# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' bark in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 201.87 _exptl_crystal_F_000 784.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.6570 _cell_length_b 14.4120 _cell_length_c 14.6990 _cell_angle_alpha 62.880 _cell_angle_beta 88.320 _cell_angle_gamma 72.020 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11536.89 11059.67 207.00 o 3 0 0 2808.85 2455.71 50.61 o 4 0 0 29356.68 30639.53 1878.03 o 5 0 0 5001.45 4752.71 272.47 o 6 0 0 698.45 739.52 55.75 o 7 0 0 639.91 598.86 42.73 o 8 0 0 2501.87 2400.63 61.87 o 9 0 0 162.07 81.15 27.72 o 10 0 0 697.46 638.90 134.70 o 11 0 0 161.49 188.49 42.71 o 12 0 0 726.66 1058.60 147.53 o -12 1 0 23.45 591.34 72.45 o -11 1 0 696.87 740.54 55.17 o -10 1 0 2350.14 2531.85 336.74 o -9 1 0 4047.32 4197.26 220.19 o -8 1 0 3232.86 3509.88 538.19 o -7 1 0 2661.45 2596.20 320.72 o -6 1 0 2835.41 3009.49 117.55 o -5 1 0 678.46 620.50 79.82 o -4 1 0 12431.96 12734.41 132.72 o -3 1 0 1675.91 1850.64 212.07 o -2 1 0 5465.56 5617.08 231.54 o -1 1 0 1832.95 1812.25 22.42 o 2 1 0 18.23 114.12 32.80 o 3 1 0 98.71 106.99 50.96 o 4 1 0 17081.93 18562.12 507.76 o 5 1 0 87.54 221.83 83.35 o 6 1 0 4736.59 4779.93 251.35 o 7 1 0 242.33 461.93 201.35 o 8 1 0 4852.63 4890.35 564.97 o 9 1 0 4.24 46.93 26.63 o 10 1 0 578.30 450.48 48.79 o 11 1 0 678.02 429.92 150.41 o 12 1 0 2586.65 3155.99 242.34 o -11 2 0 1791.17 2047.58 263.03 o -10 2 0 3717.75 3739.38 267.06 o -9 2 0 4204.30 4261.20 81.32 o -8 2 0 1358.63 1358.88 79.55 o -7 2 0 1477.84 1305.19 89.79 o -6 2 0 5430.13 5424.24 200.53 o -5 2 0 2725.33 2718.46 79.92 o -4 2 0 699.08 493.43 44.78 o -3 2 0 336.84 329.54 78.41 o -2 2 0 8947.69 8859.43 307.19 o -1 2 0 3408.49 3331.77 47.38 o 0 2 0 902.60 1120.31 35.28 o 1 2 0 0.90 86.56 29.23 o 2 2 0 32066.70 31466.87 601.47 o 3 2 0 3086.02 3204.18 68.72 o 4 2 0 40750.98 44368.02 1533.86 o 5 2 0 1526.40 1933.00 101.60 o 6 2 0 6030.66 6522.26 307.87 o 7 2 0 209.59 378.67 79.15 o 8 2 0 11404.01 11337.35 277.20 o 9 2 0 158.45 197.69 28.89 o 10 2 0 811.23 811.47 143.50 o 11 2 0 1336.97 1149.32 120.15 o 12 2 0 3553.99 3877.82 99.09 o -11 3 0 1193.46 1862.89 118.56 o -10 3 0 3518.06 3836.54 231.86 o -9 3 0 937.92 933.04 218.97 o -8 3 0 39.70 51.12 23.95 o -7 3 0 1950.20 2023.82 69.32 o -6 3 0 