# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' a in C 2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1425.54 _exptl_crystal_F_000 4160.00 _reflns_d_resolution_high 0.7828 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 22.0704 _cell_length_b 16.1036 _cell_length_c 23.4789 _cell_angle_alpha 90.000 _cell_angle_beta 109.700 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 84934.05 78656.93 2710.87 o 4 0 0 42216.66 41334.75 653.98 o 6 0 0 450617.84 418170.66 7862.20 o 8 0 0 4304.34 4453.07 175.12 o 10 0 0 95651.27 95158.64 6346.79 o 12 0 0 85787.35 77617.27 902.55 o 14 0 0 4113.49 4833.53 758.39 o 16 0 0 359.52 514.95 434.06 o 18 0 0 11.72 73.92 188.87 o 20 0 0 1136.69 1132.23 692.56 o 22 0 0 1269.07 1907.54 444.78 o 24 0 0 1017.49 1500.20 527.94 o 26 0 0 276.12 320.44 22.95 o 1 1 0 129745.91 128052.11 6699.82 o 3 1 0 174.18 427.47 804.56 o 5 1 0 18567.98 20006.20 278.84 o 7 1 0 17198.36 20924.93 703.56 o 9 1 0 11643.44 12040.93 1162.39 o 11 1 0 5673.34 6923.62 1091.69 o 13 1 0 49652.58 47927.30 480.20 o 15 1 0 3536.81 3947.74 482.49 o 17 1 0 7647.54 7515.68 476.31 o 19 1 0 2803.15 3949.97 585.60 o 21 1 0 3585.56 3475.27 330.54 o 23 1 0 1772.42 1515.34 340.64 o 25 1 0 213.62 234.05 177.66 o 0 2 0 6812.00 6637.90 194.43 o 2 2 0 1439.43 3242.99 574.17 o 4 2 0 277196.56 261005.13 1044.41 o 6 2 0 8339.93 11055.67 1133.93 o 8 2 0 64590.11 63048.51 822.21 o 10 2 0 86244.82 77263.70 231.45 o 12 2 0 6807.68 7870.78 700.55 o 14 2 0 115281.20 114350.89 1411.21 o 16 2 0 28337.09 28921.31 606.45 o 18 2 0 9358.85 11339.53 1078.84 o 20 2 0 15744.33 12886.44 2981.73 o 22 2 0 1302.02 1314.76 60.14 o 24 2 0 4208.64 3607.38 258.92 o 26 2 0 1878.11 2646.14 886.03 o 1 3 0 97500.34 89905.60 1118.78 o 3 3 0 592646.94 545135.56 781.67 o 5 3 0 2752.77 2695.60 263.57 o 7 3 0 30516.75 29871.30 474.93 o 9 3 0 92996.93 93158.94 1112.81 o 11 3 0 1154.73 947.25 510.04 o 13 3 0 12830.26 13844.17 240.36 o 15 3 0 4770.14 4681.31 147.36 o 17 3 0 6122.95 6014.65 560.16 o 19 3 0 215.76 287.54 73.28 o 21 3 0 261.83 422.71 449.58 o 23 3 0 1343.09 1315.43 142.26 o 25 3 0 188.15 457.56 490.42 o 0 4 0 48244.00 46704.51 531.39 o 2 4 0 37441.05 39885.79 825.96 o 4 4 0 202341.86 199653.38 451.27 o 6 4 0 149468.22 140025.69 2379.87 o 8 4 0 12698.36 14936.50 453.49 o 10 4 0 10573.27 10667.67 298.86 o 12 4 0 9769.97 8909.81 144.16 o 14 4 0 752.38 1767.79 528.45 o 16 4 0 810.18 726.18 553.86 o 18 4 0 5.61 38.65 84.93 o 20 4 0 680.22 