
C15 C16 H16 . . 120.1 ?
C17 C16 H16 . . 120.1 ?
C18 C17 C16 . . 120.0(3) ?
C18 C17 H17 . . 120.0 ?
C16 C17 H17 . . 120.0 ?
C17 C18 C19 . . 119.8(3) ?
C17 C18 H18 . . 120.1 ?
C19 C18 H18 . . 120.1 ?
C20 C19 C18 . . 120.6(3) ?
C20 C19 H19 . . 119.7 ?
C18 C19 H19 . . 119.7 ?
C19 C20 C15 . . 119.5(3) ?
C19 C20 H20 . . 120.3 ?
C15 C20 H20 . . 120.3 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_D
_geom_hbond_site_symmetry_H
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O4 H4A O5 . . 5_577 0.82 1.94 2.688(4) 151.0 yes
O5 H5B O1 . . ? 0.89(2) 1.96(3) 2.831(4) 166(4) yes
O5 H5A O3 . . ? 0.88(2) 1.95(3) 2.823(4) 173(4) yes
C4 H4 O4 . . 7_577 0.93 2.48 3.383(4) 163.0 yes
C13 H13C O1 . . 1_545 0.96 2.51 3.459(4) 171.5 yes
data_global
_journal_date_recd_electronic 2006-07-03
_journal_date_accepted 2006-07-21
_journal_name_full 'Acta Crystallographica, Section E'
_journal_year 2006
_journal_volume 62
_journal_issue 8
_journal_page_first o3558
_journal_page_last o3560
_journal_paper_category EO
_journal_coeditor_code HG2063
_publ_contact_author_name 'Xiao-Niu Fang'
_publ_contact_author_address
;
College of Chemistry & Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
China
;
_publ_contact_author_email fangxiaoniu@163.com
_publ_contact_author_fax '+86-796-8100490'
_publ_contact_author_phone '+86-796-8859572'
_publ_section_title
;
{(E)-2-[2-(2,3-Dimethyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrazol-4-
yliminomethyl)phenoxy]acetic acid monohydrate
;
loop_
_publ_author_name
_publ_author_address
'Hu, Rong-Hua'
;
JiangXi Province Key Laboratory of Coordination Chemistry
College of Chemistry and Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
People's Republic of China
;
'Fang, Xiao-Niu'
;
JiangXi Province Key Laboratory of Coordination Chemistry
College of Chemistry and Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
People's Republic of China
;
'Sui, Yan'
;
JiangXi Province Key Laboratory of Coordination Chemistry
College of Chemistry and Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
People's Republic of China
;
'Luo, Qiu-Yan'
;
JiangXi Province Key Laboratory of Coordination Chemistry
College of Chemistry and Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
People's Republic of China
;
'Zou, Meng-Qiang'
;
JiangXi Province Key Laboratory of Coordination Chemistry
College of Chemistry and Chemical Engineering
JingGangShan University
343009 Ji'an, JiangXi
People's Republic of China
;