# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' TREF in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 245.10 _exptl_crystal_F_000 794.00 _reflns_d_resolution_high 0.7708 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0710 _cell_length_b 11.8400 _cell_length_c 14.3000 _cell_angle_alpha 111.020 _cell_angle_beta 96.580 _cell_angle_gamma 101.560 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1083.87 1100.07 22.43 o 3 0 0 102.88 141.12 18.20 o 4 0 0 9764.57 9953.80 155.34 o 5 0 0 9234.13 9282.43 115.40 o 6 0 0 428.15 486.70 24.22 o 7 0 0 1354.43 1287.36 56.73 o 8 0 0 978.32 982.11 36.21 o 9 0 0 1280.18 1205.89 65.21 o 10 0 0 45.55 -3.23 19.98 o 11 0 0 197.43 185.21 54.12 o -11 1 0 510.21 495.79 76.71 o -10 1 0 502.25 529.58 40.49 o -9 1 0 251.05 266.54 34.84 o -8 1 0 1332.59 1333.99 43.98 o -7 1 0 3182.83 3345.30 70.25 o -6 1 0 17.56 18.14 13.11 o -5 1 0 201.25 274.46 58.81 o -4 1 0 1247.50 1332.37 33.61 o -3 1 0 24725.15 24996.51 304.80 o -2 1 0 8499.53 8516.77 89.81 o 1 1 0 55685.24 58200.23 1248.13 o 2 1 0 3165.46 3298.47 58.07 o 3 1 0 694.51 662.21 52.99 o 4 1 0 1277.50 1180.73 31.49 o 5 1 0 11849.77 12061.14 210.68 o 6 1 0 3013.78 2884.68 73.76 o 7 1 0 283.89 149.15 64.63 o 8 1 0 1689.56 1715.68 51.95 o 9 1 0 747.95 793.16 92.40 o 10 1 0 365.28 327.82 44.22 o 11 1 0 16.12 98.76 70.46 o -12 2 0 0.57 112.63 68.25 o -11 2 0 282.81 257.97 37.54 o -10 2 0 1323.18 1333.48 42.15 o -9 2 0 918.19 880.08 63.14 o -8 2 0 56.62 59.16 20.95 o -7 2 0 1945.66 2004.95 62.99 o -6 2 0 3659.24 3648.30 82.20 o -5 2 0 3495.85 3580.09 59.98 o -4 2 0 134.71 131.89 19.86 o -3 2 0 1923.91 1914.83 34.52 o -2 2 0 6649.08 6538.63 90.28 o -1 2 0 133.56 112.52 22.36 o 0 2 0 148.36 144.14 24.11 o 1 2 0 10544.00 10460.32 182.79 o 2 2 0 8005.97 7717.73 120.32 o 3 2 0 3937.76 3866.33 101.54 o 4 2 0 3557.85 3706.60 200.02 o 5 2 0 1545.32 1559.72 57.15 o 6 2 0 5558.43 5611.65 132.05 o 7 2 0 159.72 157.23 45.77 o 8 2 0 107.87 98.26 58.26 o 9 2 0 253.33 202.72 25.90 o 10 2 0 730.29 629.73 53.09 o -12 3 0 241.08 215.28 73.24 o -11 3 0 15.69 31.36 24.91 o -10 3 0 617.91 684.29 41.86 o -9 3 0 2741.76 2811.90 91.68 o -8 3 0 1074.51 1059.12 37.67 o -7 3 0 257.03 219.27 29.74 o -6 3 0 2454.45 2451.06 45.61 o -5 3 0 6960.95 6815.37 82.62 o -4 3 0 9019.09 8912.08 103.61 o -3 3 0 344.79 