# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 060511x in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 320.47 _exptl_crystal_F_000 1272.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.9641 _cell_length_b 13.0548 _cell_length_c 17.1280 _cell_angle_alpha 89.403 _cell_angle_beta 77.192 _cell_angle_gamma 86.657 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12.02 12.53 3.37 o 3 0 0 882.58 1011.79 44.77 o 4 0 0 104.29 108.94 16.64 o 5 0 0 167.27 188.96 22.41 o 6 0 0 9.89 -8.50 14.30 o 7 0 0 189.89 364.87 37.61 o 8 0 0 3422.92 3699.96 148.64 o 9 0 0 1480.50 1902.14 138.07 o 10 0 0 116.96 61.27 30.36 o 11 0 0 28.87 31.86 48.76 o 12 0 0 201.84 407.44 85.12 o 13 0 0 509.74 730.22 112.95 o 14 0 0 4.25 -24.43 51.06 o 15 0 0 10.38 -75.94 52.25 o -14 1 0 1.97 58.68 64.10 o -13 1 0 79.45 172.27 69.05 o -12 1 0 56.80 59.96 56.38 o -11 1 0 2968.54 2632.54 183.67 o -10 1 0 560.21 694.54 120.48 o -9 1 0 307.13 234.38 36.93 o -8 1 0 741.25 602.90 106.29 o -7 1 0 5080.03 5410.31 203.77 o -6 1 0 3434.93 4683.73 175.25 o -5 1 0 120.61 149.97 20.95 o -4 1 0 391.51 399.52 23.25 o -3 1 0 6937.13 6622.44 190.45 o -2 1 0 23898.63 24106.87 672.98 o -1 1 0 22.06 21.57 6.66 o 0 1 0 13.71 -9.62 6.41 o 1 1 0 1110.14 1080.56 41.35 o 2 1 0 25493.03 28774.41 972.90 o 3 1 0 2.35 1.24 9.28 o 4 1 0 443.83 505.24 29.30 o 5 1 0 414.76 469.48 29.36 o 6 1 0 5682.29 6020.50 220.10 o 8 1 0 105.61 183.28 30.53 o 9 1 0 23.39 139.48 44.12 o 10 1 0 458.01 901.33 94.35 o 11 1 0 2393.15 2736.20 126.89 o 12 1 0 27.72 18.73 53.08 o 13 1 0 113.00 203.95 73.00 o 14 1 0 0.36 3.49 58.86 o 15 1 0 202.48 357.67 94.95 o -14 2 0 2.61 -21.86 65.38 o -13 2 0 560.43 664.00 109.73 o -12 2 0 73.81 19.38 50.05 o -11 2 0 142.97 429.57 87.97 o -10 2 0 202.78 165.72 46.33 o -9 2 0 4484.69 3999.64 163.53 o -8 2 0 11.34 61.63 24.07 o -7 2 0 855.54 768.20 47.35 o -6 2 0 63.50 41.23 14.09 o -5 2 0 835.33 861.45 35.10 o -4 2 0 86.21 87.18 11.66 o -3 2 0 2634.98 2366.87 73.74 o -2 2 0 11777.64 10922.48 376.54 o -1 2 0 5382.27 4832.17 244.92 o 0 2 0 102698.59 91825.78 4441.41 o 1 2 0 2290.67 1915.59 102.95 o 2 2 0 12116.03 12372.41 424.13 o 3 2 0 5469.31 5653.36 201.00 o 4 2 0 30.39 37.72 13.63 o 5 2 0 169.88 153.17 28.05 o 6 2 0 3033.65 3335.96 131.49 o 7 2 0 230.04 288.15 59.37 o 8 2 0 4047.32 3408.48 139.14 