# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ; Dinitrato[5,16-dimethyl-2,6,13,17- tetraazatricyclo(14,4,0^1,18^,0^7,12^)docosane]copper(II) tetrahydrate ; _shelx_refln_list_code 4 _shelx_F_calc_maximum 113.79 _exptl_crystal_F_000 319.00 _reflns_d_resolution_high 0.7706 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.8129 _cell_length_b 8.7456 _cell_length_c 10.7152 _cell_angle_alpha 93.058 _cell_angle_beta 106.864 _cell_angle_gamma 108.435 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 188.25 340.31 2.60 o 3 0 0 130.55 96.52 2.20 o 4 0 0 2010.28 2193.47 38.40 o 5 0 0 1653.08 1767.71 29.23 o 6 0 0 183.93 179.85 2.71 o 7 0 0 81.51 78.58 2.74 o 8 0 0 136.22 143.46 3.87 o 9 0 0 64.00 56.65 6.50 o -9 1 0 93.45 96.32 3.03 o -8 1 0 236.43 257.17 3.78 o -7 1 0 171.87 180.17 2.64 o -6 1 0 74.31 67.93 1.85 o -5 1 0 60.29 64.10 1.08 o -4 1 0 797.01 812.75 7.69 o -3 1 0 1442.75 1368.75 13.52 o -2 1 0 780.44 1086.11 7.95 o -1 1 0 3182.96 3140.62 26.61 o 1 1 0 168.91 250.10 2.31 o 2 1 0 775.95 932.49 8.41 o 3 1 0 92.51 105.91 2.75 o 4 1 0 7.61 5.80 0.77 o 5 1 0 227.74 261.83 4.31 o 6 1 0 382.99 370.88 8.35 o 7 1 0 379.89 354.19 5.11 o 8 1 0 62.01 51.95 3.03 o -9 2 0 35.37 33.56 1.78 o -8 2 0 139.36 131.05 2.26 o -7 2 0 223.06 207.70 2.66 o -6 2 0 358.55 336.58 4.82 o -5 2 0 70.23 79.74 1.22 o -4 2 0 176.80 227.94 2.38 o -3 2 0 527.81 743.90 7.40 o -2 2 0 2405.40 3265.35 29.60 o -1 2 0 12919.28 15791.06 388.37 o 0 2 0 330.27 255.89 2.85 o 1 2 0 253.74 307.72 2.87 o 2 2 0 1039.73 997.38 10.03 o 3 2 0 1998.17 1932.65 22.41 o 4 2 0 1346.17 1384.61 16.24 o 5 2 0 146.54 169.40 2.56 o 6 2 0 118.95 121.85 2.47 o 7 2 0 190.93 195.62 7.29 o 8 2 0 120.24 121.96 4.41 o -9 3 0 25.63 26.44 1.68 o -8 3 0 115.69 125.70 2.01 o -7 3 0 266.36 279.94 5.83 o -6 3 0 19.62 23.22 1.41 o -5 3 0 57.38 52.84 0.95 o -4 3 0 279.25 256.47 2.45 o -3 3 0 384.53 323.34 2.70 o -2 3 0 4466.26 4548.72 55.08 o -1 3 0 569.97 368.45 3.10 o 0 3 0 1682.83 1386.29 14.00 o 1 3 0 237.99 170.72 2.15 o 2 3 0 157.32 141.86 1.79 o 3 3 0 459.55 445.07 9.19 o 4 3 0 1521.39 1635.94 19.71 o 5 3 0 347.53 375.16 4.75 o 6 3 0 140.76 138.39 4.41 o 7 3 0 16.22 14.14 4.29 o -9 4 0 