481.86 39.69 o -2 3 0 9800.19 9369.95 190.89 o -1 3 0 205.55 234.28 40.57 o 0 3 0 1658.69 1614.11 75.29 o 1 3 0 2885.93 2697.43 83.23 o 2 3 0 7961.73 7911.64 180.11 o 3 3 0 17491.04 17754.30 322.62 o 4 3 0 255.97 188.25 24.57 o 5 3 0 11.43 19.01 28.11 o 6 3 0 722.01 870.87 82.39 o 7 3 0 3043.48 3107.97 68.05 o 8 3 0 1455.55 1437.76 75.12 o 9 3 0 16.92 -32.09 32.09 o 10 3 0 218.06 125.43 63.83 o -12 4 0 590.55 464.96 136.49 o -11 4 0 367.65 387.67 74.11 o -10 4 0 64.74 26.26 39.58 o -9 4 0 1175.08 1256.85 51.89 o -8 4 0 2070.39 2187.17 58.88 o -7 4 0 3190.77 3098.65 54.45 o -6 4 0 39.19 51.47 21.89 o -5 4 0 6627.45 6407.67 89.84 o -4 4 0 7927.17 7850.68 128.86 o -3 4 0 1958.79 1947.11 55.54 o -2 4 0 10.23 37.63 43.59 o -1 4 0 8455.62 8236.16 163.30 o 0 4 0 12123.53 11422.12 213.79 o 1 4 0 3719.62 3763.62 85.72 o 2 4 0 351.16 441.83 49.94 o 3 4 0 3725.10 3848.70 86.28 o 4 4 0 6169.91 6204.94 159.04 o 5 4 0 2544.57 2647.70 137.60 o 6 4 0 35.91 30.70 32.26 o 7 4 0 1164.93 1219.64 109.86 o 8 4 0 827.29 742.38 62.14 o 9 4 0 727.83 697.70 109.86 o 10 4 0 4.98 51.25 61.31 o -12 5 0 458.62 473.07 100.52 o -11 5 0 802.74 811.35 185.04 o -10 5 0 660.86 731.77 55.05 o -9 5 0 0.04 -23.04 23.04 o -8 5 0 1161.29 1178.44 43.55 o -7 5 0 3450.91 3361.19 84.47 o -6 5 0 5596.93 5835.79 115.56 o -5 5 0 37.96 57.41 23.45 o -4 5 0 6306.76 6239.54 110.68 o -3 5 0 5788.12 5511.13 131.14 o -2 5 0 3637.64 3548.16 89.85 o -1 5 0 3711.35 3738.73 92.56 o 0 5 0 4644.15 4610.96 159.59 o 1 5 0 8910.59 8674.44 192.47 o 2 5 0 1743.19 1840.21 75.28 o 3 5 0 31.22 43.48 32.11 o 4 5 0 540.56 546.87 70.46 o 5 5 0 4010.55 4183.24 144.25 o 6 5 0 1787.08 1857.27 167.01 o 7 5 0 1.07 53.29 30.93 o 8 5 0 513.15 655.02 100.98 o 9 5 0 418.09 454.14 126.50 o -12 6 0 11.49 -55.48 82.67 o -11 6 0 396.77 290.82 45.40 o -10 6 0 1528.65 1507.12 81.08 o -9 6 0 994.84 1007.44 85.17 o -8 6 0 100.01 129.18 42.26 o -7 6 0 2405.13 2418.85 76.47 o -6 6 0 4013.29 4156.57 89.44 o -5 6 0 3562.95 3279.00 69.75 o -4 6 0 95.81 80.23 32.23 o -3 6 0 2610.78 2612.61 96.41 o -2 6 0 5332.47 4868.83 168.95 o -1 6 0 5026.92 4743.14 136.87 o 0 6 0 199.49 207.44 43.07 o 1 6 0 1522.72 1553.07 107.36 o 2 6 0 4641.18 4624.07 176.54 o 3 6 0 3766.51 3834.35 103.54 o 4 6 0 1199.27 1312.96 91.55 o 5 6 0 618.77 844.92 91.83 o 6 6 0 1756.30 1995.53 