811.74 293.99 o 22 4 0 1387.38 2180.66 546.87 o 24 4 0 768.39 805.27 99.16 o 26 4 0 20.00 84.47 1157.80 o 1 5 0 5138.99 5636.95 439.07 o 3 5 0 4419.16 4185.66 99.62 o 5 5 0 2382.73 2400.64 338.34 o 7 5 0 55075.78 51881.48 589.00 o 9 5 0 3022.34 3276.96 115.78 o 11 5 0 26208.44 25734.71 387.66 o 13 5 0 31795.38 29847.06 1396.98 o 15 5 0 5226.53 4543.43 315.39 o 17 5 0 22801.27 20753.49 230.46 o 19 5 0 3626.05 3551.97 265.35 o 21 5 0 2842.51 3596.13 566.40 o 23 5 0 7244.78 6969.44 518.30 o 25 5 0 268.28 849.30 1044.87 o 0 6 0 14832.87 15143.21 800.64 o 2 6 0 41984.27 42356.59 567.33 o 4 6 0 66926.38 61736.01 840.58 o 6 6 0 25327.98 24155.50 1955.22 o 8 6 0 19794.02 21361.31 1015.94 o 10 6 0 25189.63 25857.96 320.76 o 12 6 0 1405.15 2219.52 312.98 o 14 6 0 15477.61 14011.65 2397.32 o 16 6 0 18767.50 19771.73 719.84 o 18 6 0 4133.78 4861.14 683.31 o 20 6 0 8600.67 9045.28 588.58 o 22 6 0 2981.61 3052.23 166.65 o 24 6 0 1090.95 968.37 431.96 o 1 7 0 67820.17 62204.19 280.50 o 3 7 0 114724.25 108294.59 4966.79 o 5 7 0 49812.63 47527.51 1116.48 o 7 7 0 18268.11 20447.87 1114.19 o 9 7 0 62361.24 56810.16 531.69 o 11 7 0 8155.74 7627.71 595.43 o 13 7 0 18.33 129.87 366.10 o 15 7 0 84.07 187.93 541.56 o 17 7 0 1720.97 1546.41 224.90 o 19 7 0 744.88 1027.50 774.56 o 21 7 0 4.50 407.43 638.24 o 23 7 0 47.31 65.88 39.45 o 0 8 0 199590.44 188759.56 2258.68 o 2 8 0 11614.72 14381.14 1079.30 o 4 8 0 5048.52 6543.40 589.51 o 6 8 0 41250.15 40799.88 214.84 o 8 8 0 1055.79 2051.87 330.99 o 10 8 0 23008.95 23948.45 805.23 o 12 8 0 23811.97 23603.36 407.95 o 14 8 0 4684.42 3957.29 308.50 o 16 8 0 271.62 311.00 166.78 o 18 8 0 320.26 347.82 195.57 o 20 8 0 4000.35 3480.46 213.93 o 22 8 0 3.33 3.25 7.04 o 24 8 0 1983.89 1877.64 363.59 o 1 9 0 936.35 1085.27 665.64 o 3 9 0 4424.50 4518.78 363.13 o 5 9 0 25797.02 25135.20 1093.07 o 7 9 0 14981.00 14287.26 1643.97 o 9 9 0 8625.40 9408.94 667.86 o 11 9 0 51878.25 47781.42 461.95 o 13 9 0 16087.41 16856.46 517.38 o 15 9 0 7572.01 7382.58 673.93 o 17 9 0 10595.70 11049.40 2866.50 o 19 9 0 4059.97 4125.33 218.04 o 21 9 0 2225.12 2028.40 280.96 o 23 9 0 3388.89 3811.29 555.49 o 0 10 0 5846.41 7175.25 2049.33 o 2 10 0 36562.41 38597.34 720.76 o 4 10 0 5444.40 6224.08 2094.32 o 6 10 0 9356.12 8328.18 285.07 o 8 10 0 6138.41 7499.90 394.83 o 10 10 0 5318.37 5319.10 285.09 o 12 10 0 174.37 129.06 47.74 o 14 10 0 765.26 1477.45 308.03 o 16 10 0 9622.28 7396.24 536.69 o 18 10 0 614.44 1013.08 