o 10 2 0 14.84 49.01 30.61 o 11 2 0 1.51 31.90 31.56 o 12 2 0 344.35 369.06 81.17 o 13 2 0 634.75 878.61 123.69 o 14 2 0 47.33 33.06 56.75 o 15 2 0 1.07 -77.97 51.98 o -14 3 0 23.86 -1.38 60.70 o -13 3 0 165.31 76.58 61.07 o -12 3 0 21.34 -25.35 47.39 o -11 3 0 476.97 673.92 106.52 o -10 3 0 579.06 788.12 67.46 o -9 3 0 730.44 707.48 60.74 o -8 3 0 634.45 544.68 71.35 o -7 3 0 4888.07 4620.81 144.80 o -6 3 0 241.54 271.04 23.26 o -5 3 0 710.45 556.59 26.96 o -4 3 0 42.64 6.75 11.76 o -3 3 0 2823.82 2822.40 109.47 o -2 3 0 5965.37 5202.63 270.45 o -1 3 0 7513.96 7963.84 400.03 o 0 3 0 597.87 323.87 30.12 o 1 3 0 2822.76 3019.35 160.99 o 2 3 0 3490.75 3328.83 123.04 o 3 3 0 548.71 425.17 26.43 o 4 3 0 2615.39 2154.75 87.48 o 5 3 0 45.50 26.65 15.84 o 6 3 0 3228.49 3177.34 127.17 o 7 3 0 3.70 -22.20 18.42 o 8 3 0 532.12 440.45 43.39 o 9 3 0 601.85 697.88 53.46 o 10 3 0 1230.81 1097.69 66.70 o 11 3 0 42.93 49.82 32.61 o 12 3 0 24.57 41.96 51.06 o 13 3 0 46.75 90.63 66.21 o 14 3 0 1.44 10.19 56.84 o -14 4 0 22.08 -29.30 56.85 o -13 4 0 407.90 482.65 97.15 o -12 4 0 108.85 104.59 63.72 o -11 4 0 310.17 315.61 75.48 o -10 4 0 350.71 417.05 51.90 o -9 4 0 1581.92 1334.89 75.73 o -8 4 0 1.70 10.23 24.48 o -7 4 0 345.31 276.83 37.05 o -6 4 0 161.35 193.98 38.43 o -5 4 0 2850.57 2566.05 85.42 o -4 4 0 90.47 167.47 24.98 o -3 4 0 5490.79 4926.49 265.13 o -2 4 0 5.19 14.33 18.18 o -1 4 0 3192.62 2570.72 99.04 o 0 4 0 1719.13 1369.99 85.31 o 1 4 0 1336.58 1368.62 85.77 o 2 4 0 746.29 814.42 60.33 o 3 4 0 361.65 390.07 31.36 o 4 4 0 1358.21 1177.89 56.78 o 5 4 0 78.27 87.03 36.36 o 6 4 0 2493.27 2499.29 141.79 o 7 4 0 12.96 18.18 19.26 o 8 4 0 1345.32 1229.50 67.02 o 9 4 0 1768.86 1524.09 131.23 o 10 4 0 139.72 165.16 38.07 o 11 4 0 53.08 47.42 31.04 o 12 4 0 154.81 171.45 64.46 o 13 4 0 294.51 303.95 79.98 o 14 4 0 61.16 45.73 59.69 o -13 5 0 5.79 -53.26 51.79 o -12 5 0 92.70 51.70 66.67 o -11 5 0 500.92 670.06 107.07 o -10 5 0 15.49 -18.98 35.54 o -9 5 0 340.41 314.90 46.56 o -8 5 0 0.24 0.78 23.86 o -7 5 0 2290.03 1984.12 95.04 o -6 5 0 3.22 6.61 14.21 o -5 5 0 407.30 377.59 55.88 o -4 5 0 3214.14 3251.69 193.22 o -3 5 0 75.54 117.72 38.48 o -2 5 0 1459.43 1472.85 98.36 o -1 5 0 1289.51 1336.21 61.34 o 0 5 0 72.76 75.02 24.61 o 1 5 0 392.29 394.40 40.41 o 2 5 0 3577.93 3336.00 