110.81 115.43 1.91 o -8 4 0 279.40 297.90 3.64 o -7 4 0 78.31 86.06 1.97 o -6 4 0 1.01 1.23 0.66 o -5 4 0 407.68 406.64 3.06 o -4 4 0 810.24 807.75 6.58 o -3 4 0 782.63 862.65 6.93 o -2 4 0 152.70 188.77 2.23 o -1 4 0 124.44 130.17 4.55 o 0 4 0 1537.74 1704.22 20.31 o 1 4 0 231.58 253.15 6.05 o 2 4 0 5.51 3.51 1.07 o 3 4 0 582.48 582.42 7.12 o 4 4 0 323.02 309.25 4.04 o 5 4 0 403.59 390.80 12.06 o 6 4 0 31.92 28.87 4.95 o 7 4 0 55.60 53.33 2.67 o -9 5 0 47.32 45.14 2.93 o -8 5 0 190.84 152.72 11.44 o -7 5 0 5.58 2.83 1.85 o -6 5 0 28.37 26.05 1.58 o -5 5 0 51.77 53.36 1.18 o -4 5 0 374.61 406.41 4.10 o -3 5 0 1460.12 1691.86 16.36 o -2 5 0 18.51 15.71 1.45 o -1 5 0 55.91 66.26 2.34 o 0 5 0 174.47 161.68 3.38 o 1 5 0 649.34 675.25 7.79 o 2 5 0 866.79 922.34 11.78 o 3 5 0 579.55 590.95 7.90 o 4 5 0 147.76 153.46 3.58 o 5 5 0 118.74 128.61 4.74 o 6 5 0 49.92 57.52 4.46 o -9 6 0 110.68 99.60 2.40 o -8 6 0 47.53 41.26 3.80 o -7 6 0 10.66 9.09 2.03 o -6 6 0 328.95 363.85 3.46 o -5 6 0 324.18 345.84 3.43 o -4 6 0 207.14 228.36 2.74 o -3 6 0 59.25 55.57 1.24 o -2 6 0 231.87 224.52 2.76 o -1 6 0 335.78 332.60 7.95 o 0 6 0 93.08 76.82 2.84 o 1 6 0 17.19 17.28 1.67 o 2 6 0 515.11 528.96 7.39 o 3 6 0 176.85 182.99 3.44 o 4 6 0 335.17 343.63 9.11 o 5 6 0 3.76 2.26 3.17 o -9 7 0 45.94 50.97 2.81 o -8 7 0 0.86 -0.04 1.13 o -7 7 0 115.65 122.91 2.18 o -6 7 0 5.33 6.66 1.28 o -5 7 0 85.62 92.54 2.06 o -4 7 0 592.70 609.43 5.56 o -3 7 0 288.08 272.38 3.11 o -2 7 0 32.42 37.80 1.53 o -1 7 0 23.70 17.91 2.32 o 0 7 0 242.68 236.62 3.54 o 1 7 0 611.09 589.09 15.24 o 2 7 0 155.84 142.69 3.78 o 3 7 0 140.89 140.64 4.12 o 4 7 0 22.92 18.00 3.80 o 5 7 0 64.31 65.12 3.96 o -8 8 0 34.52 27.45 4.08 o -7 8 0 218.51 214.03 3.16 o -6 8 0 65.00 58.34 1.78 o -5 8 0 3.06 3.64 1.15 o -4 8 0 1.04 0.56 1.27 o -3 8 0 34.37 43.30 1.64 o -2 8 0 91.06 85.71 4.26 o -1 8 0 29.84 32.00 1.81 o 0 8 0 22.07 20.66 3.06 o 1 8 0 175.29 168.77 3.67 o 2 8 0 89.00 95.49 3.32 o 3 8 0 91.05 88.44 5.44 o 4 8 0 11.37 10.83 3.01 o -8 9 0 45.70 46.62 1.79 o -7 9 0 38.59 46.49 1.95 o -6 9 0 91.40 96.63 2.70 o -5 9 0 145.58 143.52 2.45 o -4 9 0 33.66 38.56 1.82 o -3 9 0 13.44 13.68 1.59 o -2 