# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' metalcomplex in P 21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 429.61 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.6302 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.9954 _cell_length_b 20.7450 _cell_length_c 13.5530 _cell_angle_alpha 90.000 _cell_angle_beta 93.002 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9234.79 9194.64 160.91 o 4 0 0 92827.46 92373.20 1397.64 o 6 0 0 7208.39 6776.77 162.13 o 8 0 0 11944.67 11956.09 290.89 o 10 0 0 5711.50 5901.59 189.15 o 12 0 0 800.62 768.18 79.24 o 14 0 0 1552.34 1284.43 169.40 o 2 1 0 93292.40 95563.55 1107.48 o 3 1 0 23162.26 22540.31 251.42 o 4 1 0 292.74 315.88 12.33 o 5 1 0 198.26 190.97 16.25 o 6 1 0 12946.76 12838.17 189.05 o 7 1 0 21389.84 21764.48 333.36 o 8 1 0 2797.74 2818.11 109.82 o 9 1 0 641.07 629.06 44.29 o 10 1 0 2546.34 2422.87 82.66 o 11 1 0 2091.02 2162.55 82.53 o 12 1 0 516.66 482.52 114.37 o 13 1 0 130.01 187.11 70.45 o 14 1 0 141.23 118.26 91.48 o 1 2 0 57121.91 56837.33 2341.88 o 2 2 0 17007.92 17429.49 211.85 o 3 2 0 6241.71 6179.00 104.71 o 4 2 0 879.49 1016.57 21.03 o 5 2 0 42911.85 42313.71 554.34 o 6 2 0 1622.41 1645.43 68.11 o 7 2 0 51.71 104.49 27.39 o 8 2 0 1187.48 1165.58 45.15 o 9 2 0 16905.60 17337.07 284.08 o 10 2 0 972.57 859.74 88.33 o 11 2 0 214.57 227.71 50.16 o 12 2 0 6.42 85.48 70.15 o 13 2 0 1830.74 1692.54 175.83 o 14 2 0 12.90 -99.71 99.71 o 1 3 0 9077.95 9111.35 115.07 o 2 3 0 48949.02 48600.30 559.88 o 3 3 0 16792.83 16514.60 182.58 o 4 3 0 3457.71 3350.97 46.20 o 5 3 0 375.27 350.46 66.28 o 6 3 0 9383.61 8972.03 144.74 o 7 3 0 5278.05 5474.59 105.59 o 8 3 0 7709.40 7721.04 143.71 o 9 3 0 69.40 111.97 31.62 o 10 3 0 2338.16 2257.21 69.50 o 11 3 0 2795.73 2656.13 82.88 o 12 3 0 2408.21 2476.63 538.80 o 13 3 0 52.77 -27.29 54.05 o 14 3 0 210.98 -40.95 98.86 o 0 4 0 11300.59 11166.86 183.11 o 1 4 0 8319.03 8434.56 98.00 o 2 4 0 11104.99 11553.46 127.59 o 3 4 0 3129.09 3213.55 42.88 o 4 4 0 39546.42 39786.40 460.34 o 5 4 0 710.80 647.01 27.39 o 6 4 0 3769.38 3724.50 61.00 o 7 4 0 148.13 167.14 77.66 o 8 4 0 8366.75 8433.00 134.79 o 9 4 0 249.01 326.54 101.65 o 10 4 0 3841.53 3988.60 89.44 o 11 4 0 318.99 269.77 44.77 o 12 4 0 1880.50 1667.33 94.04 o 13 4 0 9.24 58.94 65.86 o 14 4 0 1026.61 849.37 134.74 o 1 5 0 1403.96 1655.13 72.02 o 2 5 0 22537.43 22014.88 403.41 o 3 5 0 8713.01 