6114.54 5927.96 505.19 o -5 3 0 3144.28 3371.22 118.77 o -4 3 0 118.25 139.59 83.33 o -3 3 0 5728.44 5671.89 212.04 o -2 3 0 13339.63 13591.72 214.68 o -1 3 0 11215.00 11772.73 77.16 o 0 3 0 108.17 157.54 33.13 o 1 3 0 421.79 660.97 162.81 o 2 3 0 5677.94 5436.01 95.61 o 3 3 0 7.26 93.40 28.54 o 4 3 0 9958.32 9846.26 515.90 o 5 3 0 29.72 26.04 8.94 o 6 3 0 101.12 87.07 15.37 o 7 3 0 1388.34 1231.38 97.89 o 8 3 0 8407.24 7769.49 637.78 o 9 3 0 1645.97 1567.87 115.72 o 10 3 0 1163.07 1018.15 61.33 o 11 3 0 316.29 351.18 60.40 o 12 3 0 2037.84 2787.83 159.52 o -10 4 0 1201.78 1282.58 101.41 o -9 4 0 600.97 677.82 144.36 o -8 4 0 77.85 135.65 46.54 o -7 4 0 1035.09 1026.42 54.34 o -6 4 0 6702.43 6539.77 83.86 o -5 4 0 1155.25 1248.71 50.89 o -4 4 0 890.70 725.77 27.40 o -3 4 0 6563.76 6324.00 196.29 o -2 4 0 11900.65 12678.98 208.75 o -1 4 0 2631.18 3075.30 68.26 o 0 4 0 416.28 322.28 27.70 o 1 4 0 2521.77 3422.88 103.72 o 2 4 0 21270.20 20335.06 277.97 o 3 4 0 2340.66 2174.57 78.03 o 4 4 0 316.61 243.68 36.16 o 5 4 0 549.85 565.56 42.82 o 6 4 0 6791.85 6850.05 92.33 o 7 4 0 184.35 127.37 11.99 o 8 4 0 2815.78 2837.93 112.60 o 9 4 0 642.48 665.09 166.67 o 10 4 0 2152.58 2171.77 89.89 o 11 4 0 34.37 22.48 28.37 o 12 4 0 1069.66 2152.82 114.03 o 13 4 0 524.87 618.74 170.28 o -10 5 0 313.01 330.48 79.04 o -9 5 0 5.89 44.23 52.91 o -8 5 0 464.92 359.51 53.12 o -7 5 0 3020.55 2755.05 139.64 o -6 5 0 1582.33 1505.33 42.72 o -5 5 0 1512.78 1390.60 44.45 o -4 5 0 1915.82 1852.18 208.74 o -3 5 0 2564.96 2349.97 176.24 o -2 5 0 6312.57 5574.87 135.08 o -1 5 0 63.47 241.90 32.70 o 0 5 0 7237.73 9227.85 303.11 o 1 5 0 2187.34 2482.12 113.72 o 2 5 0 12701.92 12293.88 309.88 o 3 5 0 1733.45 2318.09 265.86 o 4 5 0 144.41 170.64 44.14 o 5 5 0 38.19 25.56 18.28 o 6 5 0 5914.98 5790.67 304.68 o 7 5 0 2206.75 2248.66 65.61 o 8 5 0 113.42 41.01 32.41 o 9 5 0 21.10 15.33 41.39 o 10 5 0 1321.06 1210.72 96.50 o 11 5 0 45.14 66.48 35.71 o 12 5 0 2260.92 2849.80 211.90 o 13 5 0 397.56 439.98 58.84 o -9 6 0 289.69 346.24 85.54 o -8 6 0 2869.66 2685.41 451.06 o -7 6 0 5145.30 4686.21 596.55 o -6 6 0 631.53 705.07 61.65 o -5 6 0 443.11 366.65 87.35 o -4 6 0 1138.59 1122.64 38.82 o -3 6 0 344.69 321.37 32.50 o -2 6 0 6143.50 3958.43 775.45 o -1 6 0 147.65 166.76 70.39 o 0 6 0 5143.95 6789.63 