136.77 o 7 6 0 627.35 704.40 60.48 o 8 6 0 64.62 -31.76 43.51 o 9 6 0 100.97 64.56 44.09 o -12 7 0 279.92 195.55 48.27 o -11 7 0 16.63 33.08 49.57 o -10 7 0 630.90 716.22 111.83 o -9 7 0 1309.87 1298.58 57.07 o -8 7 0 924.43 1071.62 53.12 o -7 7 0 7.57 21.12 39.15 o -6 7 0 1469.01 1455.57 57.89 o -5 7 0 4915.09 4597.39 109.20 o -4 7 0 4229.44 4130.34 117.99 o -3 7 0 61.99 105.54 47.07 o -2 7 0 7483.80 7629.33 217.77 o -1 7 0 3960.03 3854.44 115.93 o 0 7 0 4566.90 4312.07 124.58 o 1 7 0 126.02 63.25 87.66 o 2 7 0 2442.94 2461.69 109.47 o 3 7 0 1145.26 1220.16 228.32 o 4 7 0 817.33 1197.35 78.04 o 5 7 0 525.15 503.84 61.19 o 6 7 0 369.83 367.75 57.95 o 7 7 0 1037.09 1180.57 104.82 o 8 7 0 297.53 335.63 115.13 o 9 7 0 36.89 -8.49 67.09 o -12 8 0 365.71 305.59 68.81 o -11 8 0 292.88 301.12 74.90 o -10 8 0 3.79 -38.92 38.92 o -9 8 0 653.78 771.10 53.48 o -8 8 0 874.79 867.86 47.86 o -7 8 0 475.63 360.05 56.15 o -6 8 0 0.83 55.99 51.12 o -5 8 0 2038.32 1954.44 68.25 o -4 8 0 6844.10 6533.59 202.27 o -3 8 0 3167.91 3196.78 142.59 o -2 8 0 31.50 -12.00 48.25 o -1 8 0 2801.85 2542.27 219.44 o 0 8 0 1638.58 1558.90 103.47 o 1 8 0 3230.48 3259.74 124.84 o 2 8 0 427.17 403.08 59.04 o 3 8 0 2454.27 2665.90 207.51 o 4 8 0 1459.23 1633.80 145.92 o 5 8 0 817.37 824.38 79.06 o 6 8 0 173.54 211.78 87.66 o 7 8 0 69.25 31.83 53.52 o 8 8 0 452.87 272.19 67.97 o -11 9 0 575.44 598.93 57.25 o -10 9 0 438.28 331.44 75.15 o -9 9 0 0.59 71.44 42.46 o -8 9 0 707.84 708.05 74.82 o -7 9 0 3028.06 2904.19 83.99 o -6 9 0 1492.14 1499.53 76.72 o -5 9 0 75.79 117.53 45.47 o -4 9 0 3095.62 2993.43 119.36 o -3 9 0 3481.81 3231.39 232.48 o -2 9 0 1578.52 1556.02 116.37 o -1 9 0 397.25 407.23 66.64 o 0 9 0 999.48 1061.68 80.57 o 1 9 0 2733.96 2754.39 202.24 o 2 9 0 2647.97 2777.47 110.04 o 3 9 0 33.43 69.75 56.32 o 4 9 0 191.56 235.33 54.72 o 5 9 0 515.76 385.94 73.41 o 6 9 0 660.97 731.88 67.87 o 7 9 0 23.65 20.86 54.93 o -11 10 0 248.90 229.42 81.32 o -10 10 0 595.96 745.03 87.98 o -9 10 0 950.70 1102.92 68.61 o -8 10 0 199.46 262.35 61.10 o -7 10 0 1030.17 949.49 106.62 o -6 10 0 1698.37 1576.85 71.30 o -5 10 0 993.77 1043.74 102.37 o -4 10 0 45.37 69.35 56.24 o -3 10 0 1124.41 1168.84 88.01 o -2 10 0 2878.28 2824.40 119.89 o -1 10 0 2348.63 2411.66 133.36 o 0 10 0 71.69 -30.69 93.69 o 1 10 0 549.90 