# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 051230b in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 232.48 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0040 _cell_length_b 13.3190 _cell_length_c 17.4390 _cell_angle_alpha 93.785 _cell_angle_beta 99.392 _cell_angle_gamma 106.116 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8133.15 9004.26 794.68 o 2 0 0 27208.39 33573.42 2929.87 o 3 0 0 13091.69 16565.50 1464.60 o 4 0 0 6246.97 6421.60 602.16 o 5 0 0 1090.57 1283.66 223.81 o 6 0 0 2094.77 2530.84 349.70 o 7 0 0 4674.54 4422.83 478.60 o 8 0 0 2340.16 2644.16 297.60 o 9 0 0 62.42 279.56 211.05 o 10 0 0 1378.11 1452.60 293.46 o 11 0 0 689.10 698.48 419.48 o -11 1 0 207.36 -332.03 369.78 o -10 1 0 877.63 868.98 399.03 o -9 1 0 3369.08 3371.47 348.17 o -8 1 0 3304.97 3479.89 297.71 o -7 1 0 1498.73 2002.59 226.16 o -6 1 0 2792.76 2468.79 209.31 o -5 1 0 10979.28 10195.00 647.82 o -4 1 0 1994.20 1677.85 157.19 o -3 1 0 18362.41 18671.57 938.62 o -2 1 0 3208.29 2976.81 158.54 o -1 1 0 35986.16 31665.84 2689.86 o 1 1 0 12711.05 18629.62 1630.35 o 2 1 0 2649.88 3098.48 303.82 o 3 1 0 1054.04 1284.56 184.10 o 4 1 0 941.82 1351.79 217.72 o 5 1 0 5876.84 6109.28 599.90 o 6 1 0 5989.48 5746.42 589.52 o 7 1 0 1412.24 1961.02 356.62 o 8 1 0 37.83 145.29 260.57 o 9 1 0 1854.49 1931.84 442.27 o 10 1 0 1140.06 1356.93 325.56 o -11 2 0 888.11 507.92 353.75 o -10 2 0 1287.32 1304.94 393.24 o -9 2 0 362.80 172.64 173.48 o -8 2 0 67.96 -104.99 148.02 o -7 2 0 5459.40 4812.17 347.41 o -6 2 0 9018.39 8127.58 431.03 o -5 2 0 1068.48 1168.95 142.56 o -4 2 0 8656.35 7415.43 385.80 o -3 2 0 13411.67 12583.72 637.49 o -2 2 0 192.32 201.28 49.83 o -1 2 0 2822.15 2873.15 205.34 o 0 2 0 6201.55 8265.15 736.32 o 1 2 0 8748.73 11994.14 750.86 o 2 2 0 186.81 131.37 58.26 o 3 2 0 5193.52 5759.20 548.09 o 4 2 0 24967.55 29391.32 2595.74 o 5 2 0 8001.92 9317.48 878.53 o 6 2 0 147.75 74.83 205.76 o 7 2 0 272.11 496.11 273.74 o 8 2 0 1057.70 1414.59 389.26 o 9 2 0 524.48 192.82 364.28 o 10 2 0 171.47 -128.60 373.09 o -11 3 0 183.41 -31.51 341.72 o -10 3 0 12.71 -418.40 278.93 o -9 3 0 540.88 344.50 264.56 o -8 3 0 2435.78 2689.25 414.37 o -7 3 0 582.68 676.15 152.71 o -6 3 0 3514.57 3034.72 189.16 o -5 3 0 10162.15 8723.36 455.74 o -4 3 0 12343.92 11019.33 565.25 