643.79 o 20 10 0 1055.32 2115.44 629.86 o 22 10 0 660.82 1010.04 497.43 o 1 11 0 11882.17 16499.95 693.73 o 3 11 0 130824.85 114493.41 729.02 o 5 11 0 2699.94 3207.03 688.40 o 7 11 0 6637.11 6410.02 750.43 o 9 11 0 37207.81 37824.40 820.04 o 11 11 0 41.98 163.96 369.44 o 13 11 0 2917.68 3570.63 608.18 o 15 11 0 2563.62 2816.43 275.34 o 17 11 0 44.11 94.01 362.70 o 19 11 0 259.72 366.19 323.19 o 21 11 0 51.20 210.79 565.75 o 0 12 0 2387.65 2628.79 652.42 o 2 12 0 935.99 844.73 63.81 o 4 12 0 180.42 806.41 659.33 o 6 12 0 4919.87 5014.91 569.05 o 8 12 0 942.02 782.62 153.05 o 10 12 0 7.93 196.21 129.94 o 12 12 0 793.48 737.70 481.89 o 14 12 0 542.64 1298.25 705.72 o 16 12 0 1433.42 2346.65 455.44 o 18 12 0 562.32 788.91 239.26 o 20 12 0 901.22 746.20 199.37 o 1 13 0 1492.33 1968.78 367.95 o 3 13 0 2607.25 3177.31 350.30 o 5 13 0 2759.48 3135.59 337.29 o 7 13 0 2940.19 2925.38 249.02 o 9 13 0 21.90 75.50 301.97 o 11 13 0 11479.75 12749.37 1034.77 o 13 13 0 6614.34 6510.06 487.85 o 15 13 0 144.39 309.00 289.89 o 17 13 0 4777.90 5274.40 391.92 o 19 13 0 2434.53 1895.89 169.86 o 0 14 0 17004.04 16731.62 308.06 o 2 14 0 1030.74 1085.23 900.72 o 4 14 0 4052.76 4089.89 252.11 o 6 14 0 1763.53 1632.77 363.13 o 8 14 0 7888.83 8278.85 695.85 o 10 14 0 1846.34 2155.17 604.16 o 12 14 0 11716.58 12523.28 2379.41 o 14 14 0 1023.59 923.86 132.67 o 16 14 0 126.96 472.43 458.31 o 18 14 0 904.21 1311.17 523.44 o 1 15 0 1895.28 2348.86 306.67 o 3 15 0 3973.03 5145.23 457.30 o 5 15 0 913.19 1008.86 206.59 o 7 15 0 210.30 533.96 489.97 o 9 15 0 2898.71 2687.50 600.94 o 11 15 0 2963.68 4416.32 669.18 o 13 15 0 472.54 445.42 146.45 o 15 15 0 36.55 223.36 465.22 o 17 15 0 152.40 678.52 909.90 o 0 16 0 126.94 577.91 668.07 o 2 16 0 6042.34 5762.44 438.88 o 4 16 0 293.07 511.57 204.20 o 6 16 0 3030.81 3480.42 634.94 o 8 16 0 1683.85 2266.76 620.33 o 10 16 0 211.26 189.34 596.05 o 12 16 0 414.01 887.44 473.93 o 14 16 0 3083.15 2700.79 244.69 o 16 16 0 127.34 181.80 519.68 o 1 17 0 89.58 202.00 287.61 o 3 17 0 1416.13 2617.38 704.39 o 5 17 0 232.04 417.61 479.08 o 7 17 0 195.44 341.38 408.49 o 9 17 0 3.52 65.73 251.11 o 11 17 0 163.72 140.27 267.18 o 13 17 0 1560.31 1676.87 604.22 o 0 18 0 1226.89 1730.90 626.49 o 2 18 0 506.99 521.10 51.42 o 4 18 0 1147.19 1770.24 780.30 o 6 18 0 1997.86 2417.28 396.19 o 8 18 0 2697.97 3049.73 566.86 o 10 18 0 2.47 62.93 665.62 o 12 18 0 599.16 943.87 1181.67 o 1 19 0 778.87 1047.14 268.85 o 3 19 0 