185.69 o 3 5 0 958.28 1076.49 54.44 o 4 5 0 24.89 -1.01 15.52 o 5 5 0 608.03 565.98 38.88 o 6 5 0 6058.51 5202.10 198.94 o 7 5 0 89.94 87.44 31.13 o 8 5 0 1209.05 1261.05 89.03 o 9 5 0 242.74 237.64 41.35 o 10 5 0 101.52 93.60 32.97 o 11 5 0 89.00 34.59 33.59 o 12 5 0 262.12 228.83 74.65 o 13 5 0 167.57 155.83 67.31 o 14 5 0 20.04 -39.86 45.55 o -13 6 0 173.58 146.65 79.06 o -12 6 0 22.66 -36.55 45.73 o -11 6 0 288.93 272.55 77.68 o -10 6 0 52.26 88.37 37.11 o -9 6 0 715.96 740.86 101.24 o -8 6 0 2.02 25.34 43.43 o -7 6 0 28.82 121.76 51.15 o -6 6 0 79.24 106.15 45.46 o -5 6 0 2645.99 2469.72 162.92 o -4 6 0 48.96 25.99 30.58 o -3 6 0 4386.84 3977.92 227.11 o -2 6 0 31.66 -11.14 25.71 o -1 6 0 263.30 221.77 30.20 o 0 6 0 3517.10 3520.58 200.38 o 1 6 0 541.35 562.17 63.91 o 2 6 0 1318.64 1089.16 80.17 o 3 6 0 7376.51 7568.93 276.34 o 4 6 0 393.31 336.46 37.73 o 5 6 0 0.11 -21.01 17.42 o 6 6 0 1223.83 1165.91 75.40 o 7 6 0 4.67 24.51 23.13 o 8 6 0 892.04 838.69 101.37 o 9 6 0 120.36 126.16 34.41 o 10 6 0 26.47 12.37 28.95 o 11 6 0 444.80 413.55 56.63 o 12 6 0 18.30 -40.68 43.62 o 13 6 0 113.55 148.12 65.65 o 14 6 0 75.02 137.56 69.60 o -13 7 0 38.14 101.65 77.22 o -12 7 0 8.15 -51.15 53.91 o -11 7 0 483.64 248.58 81.17 o -10 7 0 121.99 44.26 58.68 o -9 7 0 242.49 277.78 74.19 o -8 7 0 10.71 -13.68 40.41 o -7 7 0 932.83 932.49 112.50 o -6 7 0 9.96 -26.36 34.16 o -5 7 0 9.23 -4.96 35.90 o -4 7 0 220.12 287.15 60.05 o -3 7 0 121.41 31.47 24.52 o -2 7 0 157.67 149.65 30.40 o -1 7 0 821.43 818.64 73.46 o 0 7 0 484.00 560.06 69.79 o 1 7 0 395.09 488.80 64.00 o 2 7 0 3212.94 3367.77 197.17 o 3 7 0 278.14 414.58 43.35 o 4 7 0 875.19 704.00 47.42 o 5 7 0 45.94 74.06 26.37 o 6 7 0 1642.16 1403.40 74.68 o 7 7 0 7.16 -27.81 23.15 o 8 7 0 621.21 650.65 61.42 o 9 7 0 294.80 428.61 118.23 o 10 7 0 2.81 0.72 29.19 o 11 7 0 434.93 462.77 60.04 o 12 7 0 174.44 402.30 83.93 o 13 7 0 114.51 90.27 68.96 o -12 8 0 25.65 23.14 73.00 o -11 8 0 30.44 -37.01 63.45 o -10 8 0 44.02 66.12 62.63 o -9 8 0 11.74 4.32 53.90 o -8 8 0 22.05 -9.28 45.92 o -7 8 0 144.03 170.80 62.71 o -6 8 0 0.28 -16.62 40.77 o -5 8 0 820.14 808.63 99.45 o -4 8 0 14.12 3.77 35.35 o -3 8 0 1854.80 1624.70 84.14 o -2 8 0 46.84 1.64 24.49 o -1 8 0 2.09 -15.43 31.77 o 0 8 0 1725.02 1765.53 125.91 o 1 8 0 97.98 58.22 