Acta Cryst. (2006). E62, m2725-m2726  [ doi:10.1107/S1600536806038591 ]

Bis(1,10-phenanthroline-²N,N')(sulfato-²O,O')zinc(II) 1,2-ethenediol solvate

Y.-M. Zhu, K.-L. Zhong and W.-J. Lu

Online 27 September 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• Disorder in solvent or counterion
• R factor = 0.038
• wR factor = 0.109
• Data-to-parameter ratio = 16.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         O1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         S1     
PLAT243_ALERT_4_C High  'Solvent' Ueq as Compared to Neighbors for        C13     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      33.00 Perc.
PLAT313_ALERT_2_C Oxygen with three covalent bonds (rare) ........        O3'     
PLAT731_ALERT_1_C Bond    Calc    1.506(9), Rep    1.508(4) ......       2.25 su-Ra
              C13  -C13     1.555   2.656                                      
PLAT733_ALERT_1_C Torsion Calc     54.9(5), Rep   54.92(16) ......       3.12 su-Ra
              N1  -ZN1 -N1  -C12    2.656   1.555   1.555   1.555              
PLAT779_ALERT_2_C Suspect or Irrelevant (Bond) Angle in CIF ......      36.90 Deg. 
              O3   -C13  -O3'     1.555   1.555   1.555                        

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  10 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   5 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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