531.99 563.94 276.09 o 5 19 0 98.38 181.17 307.31 o 7 19 0 301.91 483.66 183.97 o 9 19 0 65.42 86.31 1157.80 o 0 20 0 2206.94 3487.17 1168.82 o 2 20 0 74.52 668.42 1037.52 o 4 20 0 55.77 166.19 519.68 o 6 20 0 1633.62 1582.91 558.24 o -25 1 1 861.74 1576.56 474.80 o -23 1 1 670.05 866.68 599.92 o -21 1 1 3124.07 3448.30 376.09 o -19 1 1 5254.74 5420.49 435.24 o -17 1 1 21.50 162.94 654.87 o -15 1 1 9282.33 9115.86 1669.68 o -13 1 1 58181.43 53468.20 704.23 o -11 1 1 10836.29 11355.65 583.49 o -9 1 1 7538.20 8353.54 309.88 o -7 1 1 37401.77 35941.16 1787.66 o -5 1 1 39.39 343.74 663.42 o -3 1 1 1074.31 2130.05 303.94 o -1 1 1 30243.27 28244.54 1090.78 o 1 1 1 105650.59 97260.01 842.87 o 3 1 1 6661.27 7833.37 710.86 o 5 1 1 16047.85 14479.08 488.92 o 7 1 1 9431.54 8972.52 413.63 o 9 1 1 78033.16 84032.55 5419.90 o 11 1 1 2505.15 3755.68 421.78 o 13 1 1 4524.43 4934.47 487.48 o 15 1 1 29736.36 29537.93 723.97 o 17 1 1 4602.75 4341.06 473.61 o 19 1 1 4494.61 5273.35 655.35 o 21 1 1 1073.22 1517.03 579.32 o 23 1 1 630.18 584.10 46.14 o 25 1 1 14.85 24.51 196.72 o -26 2 1 460.41 900.72 677.60 o -24 2 1 103.92 109.61 30.30 o -22 2 1 658.52 873.40 354.37 o -20 2 1 137.07 442.86 229.40 o -18 2 1 5.28 262.26 856.47 o -16 2 1 1565.15 2730.12 560.44 o -14 2 1 1030.86 1136.67 330.73 o -12 2 1 6647.94 6803.53 412.13 o -10 2 1 5732.40 5413.30 220.82 o -8 2 1 24715.91 25034.44 533.45 o -6 2 1 19429.81 22740.75 724.18 o -4 2 1 23645.23 24985.82 634.49 o -2 2 1 4584.56 4772.31 340.18 o 0 2 1 103369.73 105627.93 4686.75 o 2 2 1 33229.99 33256.76 864.91 o 4 2 1 30204.21 28758.80 1668.76 o 6 2 1 211.16 194.12 232.29 o 8 2 1 12510.03 14168.38 478.32 o 10 2 1 5312.06 6067.73 470.98 o 12 2 1 9082.74 8557.88 666.26 o 14 2 1 1449.07 1635.08 534.37 o 16 2 1 266.30 597.56 356.79 o 18 2 1 1112.83 1197.03 207.45 o 20 2 1 139.19 374.00 367.11 o 22 2 1 30.14 68.15 109.56 o 24 2 1 14.95 88.75 250.88 o 26 2 1 229.38 357.16 270.86 o -25 3 1 14.59 180.54 245.18 o -23 3 1 319.27 385.69 192.81 o -21 3 1 1724.94 2460.35 394.35 o -19 3 1 107.65 419.75 805.89 o -17 3 1 3547.85 3959.79 304.89 o -15 3 1 68.98 319.36 671.39 o -13 3 1 4764.35 5155.04 713.95 o -11 3 1 233.60 1072.38 586.23 o -9 3 1 3473.03 4154.53 546.77 o -7 3 1 11656.85 13379.76 394.94 o -5 3 1 520632.00 478578.84 4996.65 o -3 3 1 16.28 139.58 182.25 o -1 3 1 82607.10 79384.92 581.68 o 1 3 1 424477.41 392722.09 961.31 o 3 3 1 59.90 383.61 414.28 o 5 3 1 20721.73 21768.82 732.23 o 7 3 1 