9 0 19.96 20.63 3.11 o -1 9 0 81.27 86.71 2.77 o 0 9 0 357.56 344.23 5.72 o 1 9 0 153.47 159.45 6.83 o 2 9 0 84.45 89.10 4.26 o -7 10 0 24.86 25.90 2.15 o -6 10 0 12.71 12.93 2.28 o -5 10 0 11.63 12.12 2.02 o -4 10 0 0.80 2.23 1.36 o -3 10 0 36.10 32.32 1.86 o -2 10 0 3.46 3.84 3.09 o -1 10 0 6.61 4.16 3.92 o 0 10 0 70.41 71.37 3.88 o 1 10 0 133.62 120.98 4.13 o -5 11 0 4.82 3.78 2.13 o -4 11 0 46.82 38.34 2.41 o -3 11 0 44.22 41.33 2.23 o -2 11 0 16.98 13.22 2.35 o 1 -11 1 10.42 10.44 2.87 o 2 -11 1 8.72 9.62 2.07 o 3 -11 1 22.42 28.67 2.32 o 4 -11 1 22.55 29.91 2.35 o 5 -11 1 114.19 110.52 3.80 o -1 -10 1 109.22 109.11 5.30 o 0 -10 1 35.51 44.85 3.34 o 1 -10 1 10.24 12.28 2.06 o 2 -10 1 29.59 32.77 2.11 o 3 -10 1 19.45 25.45 1.71 o 4 -10 1 212.27 214.16 3.79 o 5 -10 1 69.08 67.37 2.25 o 6 -10 1 0.88 0.26 1.37 o 7 -10 1 2.45 0.74 2.13 o -3 -9 1 2.09 0.53 2.16 o -2 -9 1 6.64 3.48 2.58 o -1 -9 1 50.29 45.02 2.62 o 0 -9 1 28.43 19.73 2.47 o 1 -9 1 153.97 134.12 5.18 o 2 -9 1 0.95 0.76 1.15 o 3 -9 1 20.87 18.82 2.39 o 4 -9 1 152.35 135.37 2.63 o 5 -9 1 89.38 75.17 1.84 o 6 -9 1 61.48 52.69 1.68 o 7 -9 1 0.60 0.98 1.13 o -4 -8 1 1.68 1.45 2.13 o -3 -8 1 232.29 235.63 5.00 o -2 -8 1 166.50 165.59 5.97 o -1 -8 1 59.84 49.87 2.82 o 0 -8 1 10.71 11.39 1.63 o 1 -8 1 463.61 469.92 7.61 o 2 -8 1 204.71 219.88 5.34 o 3 -8 1 57.34 64.41 1.79 o 4 -8 1 20.61 16.56 1.49 o 5 -8 1 30.78 34.50 1.49 o 6 -8 1 65.94 68.95 1.83 o 7 -8 1 170.81 185.11 2.59 o 8 -8 1 21.74 33.06 5.47 o -5 -7 1 20.70 16.97 2.51 o -4 -7 1 105.37 118.47 9.99 o -3 -7 1 125.27 131.19 3.35 o -2 -7 1 86.57 92.60 3.20 o -1 -7 1 39.96 42.94 2.30 o 0 -7 1 381.19 358.77 6.29 o 1 -7 1 22.40 20.58 1.35 o 2 -7 1 30.28 28.91 3.46 o 3 -7 1 374.29 384.56 3.64 o 4 -7 1 320.03 312.72 3.36 o 5 -7 1 20.73 17.19 1.53 o 6 -7 1 13.00 14.93 1.18 o 7 -7 1 44.85 44.10 2.09 o 8 -7 1 211.99 201.69 3.30 o -6 -6 1 12.34 10.88 2.85 o -5 -6 1 29.61 35.53 2.46 o -4 -6 1 264.24 265.12 4.59 o -3 -6 1 309.80 304.73 4.57 o -2 -6 1 68.81 65.53 2.80 o -1 -6 1 50.37 54.82 2.24 o 0 -6 1 337.00 341.91 3.96 o 1 -6 1 170.05 191.88 7.15 o 2 -6 1 18.01 15.66 0.94 o 3 -6 1 125.95 140.71 1.78 o 4 -6 1 155.76 138.62 2.50 o 