240.97 o 1 6 0 2977.08 2671.02 66.80 o 2 6 0 10497.76 10614.56 177.46 o 3 6 0 1037.46 997.65 42.51 o 4 6 0 4332.48 4229.72 159.45 o 5 6 0 1132.63 986.69 122.92 o 6 6 0 12911.40 12815.22 109.62 o 7 6 0 1743.82 1651.58 290.08 o 8 6 0 5094.71 5215.46 259.14 o 9 6 0 12.30 38.29 53.88 o 10 6 0 3432.37 3474.12 129.17 o 11 6 0 192.92 243.76 65.85 o 12 6 0 2168.03 3043.74 154.18 o 13 6 0 537.26 463.73 104.18 o -9 7 0 1923.62 2107.11 121.58 o -8 7 0 1130.65 1260.94 75.55 o -7 7 0 634.54 582.78 59.72 o -6 7 0 73.73 53.79 28.76 o -5 7 0 324.46 225.35 38.32 o -4 7 0 855.62 761.68 58.65 o -3 7 0 942.56 778.47 117.35 o -2 7 0 1022.39 1031.55 64.75 o -1 7 0 1209.01 1122.77 56.49 o 0 7 0 2020.18 2910.19 75.56 o 1 7 0 792.68 685.06 66.70 o 2 7 0 3337.87 3030.98 150.25 o 3 7 0 872.72 895.32 60.98 o 4 7 0 6548.90 6310.72 147.75 o 5 7 0 1073.68 932.06 51.08 o 6 7 0 9868.14 9801.32 247.82 o 7 7 0 14.91 37.67 22.88 o 8 7 0 877.52 896.05 168.86 o 9 7 0 75.55 114.46 42.06 o 10 7 0 1899.36 1856.78 114.55 o 11 7 0 4.43 42.84 70.77 o 12 7 0 225.95 1109.05 208.19 o 13 7 0 62.32 100.25 43.17 o -8 8 0 757.20 976.29 111.68 o -7 8 0 211.03 117.55 33.61 o -6 8 0 10.72 45.63 25.66 o -5 8 0 1110.09 849.28 62.01 o -4 8 0 3015.24 2854.86 164.67 o -3 8 0 6934.92 6262.74 256.59 o -2 8 0 80.47 79.18 31.11 o -1 8 0 2296.38 2359.58 64.23 o 0 8 0 705.48 883.55 59.20 o 1 8 0 1469.40 1815.87 75.96 o 2 8 0 999.46 789.13 128.84 o 3 8 0 77.99 100.48 34.27 o 4 8 0 8096.35 7588.03 352.76 o 5 8 0 2642.75 2390.85 59.35 o 6 8 0 2919.93 2708.34 190.34 o 7 8 0 571.93 518.86 64.08 o 8 8 0 1318.26 1205.68 67.54 o 9 8 0 1.59 28.98 33.46 o 10 8 0 4647.95 4528.98 96.76 o 11 8 0 178.51 241.27 71.67 o 12 8 0 653.09 1277.49 108.86 o -7 9 0 776.41 508.58 130.26 o -6 9 0 81.98 75.55 47.92 o -5 9 0 2651.41 2499.17 76.69 o -4 9 0 2616.37 2755.52 198.52 o -3 9 0 3964.21 3557.73 255.59 o -2 9 0 222.37 114.16 40.85 o -1 9 0 470.22 453.11 51.71 o 0 9 0 1403.51 1541.81 56.36 o 1 9 0 1559.48 2028.52 103.80 o 2 9 0 2513.42 2139.22 223.17 o 3 9 0 1136.86 924.67 205.09 o 4 9 0 1223.02 1077.05 43.67 o 5 9 0 89.21 101.20 28.65 o 6 9 0 1085.33 993.49 58.00 o 7 9 0 893.74 805.13 50.02 o 8 9 0 3082.68 3067.82 344.29 o 9 9 0 24.54 41.56 29.84 o 10 9 0 3617.17 3760.43 101.75 o 11 9 0 0.02 109.86 134.50 o 12 9 0 345.20 631.65 84.04 o -6 10 0 727.67 