491.92 70.22 o 2 10 0 2207.80 2338.50 110.04 o 3 10 0 564.46 655.61 121.51 o 4 10 0 0.87 89.00 93.95 o 5 10 0 189.47 138.47 98.07 o 6 10 0 206.51 108.14 69.01 o -10 11 0 393.89 196.06 50.67 o -9 11 0 554.43 718.69 74.71 o -8 11 0 634.28 791.89 104.39 o -7 11 0 28.48 -12.69 42.09 o -6 11 0 340.67 281.74 70.90 o -5 11 0 1025.58 1087.38 119.29 o -4 11 0 605.18 649.64 149.53 o -3 11 0 125.93 15.91 74.65 o -2 11 0 202.88 81.88 75.75 o -1 11 0 2264.51 2433.41 198.08 o 0 11 0 891.59 1063.40 90.17 o 1 11 0 2.07 4.28 68.66 o 2 11 0 240.97 410.67 121.22 o 3 11 0 609.19 491.45 374.52 o 4 11 0 375.43 271.15 197.80 o 5 11 0 0.97 65.33 74.52 o -9 12 0 225.82 273.34 72.97 o -8 12 0 787.00 926.49 218.94 o -7 12 0 644.18 1016.36 253.68 o -6 12 0 57.80 51.60 49.35 o -5 12 0 111.05 76.19 79.05 o -4 12 0 654.89 590.26 106.91 o -3 12 0 691.48 825.24 91.48 o -2 12 0 19.17 45.04 65.91 o -1 12 0 314.83 349.97 117.90 o 0 12 0 769.85 995.70 115.92 o 1 12 0 563.90 834.61 90.02 o 2 12 0 23.51 107.78 70.46 o 3 12 0 262.88 146.49 69.21 o 4 12 0 460.03 225.82 105.97 o -8 13 0 247.97 169.04 84.83 o -7 13 0 565.95 678.99 168.15 o -6 13 0 606.56 667.21 163.93 o -5 13 0 87.60 19.47 69.01 o -4 13 0 522.43 403.87 145.87 o -3 13 0 607.84 598.55 93.14 o -2 13 0 590.05 483.13 151.49 o -1 13 0 10.23 -58.77 71.17 o 0 13 0 139.78 225.23 78.15 o 1 13 0 634.40 615.64 160.41 o 2 13 0 480.86 653.41 273.26 o -6 14 0 501.80 541.52 120.40 o -5 14 0 468.43 417.41 164.69 o -4 14 0 19.30 -37.94 76.70 o -3 14 0 192.45 106.66 122.06 o -2 14 0 627.65 827.29 107.52 o -1 14 0 294.82 103.93 138.39 o 0 -14 1 23.82 66.11 133.67 o 1 -14 1 257.11 307.19 138.16 o 2 -14 1 641.92 905.67 108.81 o 3 -14 1 279.57 208.81 84.25 o 4 -14 1 257.34 302.89 111.25 o 5 -14 1 184.51 251.13 85.30 o 6 -14 1 614.74 658.59 192.90 o -2 -13 1 519.65 460.48 108.49 o -1 -13 1 760.31 631.29 93.74 o 0 -13 1 482.09 774.48 236.92 o 1 -13 1 39.25 78.91 122.50 o 2 -13 1 204.38 222.86 79.00 o 3 -13 1 1161.09 888.83 147.86 o 4 -13 1 1181.04 1365.82 142.87 o 5 -13 1 109.12 213.38 89.20 o 6 -13 1 174.49 260.31 83.45 o 7 -13 1 588.02 626.30 140.82 o 8 -13 1 449.15 373.23 64.15 o -4 -12 1 282.86 345.19 165.90 o -3 -12 1 502.26 378.55 150.08 o -2 -12 1 38.24 119.36 70.19 o -1 -12 1 179.67 24.01 75.94 o 0 -12 1 1220.29 1294.59 100.42 o 1 -12 1 1144.28 1127.47 148.70 