5 -6 1 263.13 254.01 2.69 o 6 -6 1 75.50 71.57 1.75 o 7 -6 1 40.93 39.48 1.85 o 8 -6 1 10.38 11.67 1.69 o 9 -6 1 152.14 157.72 2.77 o -6 -5 1 3.43 3.45 2.23 o -5 -5 1 136.29 142.76 3.87 o -4 -5 1 153.55 150.35 3.00 o -3 -5 1 183.99 179.05 2.96 o -2 -5 1 250.12 221.71 3.61 o -1 -5 1 647.75 630.93 6.60 o 0 -5 1 318.34 288.37 3.33 o 1 -5 1 483.76 442.38 4.69 o 2 -5 1 355.19 322.97 3.00 o 3 -5 1 189.16 157.83 1.66 o 4 -5 1 336.81 344.78 3.31 o 5 -5 1 355.13 373.98 3.96 o 6 -5 1 115.97 136.24 3.25 o 7 -5 1 106.64 118.47 2.96 o 8 -5 1 55.67 62.85 1.74 o 9 -5 1 55.17 58.87 1.94 o -7 -4 1 25.19 21.44 2.25 o -6 -4 1 210.25 223.43 4.11 o -5 -4 1 79.06 96.80 3.47 o -4 -4 1 370.50 402.94 8.21 o -3 -4 1 7.41 8.49 1.33 o -2 -4 1 381.30 344.35 7.96 o -1 -4 1 164.82 135.78 1.78 o 0 -4 1 425.07 394.35 4.58 o 1 -4 1 114.63 101.84 1.51 o 2 -4 1 24.83 46.64 1.43 o 3 -4 1 25.83 21.33 0.58 o 4 -4 1 130.49 150.27 1.91 o 5 -4 1 58.23 56.75 1.19 o 6 -4 1 1.54 2.08 0.76 o 7 -4 1 71.62 62.65 1.84 o 8 -4 1 208.76 213.38 2.95 o 9 -4 1 13.82 15.90 1.26 o -8 -3 1 38.42 37.54 3.52 o -7 -3 1 71.94 70.89 3.62 o -6 -3 1 176.76 177.18 4.96 o -5 -3 1 554.33 564.31 7.51 o -4 -3 1 428.34 459.16 5.24 o -3 -3 1 358.58 357.90 4.34 o -2 -3 1 214.43 226.46 2.42 o -1 -3 1 731.87 904.21 9.03 o 0 -3 1 501.15 663.15 12.87 o 1 -3 1 425.33 657.71 5.11 o 2 -3 1 29.18 66.22 1.25 o 3 -3 1 608.06 729.04 4.66 o 4 -3 1 548.68 546.03 4.66 o 5 -3 1 67.80 67.28 1.14 o 6 -3 1 78.21 65.03 1.50 o 7 -3 1 136.96 134.29 2.06 o 8 -3 1 74.48 79.56 2.40 o 9 -3 1 10.29 5.18 1.70 o -8 -2 1 158.22 148.43 4.94 o -7 -2 1 143.09 129.65 6.38 o -6 -2 1 1.06 0.28 1.63 o -5 -2 1 192.78 207.92 3.38 o -4 -2 1 426.26 488.78 6.85 o -3 -2 1 1589.20 1674.63 19.39 o -2 -2 1 38.52 20.27 2.19 o -1 -2 1 144.35 230.44 3.43 o 0 -2 1 183.40 95.26 1.52 o 1 -2 1 1756.70 1443.73 9.86 o 2 -2 1 964.95 742.94 4.68 o 3 -2 1 32.45 10.13 0.59 o 4 -2 1 133.71 108.11 1.21 o 5 -2 1 412.49 440.92 5.37 o 6 -2 1 242.64 260.39 2.70 o 7 -2 1 73.97 83.71 1.73 o 8 -2 1 71.15 60.90 1.57 o 9 -2 1 121.67 122.86 3.36 o -8 -1 1 114.18 123.62 2.49 o -7 -1 1 440.07 459.32 8.31 o -6 -1 1 861.32 920.56 17.66 o -5 -1 1 105.66 106.31 2.58 o -4 -1 1 