36.73 o 2 8 0 901.73 896.79 94.58 o 3 8 0 1764.49 1729.25 123.52 o 5 8 0 64.05 45.78 28.61 o 6 8 0 725.33 861.26 68.56 o 7 8 0 12.10 -18.39 25.77 o 8 8 0 614.35 737.61 66.54 o 9 8 0 40.58 -10.18 31.54 o 10 8 0 372.73 431.47 106.85 o 11 8 0 32.34 41.84 37.64 o 12 8 0 21.76 -7.07 55.10 o -11 9 0 98.40 14.69 61.43 o -10 9 0 20.60 -41.05 51.06 o -9 9 0 83.13 58.31 63.82 o -8 9 0 13.96 -20.30 49.87 o -7 9 0 459.12 494.22 91.18 o -6 9 0 20.33 48.67 50.96 o -5 9 0 208.15 214.78 63.27 o -4 9 0 34.19 17.49 32.69 o -3 9 0 297.33 580.56 59.86 o -2 9 0 1129.20 1075.02 98.17 o -1 9 0 1785.75 2039.56 147.12 o 1 9 0 725.95 835.91 98.99 o 2 9 0 2123.26 2128.09 147.49 o 3 9 0 713.53 1082.83 95.97 o 4 9 0 691.77 740.79 61.02 o 5 9 0 49.94 15.43 29.22 o 6 9 0 509.27 661.40 64.00 o 7 9 0 0.84 -4.73 31.53 o 8 9 0 439.91 587.40 65.54 o 9 9 0 175.01 257.74 88.34 o 10 9 0 51.17 69.90 41.23 o 11 9 0 149.32 118.30 45.59 o -10 10 0 0.09 -2.66 61.89 o -9 10 0 95.88 81.82 64.10 o -8 10 0 12.21 -38.11 53.72 o -7 10 0 123.13 19.19 55.10 o -6 10 0 30.82 -2.78 37.79 o -5 10 0 529.51 594.46 68.85 o -4 10 0 70.72 68.77 42.15 o -3 10 0 1032.26 1115.11 80.73 o -2 10 0 43.14 15.61 44.17 o -1 10 0 18.24 118.09 60.14 o 0 10 0 400.61 497.25 84.66 o 1 10 0 725.79 977.77 112.77 o 2 10 0 110.45 148.76 57.12 o 3 10 0 210.54 182.55 61.15 o 4 10 0 1244.46 1107.31 78.01 o 5 10 0 181.96 228.88 49.82 o 6 10 0 606.99 893.76 79.57 o 7 10 0 2.64 -13.26 33.65 o 8 10 0 87.57 94.99 41.69 o 9 10 0 47.00 93.64 41.22 o 10 10 0 136.10 173.28 69.97 o 11 10 0 28.10 39.30 60.51 o -9 11 0 2.97 -53.45 56.66 o -8 11 0 10.47 33.24 63.45 o -7 11 0 558.01 755.74 82.46 o -6 11 0 38.35 38.87 41.22 o -5 11 0 336.83 525.37 67.16 o -4 11 0 172.79 311.15 56.09 o -3 11 0 20.73 -10.65 46.84 o -2 11 0 335.40 417.45 86.41 o -1 11 0 521.73 480.90 94.12 o 0 11 0 139.04 151.52 65.10 o 1 11 0 9.75 -6.98 50.96 o 2 11 0 471.29 530.49 95.04 o 3 11 0 479.56 687.64 72.88 o 4 11 0 378.06 467.16 62.82 o 5 11 0 69.22 98.03 43.43 o 6 11 0 308.66 371.93 60.67 o 7 11 0 304.22 365.31 61.13 o 8 11 0 644.71 852.07 177.13 o 9 11 0 0.17 -17.63 52.25 o 10 11 0 0.35 -6.15 58.04 o -8 12 0 12.69 0.88 54.69 o -7 12 0 40.19 65.63 111.71 o -6 12 0 35.64 -15.05 49.45 o -5 12 0 374.16 461.87 66.92 o -4 12 0 0.89 1.93 52.16 o -3 12 0 1004.96 1271.73 150.15 o -2 12 0 137.43 