8141.57 100.04 o 4 5 0 63.39 74.06 10.28 o 5 5 0 3045.45 3042.52 53.41 o 6 5 0 5718.62 5754.90 84.16 o 7 5 0 11214.00 11067.30 156.85 o 8 5 0 1359.15 1376.15 44.72 o 9 5 0 270.98 220.08 30.16 o 10 5 0 645.40 754.60 44.56 o 11 5 0 3970.62 4189.72 229.58 o 12 5 0 807.61 731.35 106.50 o 13 5 0 34.48 129.59 72.45 o 14 5 0 90.22 179.31 98.86 o 0 6 0 8114.69 8442.14 139.06 o 1 6 0 21305.14 21144.93 316.39 o 2 6 0 25.81 49.40 14.54 o 3 6 0 4431.76 4497.69 55.43 o 4 6 0 14087.52 14536.74 213.84 o 5 6 0 23135.67 22901.63 294.28 o 6 6 0 632.09 599.28 23.11 o 7 6 0 670.30 748.58 51.86 o 8 6 0 792.36 791.61 37.03 o 9 6 0 4831.51 5035.18 104.05 o 10 6 0 392.45 399.81 54.76 o 11 6 0 6.07 -8.93 44.91 o 12 6 0 817.90 715.43 66.16 o 13 6 0 2663.09 2577.34 123.85 o 14 6 0 419.20 246.68 157.75 o 1 7 0 165.87 159.01 11.15 o 2 7 0 52816.21 53019.93 635.40 o 3 7 0 11540.00 11852.04 128.89 o 4 7 0 1432.48 1278.71 27.06 o 5 7 0 260.16 271.30 16.62 o 6 7 0 21256.37 21068.81 300.19 o 7 7 0 7120.51 6891.88 113.94 o 8 7 0 4612.40 4433.42 131.19 o 9 7 0 29.74 34.50 74.15 o 10 7 0 2796.46 2836.31 79.14 o 11 7 0 664.38 667.39 115.23 o 12 7 0 2143.41 2158.84 106.88 o 13 7 0 454.04 365.63 78.99 o 0 8 0 86484.06 88170.16 1379.16 o 1 8 0 16679.84 16695.73 319.15 o 2 8 0 4363.21 4598.81 54.18 o 3 8 0 9123.92 9045.25 106.08 o 4 8 0 25056.77 24972.61 325.43 o 5 8 0 5292.65 5131.83 98.74 o 6 8 0 6275.55 6138.55 96.41 o 7 8 0 2212.19 2222.03 48.91 o 8 8 0 5000.92 5043.73 95.58 o 9 8 0 648.81 663.02 83.85 o 10 8 0 4550.45 4576.91 121.74 o 11 8 0 659.41 690.94 69.06 o 12 8 0 358.16 335.47 71.42 o 13 8 0 845.87 693.34 111.86 o 1 9 0 55353.11 57337.86 845.82 o 2 9 0 12026.18 12415.56 135.81 o 3 9 0 78412.10 80201.00 925.06 o 4 9 0 481.78 466.77 19.14 o 5 9 0 5403.40 5182.64 81.72 o 6 9 0 36.60 76.38 19.70 o 7 9 0 19262.43 19276.60 292.26 o 8 9 0 19.47 99.29 31.58 o 9 9 0 33.82 -13.44 35.89 o 10 9 0 98.44 107.90 96.92 o 11 9 0 4043.10 3995.05 170.38 o 12 9 0 241.84 295.11 71.23 o 13 9 0 228.09 243.44 199.06 o 0 10 0 26008.18 26659.19 447.56 o 1 10 0 31486.72 31491.62 354.27 o 2 10 0 1674.41 1563.12 24.29 o 3 10 0 6643.69 6317.76 80.12 o 4 10 0 9224.04 9098.20 132.48 o 5 10 0 35192.83 35841.62 562.00 o 6 10 0 3526.45 3362.59 68.32 o 7 10 0 975.91 925.47 40.13 o 8 10 0 3198.95 3029.17 92.00 o 9 10 0 9176.81 9353.77 321.36 o 10 10 0 2472.16 2526.62 97.97 o 11 10 0 685.13 789.72 113.29 o 12 10 0 348.26 