199.45 194.78 2.61 o -3 -1 1 1974.24 1914.55 34.13 o -2 -1 1 9305.25 9800.67 197.68 o -1 -1 1 408.03 309.51 18.23 o 1 -1 1 43.46 34.82 0.71 o 2 -1 1 1867.53 2073.80 20.19 o 3 -1 1 904.63 1017.08 9.51 o 4 -1 1 150.91 167.78 1.89 o 5 -1 1 61.75 65.45 1.38 o 6 -1 1 121.15 124.44 2.16 o 7 -1 1 15.13 10.03 1.17 o 8 -1 1 16.13 10.26 1.04 o 9 -1 1 137.16 122.17 2.71 o -9 0 1 76.12 78.32 4.27 o -8 0 1 21.96 18.58 4.54 o -7 0 1 67.02 72.69 2.43 o -6 0 1 696.48 683.55 8.86 o -5 0 1 1033.26 1008.44 15.05 o -4 0 1 453.03 525.81 6.99 o -3 0 1 50.84 37.39 1.18 o -2 0 1 722.16 642.55 7.58 o 1 0 1 380.76 606.27 4.40 o 2 0 1 1092.27 1071.61 9.61 o 3 0 1 287.72 333.80 2.97 o 4 0 1 1124.18 1093.71 15.19 o 5 0 1 495.86 506.19 5.39 o 6 0 1 43.29 43.71 1.56 o 7 0 1 25.13 22.39 1.58 o 8 0 1 274.23 247.54 17.08 o -9 1 1 85.01 76.45 2.28 o -8 1 1 159.54 159.18 2.57 o -7 1 1 269.91 292.52 3.36 o -6 1 1 132.82 127.14 1.67 o -5 1 1 395.70 420.55 3.37 o -4 1 1 1538.12 1795.29 15.98 o -3 1 1 2207.06 2484.45 29.37 o -2 1 1 49.38 27.65 0.36 o -1 1 1 1188.77 952.69 8.24 o 0 1 1 350.89 197.27 1.56 o 1 1 1 3750.27 3404.24 43.89 o 2 1 1 3324.53 3240.83 41.69 o 3 1 1 226.35 198.89 2.43 o 4 1 1 1.41 4.57 0.72 o 5 1 1 225.12 264.63 4.92 o 6 1 1 135.60 159.86 3.45 o 7 1 1 139.78 150.10 2.65 o 8 1 1 27.71 34.38 2.58 o -9 2 1 58.75 62.70 1.51 o -8 2 1 148.86 166.49 2.95 o -7 2 1 575.21 620.48 5.98 o -6 2 1 344.77 360.01 5.64 o -5 2 1 207.73 185.60 2.37 o -4 2 1 655.09 596.38 4.07 o -3 2 1 1735.66 1620.89 16.71 o -2 2 1 12947.24 14135.62 271.21 o -1 2 1 83.15 52.91 1.34 o 0 2 1 7.94 6.48 0.68 o 1 2 1 911.76 918.56 11.74 o 2 2 1 5786.09 6700.69 116.60 o 3 2 1 396.15 389.01 4.11 o 4 2 1 126.17 109.32 4.41 o 5 2 1 80.32 83.51 2.07 o 6 2 1 75.38 74.23 1.98 o 7 2 1 219.89 197.41 7.14 o 8 2 1 29.64 24.62 2.73 o -9 3 1 23.75 23.64 1.43 o -8 3 1 153.70 150.63 1.88 o -7 3 1 474.57 480.61 5.84 o -6 3 1 382.71 390.85 4.10 o -5 3 1 11.85 9.34 0.55 o -4 3 1 118.42 159.11 1.50 o -3 3 1 1575.97 1966.33 20.69 o -2 3 1 2630.89 3266.59 43.50 o -1 3 1 36.57 24.56 0.91 o 0 3 1 116.68 119.55 3.20 o 1 3 1 1832.71 2175.29 25.59 o 2 3 1 128.03 185.36 2.97 o 3 3 1 41.32 38.98 1.44 o 4 3 1 185.08 176.56 