o -3 3 0 808.41 823.38 108.67 o -2 3 0 1355.11 1310.14 130.29 o -1 3 0 22826.47 24144.94 2132.79 o 0 3 0 25638.74 32651.12 2872.27 o 1 3 0 11415.66 15849.61 991.49 o 2 3 0 37822.97 52991.74 3279.34 o 3 3 0 14576.84 16209.79 1019.46 o 4 3 0 1160.85 1551.08 263.74 o 5 3 0 368.39 388.87 216.81 o 6 3 0 6179.94 6074.61 642.24 o 7 3 0 3568.45 3606.56 479.50 o 8 3 0 46.08 468.06 350.07 o 9 3 0 339.45 593.65 410.08 o 10 3 0 588.03 317.35 412.86 o -11 4 0 16.37 -430.02 286.68 o -10 4 0 401.74 287.72 299.23 o -9 4 0 703.91 642.60 276.44 o -8 4 0 527.40 601.85 262.30 o -7 4 0 3649.79 3106.63 205.17 o -6 4 0 4568.69 4026.57 239.25 o -5 4 0 9966.37 8800.40 462.44 o -4 4 0 48.67 -33.55 67.13 o -3 4 0 15071.94 12966.76 810.85 o -2 4 0 1120.83 1415.58 158.08 o -1 4 0 2619.33 2311.17 250.81 o 0 4 0 1556.26 1939.72 147.62 o 1 4 0 22680.02 31899.03 1983.12 o 2 4 0 13069.36 16860.47 1061.55 o 3 4 0 864.94 1195.44 173.95 o 4 4 0 2439.96 2304.25 301.64 o 5 4 0 6630.44 5641.66 579.67 o 6 4 0 2409.08 3537.82 508.83 o 7 4 0 1955.14 2292.60 466.79 o 8 4 0 1197.33 1898.15 481.31 o 9 4 0 691.06 635.01 465.66 o -11 5 0 201.82 -172.44 313.00 o -10 5 0 454.59 295.02 307.65 o -9 5 0 139.58 521.68 310.81 o -8 5 0 564.59 316.45 244.41 o -7 5 0 1246.17 1035.42 133.98 o -6 5 0 1006.48 950.46 119.47 o -5 5 0 144.28 58.61 78.09 o -4 5 0 21790.39 20712.85 1605.27 o -3 5 0 5148.65 5045.43 345.48 o -2 5 0 1790.10 2256.50 279.46 o -1 5 0 3809.79 4132.69 410.76 o 0 5 0 16840.65 21110.23 1322.27 o 1 5 0 8450.21 11167.63 714.99 o 2 5 0 423.28 610.89 123.39 o 3 5 0 1700.46 2140.17 201.40 o 4 5 0 3559.48 3765.39 426.71 o 5 5 0 233.66 199.07 257.12 o 6 5 0 4337.90 4231.51 510.41 o 7 5 0 3468.54 3718.16 498.30 o 8 5 0 421.60 281.56 408.95 o 9 5 0 53.97 45.50 473.40 o -11 6 0 191.09 -182.60 343.61 o -10 6 0 272.39 736.61 384.29 o -9 6 0 1160.21 847.70 313.83 o -8 6 0 658.03 875.96 238.22 o -7 6 0 443.66 427.97 185.21 o -6 6 0 84.16 -64.31 97.96 o -5 6 0 9714.46 9492.69 623.44 o -4 6 0 560.83 299.97 129.83 o -3 6 0 7709.87 6535.03 443.37 o -2 6 0 15740.13 13374.44 1214.39 o -1 6 0 23046.83 25365.27 2257.17 o 0 6 0 25.26 2.72 94.32 o 1 6 0 16866.58 21263.82 1337.78 o 2 6 0 1592.83 2311.68 295.06 o 3 6 0 686.04 1024.00 168.57 o 4 6 0 5.18 -82.57 216.89 o 5 6 0 2015.60 3160.45 470.93 o 6 6 0 5422.75 4801.55 