701.62 178.04 o -5 10 0 3081.49 2927.05 347.29 o -4 10 0 2314.58 2448.45 179.94 o -3 10 0 149.36 200.24 47.40 o -2 10 0 3374.97 2817.91 134.64 o -1 10 0 1405.87 1401.84 148.70 o 0 10 0 5617.86 7215.65 223.80 o 1 10 0 771.49 769.29 59.61 o 2 10 0 631.35 595.15 34.88 o 3 10 0 221.13 179.85 66.02 o 4 10 0 122.03 83.33 33.24 o 5 10 0 34.24 72.66 47.50 o 6 10 0 620.57 462.94 29.35 o 7 10 0 522.89 440.17 69.44 o 8 10 0 1770.47 1830.24 78.17 o 9 10 0 1285.65 1106.89 65.00 o 10 10 0 2307.09 2535.35 328.53 o 11 10 0 442.40 576.41 73.14 o 12 10 0 1281.20 1469.08 122.33 o -5 11 0 1245.92 1057.71 81.39 o -4 11 0 76.36 95.55 38.40 o -3 11 0 7.10 70.07 68.54 o -2 11 0 228.59 173.86 80.82 o -1 11 0 2638.68 2760.85 263.54 o 0 11 0 2547.20 3265.79 190.86 o 1 11 0 1353.15 1733.84 192.56 o 2 11 0 199.81 205.95 46.96 o 3 11 0 1611.81 1578.18 113.80 o 4 11 0 4556.80 3979.96 273.92 o 5 11 0 1834.77 1619.67 176.50 o 6 11 0 2790.40 2571.62 69.14 o 7 11 0 801.47 589.74 94.78 o 8 11 0 3570.26 3518.78 209.57 o 9 11 0 325.49 209.57 41.51 o 10 11 0 1045.22 1029.96 148.24 o 11 11 0 799.23 883.00 81.60 o -4 12 0 2.12 45.85 33.44 o -3 12 0 198.86 162.04 43.73 o -2 12 0 826.01 695.27 72.25 o -1 12 0 3310.77 3229.69 100.48 o 0 12 0 2149.61 2616.82 147.38 o 1 12 0 1969.45 2437.42 110.60 o 2 12 0 2819.70 2955.98 174.85 o 3 12 0 1943.52 1868.27 129.09 o 4 12 0 7561.71 8637.26 208.97 o 5 12 0 994.76 902.10 50.03 o 6 12 0 4777.04 4523.44 126.41 o 7 12 0 188.32 296.10 47.25 o 8 12 0 2430.77 2370.86 96.86 o 9 12 0 76.06 61.86 52.28 o 10 12 0 822.68 684.52 205.94 o 11 12 0 14.51 73.85 31.04 o -3 13 0 2492.43 2378.62 334.56 o -2 13 0 747.78 728.86 239.67 o -1 13 0 3847.24 3844.89 134.73 o 0 13 0 435.40 595.82 56.61 o 1 13 0 209.42 1148.71 73.26 o 2 13 0 1841.66 1641.25 171.10 o 3 13 0 1049.64 778.74 84.85 o 4 13 0 2869.84 2951.99 125.30 o 5 13 0 61.49 87.32 57.19 o 6 13 0 561.98 560.67 85.59 o 7 13 0 680.27 666.24 53.81 o 8 13 0 2255.46 2229.90 96.28 o 9 13 0 112.32 116.49 36.49 o 10 13 0 1098.91 1095.21 72.66 o -1 14 0 1006.21 1101.04 151.36 o 0 14 0 95.23 82.20 36.27 o 1 14 0 119.69 1477.29 163.15 o 2 14 0 911.35 860.51 71.47 o 3 14 0 3405.32 2969.75 136.01 o 4 14 0 272.97 202.79 73.80 o 5 14 0 403.97 422.19 106.67 o 6 14 0 128.31 157.32 82.14 o 7 14 0 2229.22 2366.93 141.11 o 8 14 0 3013.10 3342.12 