2.95 o 5 3 1 234.37 243.92 4.64 o 6 3 1 138.18 144.73 3.87 o 7 3 1 6.30 8.02 3.93 o -9 4 1 55.88 48.22 1.43 o -8 4 1 187.20 178.96 2.47 o -7 4 1 90.00 93.64 1.57 o -6 4 1 466.55 507.26 6.15 o -5 4 1 510.08 534.66 5.06 o -4 4 1 330.17 408.59 11.05 o -3 4 1 2323.86 2672.20 27.40 o -2 4 1 182.96 165.18 1.88 o -1 4 1 1986.73 2036.38 27.50 o 0 4 1 3850.00 3858.06 56.27 o 1 4 1 2317.85 2313.26 28.68 o 2 4 1 9.54 6.35 1.16 o 3 4 1 230.42 238.79 3.13 o 4 4 1 523.46 531.22 7.09 o 5 4 1 358.96 363.99 5.77 o 6 4 1 162.04 173.35 5.66 o 7 4 1 18.28 21.57 2.67 o -9 5 1 105.89 113.25 3.10 o -8 5 1 104.29 116.24 5.25 o -7 5 1 155.95 178.93 4.82 o -6 5 1 53.83 53.74 1.23 o -5 5 1 10.67 10.26 1.17 o -4 5 1 1965.23 2119.91 21.10 o -3 5 1 764.38 762.63 8.25 o -2 5 1 13.99 5.56 0.85 o -1 5 1 6.84 10.47 0.95 o 0 5 1 1067.52 1182.91 13.78 o 1 5 1 395.80 406.88 5.89 o 2 5 1 357.46 401.04 5.39 o 3 5 1 11.81 11.78 1.40 o 4 5 1 72.70 74.61 3.71 o 5 5 1 165.39 159.89 4.50 o 6 5 1 142.98 145.05 5.78 o -9 6 1 57.67 63.42 3.13 o -8 6 1 9.42 8.84 1.98 o -7 6 1 256.08 249.70 3.74 o -6 6 1 312.00 300.18 3.72 o -5 6 1 293.49 338.22 3.76 o -4 6 1 340.19 386.11 10.62 o -3 6 1 191.21 171.17 2.80 o -2 6 1 1066.10 1110.85 13.12 o -1 6 1 594.54 655.97 7.20 o 0 6 1 53.20 46.49 1.57 o 1 6 1 211.30 181.11 2.95 o 2 6 1 441.82 425.51 6.30 o 3 6 1 359.13 353.31 5.18 o 4 6 1 81.56 82.66 5.20 o 5 6 1 183.63 197.23 4.35 o -9 7 1 0.64 1.23 2.04 o -8 7 1 62.10 53.48 3.31 o -7 7 1 72.09 64.79 2.78 o -6 7 1 25.76 28.16 1.21 o -5 7 1 195.48 236.17 3.28 o -4 7 1 92.16 99.96 3.41 o -3 7 1 377.31 366.90 4.52 o -2 7 1 204.61 213.41 4.68 o -1 7 1 139.05 175.59 2.95 o 0 7 1 103.58 121.67 3.09 o 1 7 1 467.68 481.88 6.43 o 2 7 1 103.41 106.96 3.42 o 3 7 1 59.53 59.29 4.22 o 4 7 1 142.84 157.95 4.82 o -8 8 1 140.45 148.60 2.85 o -7 8 1 222.34 216.72 19.75 o -6 8 1 138.20 169.47 3.05 o -5 8 1 29.55 36.89 1.80 o -4 8 1 52.28 50.02 2.01 o -3 8 1 361.29 365.61 5.01 o -2 8 1 338.13 330.18 7.06 o -1 8 1 43.82 48.89 3.40 o 0 8 1 214.39 205.42 6.84 o 1 8 1 89.97 88.84 4.65 o 2 8 1 182.96 165.79 3.96 o 3 8 1 35.04 35.97 2.68 o -8 9 1 21.08 17.54 2.55 o -7 9 1 15.62 16.66 1.99 o -6 9 1 49.34 55.47 2.04 