20101.33 20233.41 184.62 o 9 3 1 15.31 269.09 156.09 o 11 3 1 1974.51 2275.03 434.87 o 13 3 1 5368.21 5382.72 384.25 o 15 3 1 396.85 1074.78 445.93 o 17 3 1 589.41 879.03 260.33 o 19 3 1 667.34 697.83 158.84 o 21 3 1 101.13 120.31 169.71 o 23 3 1 350.38 415.22 92.28 o 25 3 1 42.29 105.73 178.79 o -26 4 1 53.44 31.22 270.86 o -24 4 1 36.26 72.42 207.01 o -22 4 1 2343.13 2562.63 163.43 o -20 4 1 2762.31 3200.41 576.61 o -18 4 1 3243.20 4478.83 570.20 o -16 4 1 9035.94 10013.62 874.09 o -14 4 1 2286.32 3293.19 575.30 o -12 4 1 1740.63 2020.15 592.67 o -10 4 1 18892.47 18379.05 336.97 o -8 4 1 5943.23 5156.20 322.73 o -6 4 1 14489.72 16545.44 752.93 o -4 4 1 32934.88 32449.08 579.29 o -2 4 1 6898.88 7119.84 127.73 o 0 4 1 1496.64 1808.50 360.84 o 2 4 1 7430.53 6866.97 239.12 o 4 4 1 7759.91 6739.32 436.59 o 6 4 1 17184.72 21095.68 503.17 o 8 4 1 808.84 1598.33 248.51 o 10 4 1 4976.66 5884.04 704.42 o 12 4 1 14110.84 13720.90 179.04 o 14 4 1 2371.36 2480.75 334.67 o 16 4 1 5931.02 5802.47 410.42 o 18 4 1 6670.22 5780.45 254.43 o 20 4 1 557.09 855.59 599.39 o 22 4 1 644.53 912.28 337.28 o 24 4 1 1440.64 1794.06 558.01 o -25 5 1 357.30 720.33 410.21 o -23 5 1 825.47 1410.65 703.69 o -21 5 1 551.89 805.32 435.05 o -19 5 1 2276.63 2221.28 313.64 o -17 5 1 5728.48 5533.05 546.31 o -15 5 1 3759.25 3313.65 369.56 o -13 5 1 14855.33 17171.94 467.05 o -11 5 1 13607.30 13019.73 1814.29 o -9 5 1 5952.34 6495.09 999.88 o -7 5 1 5255.71 6712.37 644.20 o -5 5 1 4847.18 4526.52 217.60 o -3 5 1 32051.47 31151.30 256.78 o -1 5 1 1139.91 1389.57 252.04 o 1 5 1 43749.64 42277.50 662.91 o 3 5 1 674.87 677.63 218.99 o 5 5 1 295.27 1101.28 585.79 o 7 5 1 1598.91 2575.08 459.09 o 9 5 1 23863.67 25305.65 587.56 o 11 5 1 10394.42 10040.90 634.95 o 13 5 1 14942.25 13552.17 2597.48 o 15 5 1 5058.42 5199.06 552.85 o 17 5 1 2059.01 2387.32 320.04 o 19 5 1 1261.51 2371.65 426.35 o 21 5 1 2392.15 2644.89 472.37 o 23 5 1 255.83 401.79 169.06 o 25 5 1 253.56 424.19 405.83 o -24 6 1 1187.31 1136.29 251.63 o -22 6 1 13.12 116.59 446.76 o -20 6 1 12.81 200.93 653.89 o -18 6 1 1.38 8.61 194.65 o -16 6 1 230.16 710.78 787.76 o -14 6 1 8443.84 8127.19 277.21 o -12 6 1 247.04 327.55 265.81 o -10 6 1 3444.27 5037.46 538.75 o -8 6 1 37736.55 39587.09 761.08 o -6 6 1 59753.98 57056.57 989.32 o -4 6 1 6501.28 6693.34 267.48 o -2 6 1 159851.33 148169.63 689.08 o 0 6 1 5000.52 5430.86 333.59 o 2 6 1 31025.32 31291.27 2714.08 o 4 6 1 60727.68 57841.40 208.00 