126.21 o 9 14 0 230.12 179.03 77.51 o 1 15 0 2034.24 2381.47 96.91 o 2 15 0 62.30 39.79 40.68 o 3 15 0 5296.31 5049.06 170.20 o 4 15 0 9.95 72.53 61.47 o 5 15 0 1073.79 1031.85 133.98 o 6 15 0 922.32 1001.71 138.31 o 7 15 0 1789.26 1806.87 159.96 o 8 15 0 1322.28 1766.01 145.49 o -6 -15 1 1557.95 1621.75 134.71 o -5 -15 1 200.92 88.73 51.42 o -4 -15 1 1027.50 981.40 135.87 o -3 -15 1 584.53 357.03 70.42 o -2 -15 1 3132.02 3439.17 154.33 o -8 -14 1 1681.87 1922.79 141.44 o -7 -14 1 8.09 105.44 64.25 o -6 -14 1 2566.22 2397.56 143.46 o -5 -14 1 761.26 483.02 69.66 o -4 -14 1 856.20 768.28 105.66 o -3 -14 1 840.06 793.93 95.21 o -2 -14 1 3321.21 3894.67 158.98 o -1 -14 1 667.30 843.38 79.11 o 0 -14 1 6.12 54.73 35.58 o 1 -14 1 579.57 617.38 62.67 o -10 -13 1 1931.88 2008.56 151.58 o -9 -13 1 138.12 107.07 39.21 o -8 -13 1 3619.46 4218.95 159.84 o -7 -13 1 91.65 94.13 64.41 o -6 -13 1 3406.90 3169.10 143.42 o -5 -13 1 7.06 18.10 39.93 o -4 -13 1 1586.55 1564.47 114.01 o -3 -13 1 122.74 164.40 83.44 o -2 -13 1 1856.57 1869.31 156.32 o -1 -13 1 9.61 74.68 32.41 o 0 -13 1 87.74 39.89 30.33 o 1 -13 1 838.64 914.47 97.62 o 2 -13 1 3242.73 3103.79 353.17 o -11 -12 1 57.85 160.26 173.18 o -10 -12 1 752.21 725.37 64.82 o -9 -12 1 12.24 47.39 29.57 o -8 -12 1 1085.98 1151.54 119.42 o -7 -12 1 571.47 371.78 39.66 o -6 -12 1 1377.68 984.18 65.05 o -5 -12 1 832.67 569.42 66.45 o -4 -12 1 1726.80 1585.14 113.23 o -3 -12 1 244.08 241.45 63.09 o -2 -12 1 2698.17 2648.44 95.82 o -1 -12 1 18.81 118.73 101.42 o 0 -12 1 3216.05 3985.24 107.43 o 1 -12 1 433.68 427.00 62.31 o 2 -12 1 4872.23 5019.61 117.35 o 3 -12 1 175.12 64.66 37.17 o 4 -12 1 227.04 110.35 35.05 o -11 -11 1 251.00 314.65 57.81 o -10 -11 1 122.35 207.90 65.75 o -9 -11 1 113.81 70.85 25.81 o -8 -11 1 3898.31 4038.57 246.68 o -7 -11 1 224.88 391.08 113.29 o -6 -11 1 3183.06 3030.82 132.10 o -5 -11 1 582.50 475.39 104.08 o -4 -11 1 9981.43 10039.89 169.31 o -3 -11 1 9.91 64.70 63.68 o -2 -11 1 4932.94 4792.69 205.69 o -1 -11 1 678.60 450.29 77.39 o 0 -11 1 3317.93 4420.34 111.01 o 1 -11 1 415.30 447.64 59.14 o 2 -11 1 1875.48 1530.98 74.30 o 3 -11 1 699.76 537.59 55.39 o 4 -11 1 6.10 19.80 23.63 o 5 -11 1 979.26 961.20 178.19 o -12 -10 1 419.76 756.27 123.59 o -11 -10 1 806.39 940.71 82.81 o -10 -10 1 406.90 492.10 70.86 o -9 -10 1 43.68 86.56 48.27 o -8 -10 1 7401.81 7484.82 229.30 o -7 -10 1 489.94 513.42 134.39 o -6 -10 1 621.16 518.45 36.03 o -5 -10 1 1271.16 1093.91 72.76 o -4 -10 1 5068.43 4784.54 472.06 o -3 -10 1 1206.62 991.98 90.58 o -2 -10 1 21.20 63.89 30.52 o -1 -10 1 466.34 422.36 50.15 o 0 -10 1 2397.22 3214.99 125.22 o 1 -10 1 1.92 127.67 45.27 o 2 -10 1 675.60 479.88 56.41 o 3 -10 1 106.17 92.82 40.86 o 4 -10 1 1261.91 1248.99 133.79 o 5 -10 1 256.52 150.74 39.75 o 6 -10 1 2318.09 1951.05 193.71 o -12 -9 1 533.66 719.32 75.51 o -11 -9 1 216.92 308.09 61.86 o -10 -9 1 2264.59 2505.00 149.11 o -9 -9 1 537.12 470.60 66.11 o -8 -9 1 3942.66 4014.03 130.09 o -7 -9 1 798.72 800.18 128.09 o -6 -9 1 491.04 453.01 48.02 o -5 -9 1 155.96 154.08 30.78 o -4 -9 1 3683.47 3432.70 405.10 o -3 -9 1 90.49 104.85 93.14 o -2 -9 1 2714.60 2424.36 53.15 o -1 -9 1 545.06 1154.05 77.56 o 0 -9 1 7197.78 9749.08 150.78 o 1 -9 1 63.65 139.60 38.37 o 2 -9 1 509.12 505.60 84.50 o 3 -9 1 398.08 412.38 56.68 o 4 -9 1 5401.64 5485.44 220.22 o 5 -9 1 178.26 251.97 58.45 o 6 -9 1 2030.04 1730.98 231.03 o 7 -9 1 479.84 395.14 163.75 o -12 -8 1 991.97 1423.25 147.37 o -11 -8 1 87.33 68.41 32.42 o -10 -8 1 3252.61 3327.20 98.66 o -9 -8 1 2705.29 2629.61 84.27 o -8 -8 1 896.43 872.93 59.93 o -7 -8 1 8.05 18.88 20.89 o -6 -8 1 1748.97 1639.86 62.64 o -5 -8 1 721.03 602.27 45.60 o -4 -8 1 7929.40 7486.04 540.04 o -3 -8 1 306.30 267.21 147.52 o -2 -8 1 3654.07 2997.34 204.76 o -1 -8 1 38.28 32.68 17.88 o 0 -8 1 5756.88 7279.18 100.32 o 1 -8 1 2134.43 2070.72 65.58 o 2 -8 1 337.57 349.64 57.51 o 3 -8 1 2032.86 1926.37 220.55 o 4 -8 1 7157.64 7455.33 448.02 o 5 -8 1 165.98 99.44 30.60 o 6 -8 1 23.49 51.63 41.89 o 7 -8 1 1015.70 1004.53 89.27 o 8 -8 1 1663.11 1684.58 302.51 o -12 -7 1 432.68 667.42 112.48 o -11 -7 1 694.95 533.69 85.93 o -10 -7 1 3121.55 3099.01 94.36 o -9 -7 1 381.08 321.86 56.95 o -8 -7 1 339.79 300.94 87.22 o -7 -7 1 9.47 22.42 18.26 o -6 -7 1 7389.16 7394.43 302.63 o -5 -7 1 3822.50 3567.44 176.57 o -4 -7 1 5853.66 5372.94 174.11 o -3 -7 1 2353.26 2170.42 215.06 o -2 -7 1 1805.10 1639.02 36.71 o -1 -7 1 149.86 114.03 47.58 o 0 -7 1 14166.08 19677.18 339.81 o 1 -7 1 2.76 47.70 26.27 o 2 -7 1 2869.98 2749.73 74.52 o 3 -7 1 226.82 147.08 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