o -5 9 1 103.23 88.23 2.06 o -4 9 1 127.10 120.54 2.64 o -3 9 1 42.02 36.71 2.15 o -2 9 1 9.74 10.91 1.80 o -1 9 1 119.45 111.81 4.96 o 0 9 1 239.96 224.08 5.39 o 1 9 1 153.36 142.67 3.90 o 2 9 1 21.39 17.75 3.11 o -7 10 1 5.98 6.89 1.65 o -6 10 1 70.47 68.35 2.43 o -5 10 1 27.06 29.84 1.78 o -4 10 1 40.74 38.62 4.38 o -3 10 1 55.48 59.36 2.67 o -2 10 1 50.42 55.72 2.75 o -1 10 1 51.70 58.10 2.97 o 0 10 1 15.33 15.84 3.05 o -5 11 1 26.93 30.79 2.09 o -4 11 1 21.60 16.54 5.29 o -3 11 1 34.62 38.92 2.82 o -2 11 1 77.58 72.39 3.44 o 1 -11 2 39.81 39.86 8.91 o 2 -11 2 39.52 37.04 2.47 o 3 -11 2 6.31 5.21 1.62 o 4 -11 2 238.99 219.06 5.00 o -1 -10 2 87.31 81.37 4.12 o 0 -10 2 6.22 3.74 2.34 o 1 -10 2 4.21 4.41 1.73 o 2 -10 2 26.63 26.67 2.01 o 3 -10 2 259.15 245.56 4.61 o 4 -10 2 480.60 461.80 5.97 o 5 -10 2 7.65 11.62 1.62 o 6 -10 2 3.00 4.38 1.40 o -3 -9 2 1.09 2.49 3.84 o -2 -9 2 57.76 64.71 3.12 o -1 -9 2 23.30 28.58 6.97 o 0 -9 2 92.05 105.62 3.53 o 1 -9 2 41.56 47.98 4.16 o 2 -9 2 0.86 2.31 1.29 o 3 -9 2 282.07 287.43 4.45 o 4 -9 2 61.18 74.19 2.43 o 5 -9 2 97.28 106.29 3.16 o 6 -9 2 18.02 17.85 1.52 o 7 -9 2 26.69 29.51 1.46 o -4 -8 2 53.10 57.81 3.23 o -3 -8 2 335.79 330.66 7.00 o -2 -8 2 60.37 62.16 3.04 o -1 -8 2 61.34 54.76 2.28 o 0 -8 2 40.32 43.99 2.37 o 1 -8 2 488.79 473.13 6.69 o 2 -8 2 1046.86 1011.61 10.42 o 3 -8 2 71.15 63.20 1.72 o 4 -8 2 64.06 63.54 1.86 o 5 -8 2 53.41 47.52 1.56 o 6 -8 2 463.43 438.85 5.51 o 7 -8 2 108.40 95.25 3.14 o 8 -8 2 28.71 27.67 1.71 o -5 -7 2 8.57 6.22 2.74 o -4 -7 2 7.05 4.79 2.40 o -3 -7 2 175.15 169.56 4.39 o -2 -7 2 1.29 1.57 1.45 o -1 -7 2 59.18 63.83 3.08 o 0 -7 2 7.29 6.95 1.24 o 1 -7 2 2.24 2.53 1.02 o 2 -7 2 532.37 536.55 5.64 o 3 -7 2 202.79 201.09 3.49 o 4 -7 2 56.77 60.45 1.72 o 5 -7 2 25.62 22.48 2.18 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56.87 4.02 o 5 -3 9 218.04 235.02 7.53 o -8 -2 9 29.65 34.17 4.94 o -7 -2 9 95.90 102.26 3.38 o -6 -2 9 115.73 113.56 3.62 o -5 -2 9 44.17 48.54 2.19 o -4 -2 9 5.17 8.07 1.49 o -3 -2 9 15.50 19.58 0.95 o -2 -2 9 887.89 935.53 9.59 o -1 -2 9 284.33 305.15 3.54 o 0 -2 9 11.17 3.14 0.41 o 1 -2 9 1.70 5.28 3.38 o 2 -2 9 266.86 262.36 