565.23 o 7 6 0 138.24 -28.13 362.25 o 8 6 0 456.50 616.97 456.48 o 9 6 0 817.39 1163.11 552.37 o -11 7 0 231.90 484.76 420.16 o -10 7 0 1531.51 1188.45 435.51 o -9 7 0 751.14 962.76 376.17 o -8 7 0 99.31 -30.20 212.84 o -7 7 0 542.17 493.08 209.46 o -6 7 0 2084.37 2618.91 279.52 o -5 7 0 181.41 161.64 183.04 o -4 7 0 3374.90 3016.78 251.94 o -3 7 0 7479.50 7095.95 687.59 o -2 7 0 2388.46 2122.41 280.96 o -1 7 0 11.76 -148.42 105.81 o 0 7 0 5944.13 7025.61 473.75 o 1 7 0 6631.25 7191.59 487.16 o 2 7 0 3004.64 2945.70 247.99 o 3 7 0 124.74 37.94 203.05 o 4 7 0 1687.16 1634.48 353.23 o 5 7 0 5765.40 5682.04 624.80 o 6 7 0 63.07 -381.21 302.62 o 7 7 0 669.12 419.33 363.83 o 8 7 0 637.67 589.59 483.10 o -11 8 0 329.34 339.09 434.60 o -10 8 0 34.02 143.87 367.44 o -9 8 0 539.91 952.68 398.06 o -8 8 0 2407.36 3541.71 386.99 o -7 8 0 323.38 53.29 210.34 o -6 8 0 92.26 -13.75 172.71 o -5 8 0 431.37 580.39 183.20 o -4 8 0 4417.73 3848.17 359.44 o -3 8 0 4572.39 3361.77 384.89 o -2 8 0 4490.98 3473.67 395.42 o -1 8 0 3999.79 3623.25 360.49 o 0 8 0 207.54 -166.58 137.78 o 1 8 0 131.71 -229.91 153.28 o 2 8 0 3214.43 3122.86 271.76 o 3 8 0 3560.24 3422.31 420.39 o 4 8 0 2412.64 3042.15 474.01 o 5 8 0 113.56 -192.90 318.64 o 6 8 0 1284.92 1114.90 398.13 o 7 8 0 2007.70 1355.33 459.80 o -11 9 0 46.51 -173.04 455.59 o -10 9 0 398.77 478.74 464.45 o -9 9 0 1659.06 2495.11 378.16 o -8 9 0 99.02 459.94 270.15 o -7 9 0 2068.95 3295.10 368.22 o -6 9 0 3270.63 3310.87 320.86 o -5 9 0 2469.58 2524.39 288.33 o -4 9 0 3071.42 2824.29 370.83 o -3 9 0 2713.74 3231.29 438.36 o -2 9 0 11684.58 10975.05 1037.44 o -1 9 0 681.94 565.91 179.01 o 0 9 0 2853.70 3316.01 570.57 o 1 9 0 10047.25 11130.22 743.95 o 2 9 0 4828.03 4832.62 378.24 o 3 9 0 925.94 1006.08 366.39 o 4 9 0 661.18 204.86 317.28 o 5 9 0 2772.07 2310.27 469.80 o 6 9 0 2325.99 2022.46 506.20 o 7 9 0 14.07 47.98 460.62 o -10 10 0 333.78 -252.84 432.57 o -9 10 0 43.04 467.14 432.72 o -8 10 0 2023.99 2984.22 389.88 o -7 10 0 2027.42 2550.47 688.19 o -6 10 0 331.19 262.03 209.00 o -5 10 0 143.97 235.31 237.11 o -4 10 0 5134.53 3565.35 432.65 o -3 10 0 7903.07 6560.20 679.62 o -2 10 0 398.50 -27.91 652.16 o -1 10 0 1692.13 2227.79 397.90 o 0 10 0 5663.96 5707.51 426.72 o 1 10 0 7425.24 7048.10 510.19 o 2 10 0 3257.55 3703.50 351.74 