110.28 74.19 o -1 12 0 11.81 -16.16 61.52 o 0 12 0 334.36 357.30 87.14 o 1 12 0 314.15 271.54 84.57 o 2 12 0 167.52 201.38 75.94 o 3 12 0 94.58 37.53 41.05 o 4 12 0 499.87 556.58 100.51 o 5 12 0 417.57 421.96 64.83 o 6 12 0 673.27 843.94 103.85 o 7 12 0 110.56 161.07 69.14 o 8 12 0 2.39 -18.83 61.34 o 9 12 0 67.66 63.55 66.21 o 10 12 0 52.73 7.25 65.47 o -7 13 0 100.16 143.30 56.02 o -6 13 0 38.78 64.66 47.26 o -5 13 0 200.46 323.78 94.31 o -4 13 0 1.74 -41.78 58.32 o -3 13 0 14.03 81.08 66.57 o -2 13 0 2.73 -12.86 59.51 o -1 13 0 525.45 677.32 122.77 o 0 13 0 188.28 260.43 89.90 o 1 13 0 97.63 102.02 73.18 o 2 13 0 19.05 23.51 67.40 o 3 13 0 100.71 157.88 52.75 o 4 13 0 52.65 -32.49 41.20 o 5 13 0 2.36 89.99 74.11 o 6 13 0 70.14 -33.34 64.55 o 7 13 0 48.13 95.96 74.10 o 8 13 0 279.94 347.75 99.45 o -5 14 0 20.57 59.87 70.34 o -4 14 0 3.10 61.80 68.23 o -3 14 0 349.24 500.19 119.01 o -2 14 0 72.27 -20.66 64.92 o -1 14 0 16.01 30.67 71.17 o 0 14 0 33.36 50.41 80.53 o 1 14 0 63.68 -11.48 65.93 o 2 14 0 37.93 23.88 73.00 o 3 14 0 108.31 67.98 57.76 o 4 14 0 85.96 100.37 79.43 o 5 14 0 159.63 52.25 79.16 o 6 14 0 49.87 70.34 76.31 o 7 14 0 0.67 4.32 66.21 o -3 15 0 15.59 -26.17 67.77 o -2 15 0 11.67 -27.18 76.21 o -1 15 0 186.16 195.59 96.69 o 0 15 0 0.73 -30.86 71.16 o 1 15 0 0.36 25.44 76.95 o 2 15 0 1.25 -20.75 66.75 o 3 15 0 35.38 -19.10 72.91 o 4 15 0 8.34 50.23 81.82 o -4 -15 1 80.15 232.42 104.32 o -3 -15 1 8.54 18.65 52.98 o -2 -15 1 15.30 12.86 83.10 o -1 -15 1 0.25 -97.25 73.93 o 0 -15 1 14.24 -4.68 71.26 o 1 -15 1 9.26 -65.93 67.58 o 2 -15 1 19.75 37.56 86.32 o 3 -15 1 3.92 27.55 81.18 o -7 -14 1 14.87 19.56 74.01 o -6 -14 1 76.35 111.29 87.23 o -5 -14 1 1.99 -43.07 67.21 o -4 -14 1 7.57 -48.93 44.50 o -3 -14 1 65.77 39.87 49.28 o -2 -14 1 157.18 302.38 101.38 o -1 -14 1 50.73 -25.99 63.54 o 0 -14 1 0.18 -74.19 63.82 o 1 -14 1 113.90 94.76 86.59 o 2 -14 1 9.20 52.53 81.82 o 3 -14 1 10.42 19.01 75.94 o 4 -14 1 22.08 -9.28 68.87 o 5 -14 1 0.90 -25.16 63.82 o -8 -13 1 0.32 -60.42 62.53 o -7 -13 1 97.01 132.88 77.96 o -6 -13 1 0.16 -15.28 42.07 o -5 -13 1 225.68 292.71 65.65 o -4 -13 1 222.04 214.33 70.16 o -3 -13 1 74.22 110.28 69.42 o -2 -13 1 40.65 4.96 69.05 o -1 -13 1 81.55 81.91 70.71 o 0 -13 1 151.39 171.17 79.15 o 1 -13 1 363.71 547.84 113.87 o 2 -13 