243.08 75.39 o 13 10 0 442.82 556.13 113.72 o 1 11 0 6.20 15.17 8.06 o 2 11 0 53604.18 53661.42 653.86 o 3 11 0 3343.34 3532.75 49.73 o 4 11 0 13503.48 13610.50 193.16 o 5 11 0 46.64 39.57 17.57 o 6 11 0 15200.45 15379.06 228.94 o 7 11 0 733.88 895.63 73.43 o 8 11 0 12440.34 12316.28 262.49 o 9 11 0 22.93 104.23 52.70 o 10 11 0 3282.87 3432.58 137.94 o 11 11 0 32.25 104.33 111.46 o 12 11 0 3205.36 3111.07 184.37 o 13 11 0 138.58 101.72 126.00 o 0 12 0 19879.81 19690.32 320.82 o 1 12 0 17840.36 17511.39 217.28 o 2 12 0 849.14 841.75 17.88 o 3 12 0 8048.42 8063.62 155.00 o 4 12 0 14176.10 14336.95 224.19 o 5 12 0 7607.93 7679.61 130.32 o 6 12 0 3587.68 3760.66 75.65 o 7 12 0 414.61 347.08 31.06 o 8 12 0 2822.50 2722.04 117.45 o 9 12 0 4433.88 4333.99 245.49 o 10 12 0 2692.51 2792.89 113.52 o 11 12 0 156.02 114.99 70.27 o 12 12 0 789.12 793.24 106.53 o 13 12 0 193.22 388.84 104.68 o 1 13 0 22477.28 21863.99 314.98 o 2 13 0 15.29 44.34 9.37 o 3 13 0 25696.25 25141.44 407.01 o 4 13 0 123.26 127.46 14.90 o 5 13 0 10150.23 10211.49 162.63 o 6 13 0 404.21 469.91 24.66 o 7 13 0 14079.86 14416.82 234.31 o 8 13 0 119.99 158.19 43.13 o 9 13 0 243.01 198.21 50.28 o 10 13 0 66.15 -23.67 88.32 o 11 13 0 2424.33 2374.77 171.12 o 12 13 0 1.76 140.95 88.32 o 13 13 0 319.42 82.14 152.41 o 0 14 0 8318.34 8367.29 141.72 o 1 14 0 7477.01 7313.76 88.70 o 2 14 0 616.27 640.29 24.84 o 3 14 0 5390.85 5242.50 121.29 o 4 14 0 4792.83 4805.92 105.98 o 5 14 0 13320.52 13330.66 207.44 o 6 14 0 3007.16 2909.60 74.80 o 7 14 0 1207.21 1256.64 84.94 o 8 14 0 2357.04 2365.20 89.80 o 9 14 0 2455.56 2803.25 100.10 o 10 14 0 1563.51 1597.34 81.98 o 11 14 0 12.47 -18.45 80.57 o 12 14 0 477.73 449.48 135.72 o 1 15 0 496.42 556.06 17.12 o 2 15 0 11867.53 12317.60 174.52 o 3 15 0 38.04 117.45 49.79 o 4 15 0 1855.46 1912.45 99.01 o 5 15 0 9.16 7.73 17.93 o 6 15 0 3868.50 4124.78 108.01 o 7 15 0 354.12 358.64 40.95 o 8 15 0 1981.58 2040.06 84.72 o 9 15 0 35.41 32.98 59.49 o 10 15 0 1880.19 2000.55 135.35 o 11 15 0 162.56 8.22 90.05 o 12 15 0 2149.69 2221.31 172.21 o 0 16 0 1305.97 1379.59 39.83 o 1 16 0 7391.96 7626.97 100.78 o 2 16 0 93.44 99.73 20.72 o 3 16 0 6632.44 6822.92 121.79 o 4 16 0 2499.12 2591.22 72.17 o 5 16 0 9352.82 9285.36 198.15 o 6 16 0 1841.65 1811.91 65.43 o 7 16 0 1046.80 968.88 62.04 o 8 16 0 559.75 574.49 50.66 o 9 16 0 2987.57 2921.59 104.79 o 10 16 0 2343.25 2449.82 129.16 o 