o 3 10 0 3384.52 3057.72 516.80 o 4 10 0 575.15 199.44 364.88 o 5 10 0 961.27 853.64 402.87 o 6 10 0 289.49 449.34 449.34 o -10 11 0 10.59 -157.85 439.42 o -9 11 0 1770.38 2427.85 395.58 o -8 11 0 1488.01 2002.08 339.34 o -7 11 0 61.04 17.36 343.08 o -6 11 0 1711.79 2170.31 417.53 o -5 11 0 4069.49 4237.60 509.43 o -4 11 0 2164.90 2873.10 454.08 o -3 11 0 734.97 943.43 306.91 o -2 11 0 3056.39 3130.64 305.10 o -1 11 0 2376.70 2610.65 485.82 o 0 11 0 713.59 675.99 241.60 o 1 11 0 184.28 122.11 354.96 o 2 11 0 3486.12 3087.05 511.69 o 3 11 0 524.83 510.48 403.84 o 4 11 0 31.04 -171.69 369.33 o 5 11 0 1008.43 1516.04 482.36 o -9 12 0 226.81 459.28 337.44 o -8 12 0 72.52 217.42 280.82 o -7 12 0 1311.85 1563.72 414.37 o -6 12 0 1043.95 1092.71 356.24 o -5 12 0 56.53 45.65 282.31 o -4 12 0 3358.14 3558.05 519.66 o -3 12 0 2589.53 3447.05 517.93 o -2 12 0 2392.62 2358.17 458.29 o -1 12 0 923.09 1116.32 390.92 o 0 12 0 4581.92 3641.95 341.81 o 1 12 0 4622.08 4043.23 371.97 o 2 12 0 176.78 26.10 397.45 o 3 12 0 685.66 620.73 425.72 o 4 12 0 1806.95 556.73 449.04 o -9 13 0 315.55 278.79 320.81 o -8 13 0 1406.43 1357.28 441.37 o -7 13 0 896.01 1509.42 422.50 o -6 13 0 503.06 398.05 322.54 o -5 13 0 2897.63 2378.33 460.10 o -4 13 0 682.49 7.52 278.17 o -3 13 0 253.40 -69.94 287.65 o -2 13 0 1466.39 1788.65 420.09 o -1 13 0 4047.99 4211.50 403.46 o 0 13 0 3426.98 3881.81 431.11 o 1 13 0 76.88 33.17 294.22 o 2 13 0 1615.87 2134.44 549.14 o 3 13 0 2315.30 2078.19 542.45 o -8 14 0 286.57 832.36 440.85 o -7 14 0 604.63 784.23 387.23 o -6 14 0 1949.53 1349.31 390.46 o -5 14 0 399.93 230.04 330.36 o -4 14 0 4.16 248.99 336.08 o -3 14 0 1904.69 2129.78 468.15 o -2 14 0 3166.68 2911.07 546.58 o -1 14 0 30.86 99.80 416.40 o 0 14 0 258.63 -68.51 292.70 o 1 14 0 893.27 379.47 450.69 o -6 15 0 37.46 198.31 355.63 o -5 15 0 385.78 698.93 397.97 o -4 15 0 1413.49 950.05 401.82 o -3 15 0 1755.86 2113.38 503.64 o -2 15 0 336.75 1146.79 467.77 o -1 15 0 1753.11 1125.65 507.93 o 0 15 0 312.04 -659.46 439.64 o 0 -15 1 429.95 161.54 466.63 o 1 -15 1 30.48 466.93 446.85 o 2 -15 1 2634.54 3171.05 579.07 o 3 -15 1 2031.71 2016.45 473.18 o 4 -15 1 27.34 206.74 379.70 o 5 -15 1 359.75 222.15 335.03 o 6 -15 1 333.64 448.58 367.29 o -2 -14 1 397.08 -214.63 452.05 o -1 -14 1 22.14 -261.03 446.71 o 