o 2 -12 1 14.79 11.57 105.44 o 3 -12 1 210.59 196.31 74.35 o 4 -12 1 1359.58 1348.07 175.88 o 5 -12 1 1372.44 1371.89 126.96 o 6 -12 1 171.10 131.09 68.37 o 7 -12 1 378.38 385.29 78.39 o 8 -12 1 594.82 680.64 63.90 o 9 -12 1 386.70 543.93 185.88 o -5 -11 1 19.83 -59.62 59.62 o -4 -11 1 96.35 122.25 61.75 o -3 -11 1 528.27 503.31 218.05 o -2 -11 1 609.22 669.78 95.48 o -1 -11 1 15.50 94.57 82.95 o 0 -11 1 310.62 359.41 71.90 o 1 -11 1 2746.56 2781.89 207.22 o 2 -11 1 1772.06 1871.53 108.75 o 3 -11 1 1.47 0.57 64.36 o 4 -11 1 609.42 923.15 229.70 o 5 -11 1 2160.57 2135.77 304.88 o 6 -11 1 1752.10 1730.17 105.76 o 7 -11 1 136.56 124.91 46.07 o 8 -11 1 149.45 226.53 72.68 o 9 -11 1 811.05 914.32 144.23 o 10 -11 1 538.51 426.83 72.61 o -6 -10 1 512.28 342.55 81.65 o -5 -10 1 193.66 141.79 71.45 o -4 -10 1 9.09 11.18 59.26 o -3 -10 1 75.98 59.01 54.34 o -2 -10 1 1379.24 1668.51 96.54 o -1 -10 1 1342.83 1288.34 88.67 o 0 -10 1 2.00 104.01 58.81 o 1 -10 1 749.31 842.78 88.50 o 2 -10 1 2911.21 2735.04 142.86 o 3 -10 1 3046.65 3008.55 151.28 o 4 -10 1 157.46 155.55 75.61 o 5 -10 1 732.87 778.84 68.04 o 6 -10 1 3705.14 3513.21 135.21 o 7 -10 1 1969.41 2104.38 103.75 o 8 -10 1 3.99 -32.07 42.98 o 9 -10 1 176.47 154.16 42.19 o 10 -10 1 556.86 473.20 150.64 o 11 -10 1 644.92 701.19 148.98 o -7 -9 1 2.69 -51.28 63.81 o -6 -9 1 200.60 207.56 55.88 o -5 -9 1 959.91 995.99 101.26 o -4 -9 1 726.96 737.11 154.25 o -3 -9 1 51.76 69.02 57.70 o -2 -9 1 1191.32 1195.87 98.95 o -1 -9 1 1658.03 1695.58 111.99 o 0 -9 1 2279.70 2223.97 103.76 o 1 -9 1 708.14 673.83 72.64 o 2 -9 1 893.28 1028.12 115.68 o 3 -9 1 3259.46 3050.23 145.37 o 4 -9 1 2989.24 2799.14 114.61 o 5 -9 1 248.45 256.20 50.40 o 6 -9 1 99.92 57.52 42.43 o 7 -9 1 2922.33 2882.34 154.04 o 8 -9 1 881.59 802.91 66.20 o 9 -9 1 137.62 189.84 43.21 o 10 -9 1 110.54 165.55 52.99 o 11 -9 1 618.31 778.55 107.39 o -8 -8 1 367.39 310.15 68.88 o -7 -8 1 494.49 470.59 71.79 o -6 -8 1 1.99 -33.30 98.48 o -5 -8 1 1011.12 911.79 150.92 o -4 -8 1 2201.32 2248.50 92.04 o -3 -8 1 4552.51 4714.07 168.07 o -2 -8 1 383.27 454.79 102.92 o -1 -8 1 316.01 225.39 99.04 o 0 -8 1 5255.32 4975.37 228.04 o 1 -8 1 3533.07 3518.23 190.58 o 2 -8 1 1159.69 1076.55 91.47 o 3 -8 1 305.81 209.58 67.41 o 4 -8 1 4758.88 4470.68 132.73 o 5 -8 1 1677.26 1812.67 77.55 o 