11 16 0 52.99 51.67 146.07 o 12 16 0 120.39 224.14 101.21 o 1 17 0 11089.49 11290.99 149.91 o 2 17 0 2729.34 2779.94 65.21 o 3 17 0 22312.04 22839.97 435.04 o 4 17 0 41.05 76.80 60.33 o 5 17 0 2030.56 2056.55 80.43 o 6 17 0 2510.38 2428.80 101.20 o 7 17 0 7139.04 7174.28 192.27 o 8 17 0 523.42 383.54 95.11 o 9 17 0 86.27 170.31 173.37 o 10 17 0 750.88 598.00 100.01 o 11 17 0 2656.89 2417.59 156.89 o 12 17 0 2.26 -92.43 92.43 o 0 18 0 14197.79 14478.28 246.00 o 1 18 0 5689.63 5722.88 82.38 o 2 18 0 418.17 421.66 18.38 o 3 18 0 417.54 359.29 20.47 o 4 18 0 14936.38 15670.53 353.84 o 5 18 0 3088.08 3133.31 95.86 o 6 18 0 1816.44 1820.79 108.22 o 7 18 0 2.15 90.44 71.24 o 8 18 0 4617.79 4773.28 341.49 o 9 18 0 728.47 718.07 144.67 o 10 18 0 1151.61 1029.04 126.74 o 11 18 0 327.14 287.94 97.70 o 1 19 0 1153.24 1192.34 30.98 o 2 19 0 20549.65 20742.98 288.29 o 3 19 0 1959.11 2095.60 237.78 o 4 19 0 2217.85 2397.88 71.87 o 5 19 0 657.21 667.10 38.45 o 6 19 0 10440.20 10745.90 300.28 o 7 19 0 882.59 878.99 85.54 o 8 19 0 4707.10 5171.10 199.39 o 9 19 0 216.28 295.43 83.49 o 10 19 0 874.02 708.72 102.65 o 11 19 0 678.97 525.49 109.83 o 0 20 0 6633.66 6465.24 144.96 o 1 20 0 15782.76 16007.23 227.74 o 2 20 0 508.34 510.58 74.88 o 3 20 0 3855.17 3955.23 90.80 o 4 20 0 1355.34 1460.63 51.73 o 5 20 0 16551.57 16677.05 411.77 o 6 20 0 2282.41 2416.19 86.44 o 7 20 0 375.78 301.13 68.17 o 8 20 0 159.31 174.33 125.15 o 9 20 0 6035.36 6264.80 269.18 o 10 20 0 1042.35 1041.40 107.84 o 11 20 0 100.04 63.04 105.65 o 1 21 0 8914.62 8982.23 156.89 o 2 21 0 4684.55 5019.29 105.36 o 3 21 0 15329.16 15691.81 289.27 o 4 21 0 74.83 132.95 57.64 o 5 21 0 1432.47 1469.71 94.02 o 6 21 0 2705.57 2946.83 126.18 o 7 21 0 9466.06 9853.16 362.57 o 8 21 0 107.84 116.00 95.02 o 9 21 0 2.27 -82.73 82.73 o 10 21 0 109.55 16.69 158.71 o 0 22 0 20552.32 21266.96 546.39 o 1 22 0 1517.81 1547.22 54.29 o 2 22 0 364.65 388.48 34.72 o 3 22 0 1029.49 990.89 108.93 o 4 22 0 12268.54 12974.43 291.66 o 5 22 0 2074.32 1966.90 147.24 o 6 22 0 2498.52 2455.31 146.28 o 7 22 0 406.62 242.29 150.84 o 8 22 0 3360.00 3134.43 165.20 o 9 22 0 305.81 348.82 91.14 o 10 22 0 1139.04 946.49 183.81 o 1 23 0 2097.24 2182.85 69.08 o 2 23 0 11076.62 10897.20 226.19 o 3 23 0 2864.02 2991.95 123.87 o 4 23 0 1035.22 1022.33 68.54 o 5 23 0 28.35 -68.36 68.36 o 6 23 0 2755.64 2670.59 120.04 o 7 23 0 1870.00 1967.08 158.87 o 8 