6.04 o 3 -2 9 287.62 299.81 7.12 o 4 -2 9 185.65 191.54 6.20 o 5 -2 9 0.60 0.82 2.89 o -8 -1 9 56.94 69.46 3.90 o -7 -1 9 94.54 101.63 3.89 o -6 -1 9 113.31 115.96 2.93 o -5 -1 9 299.02 314.53 6.14 o -4 -1 9 2.18 3.03 1.11 o -3 -1 9 457.06 439.36 6.71 o -2 -1 9 191.94 186.94 2.97 o -1 -1 9 234.33 234.99 2.35 o 0 -1 9 224.79 265.43 2.16 o 1 -1 9 482.65 445.28 8.10 o 2 -1 9 59.20 62.50 5.32 o 3 -1 9 39.97 39.07 5.51 o 4 -1 9 259.17 237.89 10.59 o 5 -1 9 90.49 84.07 5.04 o -8 0 9 59.24 56.64 7.64 o -7 0 9 113.10 113.28 13.02 o -6 0 9 78.97 80.97 4.09 o -5 0 9 50.13 48.46 1.86 o -4 0 9 83.09 85.43 1.43 o -3 0 9 424.96 465.80 5.16 o -2 0 9 5.64 6.11 0.98 o -1 0 9 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o -4 3 12 234.39 232.28 3.54 o -3 3 12 33.76 34.89 2.83 o -2 3 12 109.99 96.28 2.44 o -1 3 12 43.91 39.92 1.91 o -6 4 12 91.82 86.23 4.60 o -5 4 12 267.28 246.03 4.50 o -4 4 12 196.53 171.24 6.74 o -3 4 12 84.10 80.38 2.62 o -2 4 12 49.34 46.08 2.22 o -5 5 12 316.34 306.07 6.28 o -4 5 12 49.39 50.71 2.98 o -3 5 12 19.36 15.88 4.63 o -3 -4 13 17.25 8.36 2.21 o -2 -4 13 1.72 0.00 1.92 o -1 -4 13 156.45 147.30 7.52 o -4 -3 13 91.74 80.95 3.63 o -3 -3 13 0.87 0.99 1.26 o -2 -3 13 63.59 61.34 3.14 o -1 -3 13 44.91 44.90 3.19 o 0 -3 13 22.61 24.08 3.16 o -5 -2 13 19.30 16.61 2.20 o -4 -2 13 33.65 36.67 2.16 o -3 -2 13 47.98 50.29 1.53 o -2 -2 13 77.32 87.32 3.59 o -1 -2 13 4.01 5.12 3.89 o 0 -2 13 1.72 1.50 2.50 o -5 -1 13 56.48 54.29 2.23 o -4 -1 13 53.85 42.93 2.23 o -3 -1 13 68.87 64.73 1.64 o -2 -1 13 8.08 3.60 0.97 o -1 -1 13 63.12 54.90 5.39 o 0 -1 13 40.75 38.91 3.51 o -6 0 13 66.78 61.42 3.62 o -5 0 13 64.11 58.69 2.77 o -4 0 13 27.30 24.00 2.47 o -3 0 13 4.97 5.97 1.32 o -2 0 13 9.32 7.61 1.33 o -1 0 13 13.98 13.32 2.68 o 0 0 13 77.02 84.12 6.98 o -6 1 13 122.36 126.68 3.44 o -5 1 13 113.65 120.35 5.32 o -4 1 13 50.41 58.52 1.80 o -3 1 13 30.23 38.07 2.73 o -2 1 13 79.53 83.22 2.37 o -1 1 13 48.31 56.56 3.52 o -6 2 13 44.57 38.55 3.58 o -5 2 13 0.72 2.05 2.28 o -4 2 13 34.19 27.63 3.35 o -3 2 13 104.91 96.84 2.37 o -2 2 13 45.27 42.15 2.39 o -5 3 13 20.92 14.54 2.87 o -4 3 13 73.17 78.50 3.60 o -3 3 13 124.71 120.85 4.31 o