6 -8 1 111.57 112.72 66.45 o 7 -8 1 63.72 109.69 34.07 o 8 -8 1 796.55 1061.39 66.58 o 9 -8 1 1188.29 1240.90 152.68 o 10 -8 1 78.39 31.26 37.64 o 11 -8 1 45.13 69.23 33.08 o 12 -8 1 554.79 837.23 215.56 o -9 -7 1 0.23 5.20 40.39 o -8 -7 1 135.58 104.16 75.30 o -7 -7 1 798.20 852.49 133.16 o -6 -7 1 1579.18 1631.39 90.94 o -5 -7 1 41.75 -21.91 111.25 o -4 -7 1 374.00 450.92 82.95 o -3 -7 1 2546.92 2574.18 109.77 o -2 -7 1 3266.78 3396.70 131.11 o -1 -7 1 772.51 803.24 76.73 o 0 -7 1 1432.43 1371.30 103.48 o 1 -7 1 8235.84 7744.47 363.42 o 2 -7 1 10260.80 10606.01 228.95 o 3 -7 1 139.26 141.48 45.60 o 4 -7 1 93.30 94.68 43.78 o 5 -7 1 5185.56 5157.47 112.93 o 6 -7 1 4531.85 4283.36 111.82 o 7 -7 1 274.39 271.97 34.62 o 8 -7 1 453.86 477.99 42.59 o 9 -7 1 1223.36 1227.37 47.91 o 10 -7 1 838.74 1036.10 140.50 o 11 -7 1 52.79 105.10 54.60 o 12 -7 1 104.11 208.05 46.15 o -10 -6 1 124.57 79.90 107.64 o -9 -6 1 320.25 170.34 62.14 o -8 -6 1 207.74 215.46 52.15 o -7 -6 1 441.20 724.96 213.89 o -6 -6 1 1222.51 1316.54 114.85 o -5 -6 1 947.57 866.68 100.15 o -4 -6 1 4.39 -20.54 44.69 o -3 -6 1 797.44 837.38 66.78 o -2 -6 1 9008.61 8780.07 212.96 o -1 -6 1 3209.18 3055.40 137.88 o 0 -6 1 9.82 22.90 45.25 o 1 -6 1 78.96 129.67 51.03 o 2 -6 1 4651.69 4201.96 123.34 o 3 -6 1 10202.77 9968.45 223.55 o 4 -6 1 54.79 91.84 32.02 o 5 -6 1 587.32 570.91 50.88 o 6 -6 1 4945.48 4791.18 87.61 o 7 -6 1 4167.94 4236.63 88.24 o 8 -6 1 216.57 219.37 49.73 o 9 -6 1 276.85 214.35 83.93 o 10 -6 1 1345.46 1470.59 64.66 o 11 -6 1 483.40 590.81 42.54 o 12 -6 1 135.24 142.59 76.57 o -10 -5 1 106.16 63.81 93.77 o -9 -5 1 423.42 487.64 220.55 o -8 -5 1 550.20 402.43 50.93 o -7 -5 1 272.99 312.05 38.69 o -6 -5 1 452.13 498.85 43.36 o -5 -5 1 3792.72 3917.56 114.01 o -4 -5 1 1946.47 2022.28 65.33 o -3 -5 1 147.48 188.56 42.81 o -2 -5 1 14.97 22.87 39.67 o -1 -5 1 7458.10 7566.54 147.91 o 0 -5 1 7330.25 7042.82 140.25 o 1 -5 1 852.55 1031.41 52.89 o 2 -5 1 805.80 684.30 63.53 o 3 -5 1 8610.09 8505.53 182.23 o 4 -5 1 4398.76 4332.99 71.64 o 5 -5 1 1934.18 1974.36 45.64 o 6 -5 1 352.85 336.24 27.76 o 7 -5 1 5210.17 5403.78 84.57 o 8 -5 1 2661.30 2536.79 61.71 o 9 -5 1 328.57 284.65 38.83 o 10 -5 1 4.67 -27.98 27.98 o 11 -5 1 599.30 671.39 35.21 o 12 -5 1 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