23 0 1023.96 831.59 100.71 o 9 23 0 49.09 -40.10 142.84 o 0 24 0 186.26 229.95 43.37 o 1 24 0 4832.59 4732.00 121.96 o 2 24 0 21.64 110.98 34.16 o 3 24 0 1018.39 907.55 112.69 o 4 24 0 13.14 200.87 68.33 o 5 24 0 4928.68 5690.50 245.13 o 6 24 0 31.56 -106.86 106.86 o 7 24 0 25.16 19.14 132.30 o 8 24 0 3.27 84.81 147.80 o 9 24 0 3003.29 2938.22 288.20 o 1 25 0 524.65 593.68 40.71 o 2 25 0 4980.72 5282.36 200.52 o 3 25 0 1639.81 1516.42 95.73 o 4 25 0 196.08 347.96 66.15 o 5 25 0 183.86 262.18 73.42 o 6 25 0 2283.82 2399.48 120.46 o 7 25 0 2037.74 2146.12 214.49 o 8 25 0 25.36 -38.53 106.13 o 0 26 0 11287.33 11165.04 385.11 o 1 26 0 4.91 84.81 31.74 o 2 26 0 154.18 184.64 58.88 o 3 26 0 43.48 9.69 60.33 o 4 26 0 5993.13 6633.73 256.79 o 5 26 0 23.00 -17.20 65.42 o 6 26 0 254.40 237.46 80.45 o 7 26 0 76.11 26.65 155.08 o 8 26 0 2151.94 2136.92 254.97 o 1 27 0 1114.13 1232.05 72.46 o 2 27 0 2821.15 2596.49 130.41 o 3 27 0 1253.66 1388.62 102.75 o 4 27 0 71.63 80.20 92.56 o 5 27 0 804.26 725.04 95.48 o 6 27 0 1103.98 1242.45 142.25 o 7 27 0 1606.57 1629.55 150.98 o 0 28 0 30.86 123.82 63.48 o 1 28 0 2994.22 3078.65 114.65 o 2 28 0 137.40 173.98 75.36 o 3 28 0 1239.73 1173.90 97.91 o 4 28 0 69.17 67.60 72.93 o 5 28 0 4982.17 5281.95 250.45 o 6 28 0 97.35 108.80 101.77 o 7 28 0 15.24 31.50 120.91 o 1 29 0 808.32 675.61 69.06 o 2 29 0 4466.41 4751.72 196.86 o 3 29 0 1806.68 1653.59 112.21 o 4 29 0 240.35 179.31 80.45 o 5 29 0 94.78 98.86 92.08 o 6 29 0 3802.22 3352.52 359.25 o 0 30 0 10963.59 10955.82 639.31 o 1 30 0 276.34 92.08 147.33 o 2 30 0 88.77 82.14 70.51 o 3 30 0 712.29 872.36 113.41 o 4 30 0 7548.72 7359.40 388.75 o 5 30 0 64.15 330.02 148.53 o 1 31 0 2639.80 2733.54 293.52 o 2 31 0 3226.75 2318.50 251.36 o 3 31 0 3571.64 2895.75 206.77 o 4 31 0 343.61 372.43 148.30 o -13 0 1 1401.36 1726.22 147.35 o -11 0 1 923.43 1039.61 69.79 o -9 0 1 1832.43 1826.04 84.10 o -7 0 1 29361.91 29599.54 594.42 o -5 0 1 298.66 263.89 19.14 o -3 0 1 134359.97 134175.78 2522.27 o -1 0 1 956.51 968.82 21.35 o 1 0 1 169968.75 124906.36 8168.91 o 3 0 1 21673.15 21067.77 373.21 o 5 0 1 79395.42 80048.51 1350.91 o 7 0 1 20571.71 20263.08 421.37 o 9 0 1 5032.05 5070.34 154.23 o 11 0 1 5925.64 6356.31 259.23 o 13 0 1 10.69 142.96 109.52 o -14 1 1 899.90 620.90 151.09 o -13 1 1 309.16 417.13 68.32 o -12 1 1 17.66 -30.16 59.36 o -11 1 1 380.52 432.43 47.90 o -10 1 1 4933.71 4972.84 