0 -14 1 611.55 478.98 310.37 o 1 -14 1 4143.19 4664.83 688.34 o 2 -14 1 1924.74 1938.99 465.66 o 3 -14 1 74.00 303.97 351.42 o 4 -14 1 873.70 697.95 351.04 o 5 -14 1 460.09 443.70 333.22 o 6 -14 1 23.46 40.76 321.87 o 7 -14 1 584.73 558.23 348.71 o 8 -14 1 573.82 794.46 411.82 o -3 -13 1 127.37 337.88 472.65 o -2 -13 1 1995.02 1386.46 505.75 o -1 -13 1 2289.93 2542.71 865.79 o 0 -13 1 2003.52 1429.02 360.57 o 1 -13 1 100.73 -22.14 514.92 o 2 -13 1 780.69 954.64 390.76 o 3 -13 1 2109.99 1948.91 412.72 o 4 -13 1 1483.16 1720.74 402.94 o 5 -13 1 88.15 251.10 312.09 o 6 -13 1 1787.15 1882.51 417.61 o 7 -13 1 1398.73 1457.23 419.11 o 8 -13 1 167.55 152.44 376.84 o 9 -13 1 217.59 158.85 332.35 o -4 -12 1 0.81 -431.97 403.32 o -3 -12 1 1964.92 1308.93 462.88 o -2 -12 1 3710.13 3238.74 584.86 o -1 -12 1 1579.65 1556.42 661.23 o 0 -12 1 296.32 722.63 265.35 o 1 -12 1 3295.09 3741.69 620.13 o 2 -12 1 3435.89 3195.65 321.00 o 3 -12 1 1651.25 1906.95 385.95 o 4 -12 1 1690.30 1828.51 365.12 o 5 -12 1 4427.47 4527.81 539.29 o 6 -12 1 1582.45 1719.01 395.20 o 7 -12 1 155.96 369.85 324.50 o 8 -12 1 195.23 182.31 271.39 o 9 -12 1 749.60 1241.89 357.33 o -5 -11 1 316.30 828.90 471.38 o -4 -11 1 2612.08 1622.90 492.21 o -3 -11 1 3642.69 2906.56 537.93 o -2 -11 1 952.34 1313.91 611.11 o -1 -11 1 1442.90 1482.06 285.43 o 0 -11 1 3024.29 3698.33 365.68 o 1 -11 1 152.67 11.58 625.16 o 2 -11 1 116.12 -133.54 170.13 o 3 -11 1 4910.59 4777.26 538.46 o 4 -11 1 4785.68 5283.76 583.58 o 5 -11 1 1341.52 1586.20 361.05 o 6 -11 1 412.37 689.68 291.41 o 7 -11 1 1251.11 1297.64 270.99 o 8 -11 1 1790.96 2178.96 641.19 o 9 -11 1 15.36 430.51 317.76 o 10 -11 1 564.79 651.55 477.16 o -6 -10 1 1770.07 1517.77 508.68 o -5 -10 1 1783.91 1090.01 435.28 o -4 -10 1 2138.78 2336.82 496.20 o -3 -10 1 337.47 -124.76 333.61 o -2 -10 1 3839.09 3972.77 342.79 o -1 -10 1 4825.87 4698.74 374.10 o 0 -10 1 302.86 0.11 307.02 o 1 -10 1 3529.61 3197.04 281.65 o 2 -10 1 5531.77 4527.06 505.15 o 3 -10 1 3387.68 3490.90 426.41 o 4 -10 1 244.68 136.80 236.51 o 5 -10 1 2799.46 2983.42 393.99 o 6 -10 1 2226.66 2494.14 593.59 o 7 -10 1 1461.95 1691.33 296.78 o 8 -10 1 755.25 933.44 283.41 o 9 -10 1 1572.56 2123.99 387.17 o 10 -10 1 110.55 -226.44 465.21 o -7 -9 1 1952.40 1256.89 502.36 o -6 -9 1 814.97 378.95 412.56 o -5 -9 1 8.15 -368.20 334.13 o -4 -9 1 290.23 557.56 335.78 o -3 -9 1 7719.68 6334.51 669.02 o -2 -9 1 2654.58 2574.34 304.52 o -1 -9 1 147.96 -209.61 178.27 o 0 -9 1 13030.99 12746.75 834.17 o 1 -9 1 7026.08 6744.60 673.08 o 2 -9 1 1827.11 2343.06 347.22 o 3 -9 1 2079.17 2607.93 370.00 o 4 -9 1 5929.10 4750.04 514.70 o 5 -9 1 789.18 838.53 208.65 o 6 -9 1 80.98 87.02 195.79 o 7 -9 1 1951.99 2439.61 306.15 o 8 -9 1 5015.39 6006.04 628.56 o 9 -9 1 1309.10 1220.34 491.53 o 10 -9 1 136.82 226.21 473.25 o 11 -9 1 433.71 706.60 523.41 o -8 -8 1 1393.28 1195.67 505.15 o -7 -8 1 769.06 605.69 398.27 o -6 -8 1 357.17 -203.20 342.48 o -5 -8 1 594.33 -212.53 302.17 o -4 -8 1 5593.00 5371.37 590.80 o -3 -8 1 41.79 -33.73 182.15 o -2 -8 1 2157.56 2677.90 475.29 o -1 -8 1 6400.66 6243.10 441.65 o 0 -8 1 14790.32 16271.68 1040.38 o 1 -8 1 2855.86 2754.80 343.46 o 2 -8 1 3630.66 2520.09 314.73 o 3 -8 1 4325.97 3659.43 406.10 o 4 -8 1 1157.89 1288.67 205.63 o 5 -8 1 1163.45 1202.96 203.91 o 6 -8 1 4308.40 4300.59 741.14 o 7 -8 1 1801.53 2893.75 326.72 o 8 -8 1 118.87 294.10 246.97 o 9 -8 1 544.28 1278.39 444.31 o 10 -8 1 1711.44 2537.08 538.84 o 11 -8 1 75.46 311.19 420.23 o -8 -7 1 590.73 695.62 429.18 o -7 -7 1 138.96 174.85 379.02 o -6 -7 1 716.96 750.52 366.99 o -5 -7 1 888.98 635.16 318.41 o -4 -7 1 467.65 370.67 281.11 o -3 -7 1 8270.88 8924.15 599.71 o -2 -7 1 4541.59 4794.80 351.15 o -1 -7 1 3090.43 3033.03 246.96 o 0 -7 1 570.99 685.59 133.90 o 1 -7 1 16127.34 16480.29 1491.07 o 2 -7 1 4923.62 4644.68 478.37 o 3 -7 1 77.68 30.61 140.41 o 4 -7 1 4947.62 4291.62 320.64 o 5 -7 1 4912.17 4746.78 353.10 o 6 -7 1 297.90 448.33 261.63 o 7 -7 1 916.58 1001.83 230.44 o 8 -7 1 950.68 1070.63 252.40 o 9 -7 1 887.61 1323.22 404.67 o 10 -7 1 28.04 538.30 369.24 o 11 -7 1 497.97 457.46 410.91 o -9 -6 1 6.98 132.36 483.03 o -8 -6 1 407.94 576.28 449.79 o -7 -6 1 3134.75 3528.87 567.41 o -6 -6 1 808.33 784.83 342.93 o -5 -6 1 1635.47 2114.44 400.61 o -4 -6 1 6916.15 7100.77 705.11 o -3 -6 1 694.75 1086.23 169.98 o -2 -6 1 394.81 288.51 153.30 o -1 -6 1 4508.07 4900.00 382.30 o 0 -6 1 10398.03 10732.90 982.99 o 1 -6 1 734.47 1088.50 211.02 o 2 -6 1 2349.56 2155.87 269.46 o 3 -6 1 11685.52 10360.58 668.85 o 4 -6 1 9707.95 8240.12 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