o 6 6 1 2276.55 3337.83 480.66 o 8 6 1 3196.48 3347.27 477.44 o 10 6 1 28092.41 25900.25 777.68 o 12 6 1 58.79 197.60 384.46 o 14 6 1 551.38 850.26 379.65 o 16 6 1 5805.33 6605.79 354.85 o 18 6 1 302.00 678.67 399.43 o 20 6 1 85.04 286.62 140.60 o 22 6 1 1.87 119.42 510.67 o 24 6 1 6.30 1.30 12.85 o -25 7 1 19.09 16.53 1037.52 o -23 7 1 1112.04 1487.46 401.64 o -21 7 1 1624.94 2123.40 520.55 o -19 7 1 31.59 128.60 331.13 o -17 7 1 2573.32 3445.09 420.06 o -15 7 1 3417.64 3687.11 331.92 o -13 7 1 3.90 137.72 92.17 o -11 7 1 6179.76 6503.42 296.61 o -9 7 1 15574.82 15808.18 1082.05 o -7 7 1 21915.25 22652.38 766.66 o -5 7 1 4662.98 4536.25 287.38 o -3 7 1 36123.14 37844.30 507.28 o -1 7 1 4394.63 4692.22 488.46 o 1 7 1 14761.16 16934.83 724.92 o 3 7 1 30.52 172.73 147.62 o 5 7 1 11581.98 11681.80 1015.95 o 7 7 1 11529.98 13087.90 1009.52 o 9 7 1 504.80 531.62 56.50 o 11 7 1 93.49 155.28 114.70 o 13 7 1 148.34 474.04 638.38 o 15 7 1 318.03 623.76 127.77 o 17 7 1 4199.46 5279.47 717.82 o 19 7 1 510.82 712.32 132.22 o 21 7 1 354.28 587.76 285.19 o 23 7 1 628.22 993.11 530.24 o -24 8 1 195.42 490.30 654.65 o -22 8 1 5074.66 6061.30 710.64 o -20 8 1 6478.68 6406.30 384.25 o -18 8 1 2430.31 3239.11 632.86 o -16 8 1 15177.76 15600.59 782.73 o -14 8 1 15316.30 16135.00 668.86 o -12 8 1 15882.55 15807.10 107.51 o -10 8 1 19236.18 18303.82 556.86 o -8 8 1 4792.45 4356.95 291.98 o -6 8 1 915.22 1022.12 74.15 o -4 8 1 2490.97 2994.87 302.08 o -2 8 1 37062.20 32418.85 1925.38 o 0 8 1 8.72 120.06 179.21 o 2 8 1 1113.96 1373.05 221.04 o 4 8 1 1896.97 2813.43 855.87 o 6 8 1 3111.99 3988.40 425.11 o 8 8 1 9370.78 12126.77 1535.62 o 10 8 1 13949.58 14785.04 1307.92 o 12 8 1 14282.07 13261.46 673.01 o 14 8 1 10021.58 9529.21 809.36 o 16 8 1 10048.60 9648.50 1455.74 o 18 8 1 11773.29 11936.77 230.15 o 20 8 1 2530.85 2555.94 819.92 o 22 8 1 1770.57 2862.15 629.06 o 24 8 1 2083.24 2194.40 169.86 o -23 9 1 0.45 96.65 130.11 o -21 9 1 752.64 603.75 360.12 o -19 9 1 2293.92 2953.81 341.56 o -17 9 1 110.98 205.24 279.12 o -15 9 1 1733.37 1496.49 363.59 o -13 9 1 3033.84 2749.16 293.35 o -11 9 1 7214.95 10515.82 2440.47 o -9 9 1 21829.83 25704.35 2606.66 o -7 9 1 7815.66 7520.96 802.47 o -5 9 1 24359.73 22046.99 1762.87 o -3 9 1 10756.39 10837.11 1492.93 o -1 9 1 2856.23 2936.63 158.40 o 1 9 1 57501.88 53228.68 2178.34 o 3 9 1 7812.76 7858.09 467.34 o 5 9 1 14677.18 14521.19 255.25 o 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