103.47 o -9 1 1 4012.01 4091.83 179.90 o -8 1 1 466.82 396.47 31.82 o -7 1 1 2260.14 2318.13 58.67 o -6 1 1 17296.04 16821.15 243.76 o -5 1 1 29783.04 29140.46 351.75 o -4 1 1 3034.88 2924.32 39.43 o -3 1 1 877.95 1033.61 17.91 o -2 1 1 10387.04 10105.66 125.79 o -1 1 1 87165.74 84819.95 1816.42 o 1 1 1 88.71 163.81 7.11 o 2 1 1 1444.40 1470.83 22.68 o 3 1 1 49778.99 50027.02 566.43 o 4 1 1 46932.50 46693.81 522.69 o 5 1 1 10300.52 9717.36 136.89 o 6 1 1 1300.42 1270.50 39.67 o 7 1 1 5447.52 5429.67 105.18 o 8 1 1 8205.22 8355.97 305.86 o 9 1 1 2530.13 2799.53 69.65 o 10 1 1 1253.19 1378.65 92.09 o 11 1 1 236.22 250.45 81.42 o 12 1 1 3262.88 3321.19 238.89 o 13 1 1 740.89 768.23 86.15 o 14 1 1 611.42 408.05 214.45 o -14 2 1 9.87 -14.06 79.03 o -13 2 1 173.42 374.01 153.02 o -12 2 1 4770.60 4944.89 235.18 o -11 2 1 183.95 182.19 41.00 o -10 2 1 356.65 292.27 44.77 o -9 2 1 1079.27 931.57 96.94 o -8 2 1 18126.19 18469.59 293.73 o -7 2 1 326.82 407.11 31.95 o -6 2 1 6956.02 6807.78 114.48 o -5 2 1 2216.82 2115.10 38.48 o -4 2 1 39220.39 38902.70 433.83 o -3 2 1 3127.02 3543.92 46.95 o -2 2 1 75163.92 76500.74 839.74 o -1 2 1 77.40 135.86 5.09 o 1 2 1 1216.51 1225.08 23.09 o 2 2 1 103610.97 106017.25 1256.60 o 3 2 1 13.10 34.17 13.45 o 4 2 1 2436.53 2632.91 39.35 o 5 2 1 101.95 92.30 15.02 o 6 2 1 31619.14 31713.57 1022.20 o 7 2 1 2406.62 2487.55 60.63 o 8 2 1 1042.23 1140.40 61.07 o 9 2 1 705.92 712.32 42.72 o 10 2 1 9333.74 9694.89 202.14 o 11 2 1 555.06 523.06 46.82 o 12 2 1 1816.48 1740.73 94.52 o 13 2 1 30.05 -11.24 298.03 o 14 2 1 1426.94 1062.03 315.89 o -14 3 1 897.30 821.65 109.99 o -13 3 1 186.49 144.27 69.42 o -12 3 1 161.91 176.03 112.43 o -11 3 1 3582.02 3708.58 176.97 o -10 3 1 7796.07 8117.67 161.95 o -9 3 1 6213.54 6383.20 120.90 o -8 3 1 726.86 719.28 34.20 o -7 3 1 7612.67 7551.71 116.99 o -6 3 1 8021.34 7931.95 149.04 o -5 3 1 22900.43 22204.21 275.79 o -4 3 1 7753.34 7961.93 96.24 o -3 3 1 7192.47 7264.94 94.56 o -2 3 1 4058.37 4105.17 51.20 o -1 3 1 6034.16 5828.41 66.49 o 0 3 1 8768.34 8695.32 110.21 o 1 3 1 6777.62 6707.96 82.66 o 2 3 1 1902.74 1963.94 39.17 o 3 3 1 16422.61 16136.17 185.68 o 4 3 1 11365.94 11276.69 145.87 o 5 3 1 8419.22 8219.19 258.86 o 6 3 1 97.65 149.82 26.90 o 7 3 1 5706.60 5331.09 99.09 o 8 3 1 7501.60 7519.12 149.69 o 9 3 1 3480.91 3638.12 92.40 o 10 3 1 156.38 275.31 87.47 o 11 3 1 1487.29 1573.83 95.49 o 12 3 1 