1 87.24 41.41 67.95 o 3 -13 1 60.28 -30.21 64.00 o 4 -13 1 92.24 113.13 74.01 o 5 -13 1 37.54 -11.39 60.88 o 6 -13 1 6.28 -23.07 46.22 o 7 -13 1 19.35 -61.09 40.72 o -9 -12 1 0.96 66.02 69.24 o -8 -12 1 6.93 23.82 72.73 o -7 -12 1 219.03 380.02 76.12 o -6 -12 1 157.31 223.83 55.49 o -5 -12 1 2.39 -38.49 36.74 o -4 -12 1 5.35 -3.00 38.71 o -3 -12 1 277.32 273.37 81.08 o -2 -12 1 567.78 651.25 109.18 o -1 -12 1 480.54 752.72 120.29 o 0 -12 1 23.65 78.60 60.06 o 1 -12 1 37.15 22.77 62.08 o 2 -12 1 107.73 171.91 73.28 o 3 -12 1 102.07 179.70 78.42 o 4 -12 1 0.98 -15.34 50.88 o 5 -12 1 5.66 -43.61 39.94 o 6 -12 1 375.80 537.19 98.90 o 7 -12 1 8.62 16.93 42.00 o 8 -12 1 73.21 68.93 55.33 o -10 -11 1 66.81 39.67 63.64 o -9 -11 1 130.17 131.28 47.82 o -8 -11 1 41.03 24.41 41.75 o -7 -11 1 67.49 48.30 41.22 o -6 -11 1 25.59 18.68 38.99 o -5 -11 1 528.62 782.99 80.55 o -4 -11 1 200.91 174.06 48.78 o -3 -11 1 368.52 263.09 81.72 o -2 -11 1 122.23 115.43 61.98 o -1 -11 1 591.24 880.45 119.93 o 0 -11 1 108.43 74.75 60.24 o 1 -11 1 438.55 633.62 102.85 o 2 -11 1 146.21 192.01 72.26 o 3 -11 1 23.84 -41.05 50.42 o 4 -11 1 773.19 933.67 90.81 o 5 -11 1 0.66 8.39 42.29 o 6 -11 1 235.01 190.59 66.53 o 7 -11 1 68.86 74.84 45.13 o 8 -11 1 281.33 349.54 66.29 o 9 -11 1 17.55 11.57 64.19 o 10 -11 1 82.79 53.81 72.27 o -11 -10 1 327.81 393.30 93.30 o -10 -10 1 15.14 -0.78 39.76 o -9 -10 1 195.75 111.80 42.67 o -8 -10 1 2.51 -45.73 48.26 o -7 -10 1 376.01 386.95 126.81 o -6 -10 1 72.63 -22.93 34.45 o -5 -10 1 108.70 149.18 44.19 o -4 -10 1 12.63 -1.29 29.04 o -3 -10 1 525.30 880.63 111.48 o -2 -10 1 603.01 859.42 106.52 o -1 -10 1 512.41 523.42 86.96 o 0 -10 1 0.70 -10.19 42.06 o 1 -10 1 61.81 68.32 49.77 o 2 -10 1 1146.68 1262.00 117.37 o 3 -10 1 216.48 310.74 74.38 o 4 -10 1 34.04 26.50 36.01 o 5 -10 1 60.76 -14.55 33.59 o 6 -10 1 610.49 968.27 87.25 o 7 -10 1 0.22 -36.73 42.70 o 8 -10 1 60.50 76.68 61.25 o 9 -10 1 138.84 112.49 73.73 o 10 -10 1 62.98 -19.56 56.11 o 11 -10 1 51.97 -28.65 61.70 o -12 -9 1 11.11 28.19 57.02 o -11 -9 1 12.62 -19.74 54.92 o -10 -9 1 306.10 537.31 83.52 o -9 -9 1 122.35 203.24 47.73 o -8 -9 1 29.29 -3.70 34.19 o -7 -9 1 1.37 7.21 34.80 o -6 -9 1 21.48 -8.67 26.51 o -5 -9 1 1006.11 1070.56 115.30 o -4 -9 1 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