1413.58 1533.74 172.31 o 13 3 1 1656.70 1405.35 90.04 o 14 3 1 50.05 -38.53 113.64 o -14 4 1 0.85 106.86 108.79 o -13 4 1 1662.77 1609.25 170.37 o -12 4 1 12.25 99.63 52.76 o -11 4 1 3376.78 3472.06 89.17 o -10 4 1 12.45 18.73 32.87 o -9 4 1 1834.00 1874.98 58.31 o -8 4 1 1976.74 1989.42 55.60 o -7 4 1 19143.79 18874.23 687.40 o -6 4 1 69.73 149.11 24.47 o -5 4 1 194.42 235.82 14.34 o -4 4 1 9641.43 9963.19 121.63 o -3 4 1 79783.92 80430.35 867.43 o -2 4 1 17805.56 18403.02 202.45 o -1 4 1 2643.52 2786.23 38.96 o 0 4 1 53.76 90.03 6.91 o 1 4 1 17855.14 17579.64 203.49 o 2 4 1 20523.36 21447.82 259.94 o 3 4 1 8102.77 7953.84 101.23 o 4 4 1 3275.80 3492.66 51.33 o 5 4 1 12867.92 12485.68 174.13 o 6 4 1 703.09 720.08 61.31 o 7 4 1 2705.61 2687.02 64.68 o 8 4 1 197.70 227.23 27.38 o 9 4 1 5260.68 5204.71 100.77 o 10 4 1 685.71 721.64 46.96 o 11 4 1 2043.89 2130.76 71.37 o 12 4 1 78.38 31.19 57.12 o 13 4 1 337.12 346.07 61.79 o 14 4 1 5.33 123.82 118.24 o -14 5 1 1475.64 1249.28 139.11 o -13 5 1 324.72 379.73 115.46 o -12 5 1 72.21 14.83 54.30 o -11 5 1 295.31 272.47 50.72 o -10 5 1 9872.29 9869.51 187.90 o -9 5 1 1032.53 947.36 40.50 o -8 5 1 4121.88 4061.52 82.94 o -7 5 1 391.12 362.69 25.24 o -6 5 1 13678.62 13333.67 176.84 o -5 5 1 17328.18 17181.63 252.60 o -4 5 1 18342.61 18425.20 207.80 o -3 5 1 560.73 603.57 16.84 o -2 5 1 5798.89 5582.04 66.69 o -1 5 1 34377.11 34742.63 751.41 o 0 5 1 64338.91 65682.56 790.33 o 1 5 1 7324.78 7631.99 90.74 o 2 5 1 2887.76 2896.06 66.23 o 3 5 1 1921.84 1565.39 26.10 o 4 5 1 10717.76 9957.90 134.54 o 5 5 1 1247.69 1240.34 34.54 o 6 5 1 513.96 558.70 23.41 o 7 5 1 7723.60 7620.06 315.45 o 8 5 1 4309.43 4280.02 88.02 o 9 5 1 535.56 551.52 67.49 o 10 5 1 272.37 286.28 39.54 o 11 5 1 325.61 329.57 44.46 o 12 5 1 2026.23 2081.88 158.87 o 13 5 1 427.36 301.89 120.67 o 14 5 1 57.36 150.23 201.60 o -14 6 1 23.08 53.06 94.01 o -13 6 1 108.04 62.34 165.74 o -12 6 1 4208.91 4104.29 165.14 o -11 6 1 546.94 594.98 62.30 o -10 6 1 131.52 140.00 36.98 o -9 6 1 367.50 333.06 88.20 o -8 6 1 20949.88 21247.48 304.04 o -7 6 1 2789.30 2851.28 58.13 o -6 6 1 2210.01 2246.35 74.42 o -5 6 1 1669.20 1812.12 34.10 o -4 6 1 9083.90 8194.69 109.20 o -3 6 1 5746.65 5972.66 64.63 o -2 6 1 15077.40 15324.56 268.40 o -1 6 1 1675.03 1762.47 26.92 o 0 6 1 274.63 317.32 13.93 o 1 6 1 13668.74 14107.21 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