# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 60302bm in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 688.90 _exptl_crystal_F_000 1958.00 _reflns_d_resolution_high 0.8254 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 15.0195 _cell_length_b 15.0561 _cell_length_c 16.0797 _cell_angle_alpha 64.393 _cell_angle_beta 79.436 _cell_angle_gamma 65.578 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2020.18 2094.88 91.30 o 3 0 0 83168.90 98888.73 1633.87 o 4 0 0 38156.66 46154.45 428.93 o 5 0 0 19154.42 20422.08 339.93 o 6 0 0 25810.25 27539.58 551.41 o 7 0 0 9.42 17.56 73.40 o 8 0 0 2007.26 2328.89 299.59 o 9 0 0 4179.38 4407.00 772.05 o 10 0 0 12972.05 11274.54 1139.68 o 11 0 0 38.01 -63.94 394.02 o 12 0 0 5639.87 5793.86 1140.38 o 13 0 0 1077.16 2049.61 878.29 o 14 0 0 404.43 363.30 644.51 o 15 0 0 96.48 822.86 835.22 o 16 0 0 1589.29 868.91 878.42 o -16 1 0 2971.73 4116.78 1336.33 o -15 1 0 2628.61 2826.24 1061.36 o -14 1 0 509.91 737.47 714.65 o -13 1 0 3636.23 3008.71 965.35 o -12 1 0 262.57 48.49 510.86 o -11 1 0 1.70 -300.97 356.74 o -10 1 0 5290.84 5036.08 880.46 o -9 1 0 6885.04 6027.88 852.37 o -8 1 0 3138.66 2838.64 261.46 o -7 1 0 13142.62 13727.92 389.24 o -6 1 0 30.33 152.43 216.30 o -5 1 0 1073.51 1801.79 171.52 o -4 1 0 200.54 359.32 96.58 o -3 1 0 2757.15 2468.42 165.56 o -2 1 0 13095.86 13959.82 465.28 o 1 1 0 141041.06 177583.33 15620.07 o 2 1 0 15119.78 12767.83 285.55 o 3 1 0 69468.56 69130.19 1555.78 o 4 1 0 10246.47 9926.62 674.34 o 5 1 0 1016.18 402.52 220.80 o 6 1 0 12111.35 14350.34 967.84 o 7 1 0 30117.14 25430.85 1366.01 o 8 1 0 12475.93 12026.64 1066.12 o 9 1 0 8611.25 6724.94 928.01 o 10 1 0 13091.30 13501.58 1273.05 o 11 1 0 530.13 421.95 447.59 o 12 1 0 38852.74 36624.35 2273.61 o 13 1 0 32115.57 30225.51 2215.71 o 14 1 0 1197.04 1936.72 898.38 o 15 1 0 1085.55 1566.95 886.38 o 16 1 0 206.28 95.00 868.60 o -15 2 0 771.08 654.79 868.09 o -14 2 0 263.41 -85.49 606.07 o -13 2 0 4004.98 3703.62 1009.53 o -12 2 0 82.51 271.76 538.69 o -11 2 0 8820.66 8606.20 1182.55 o -10 2 0 6654.02 6686.66 949.26 o -9 2 0 902.73 1074.67 447.88 o -8 2 0 2968.32 2690.69 223.16 o -7 2 0 54.79 39.41 235.12 o -6 2 0 2711.99 4457.46 348.08 o -5 2 0 10065.77 8811.87 391.08 o -4 2 0 21812.40 24386.79 824.19 o -3 2 0 82781.14 97632.40 1691.82 o -2 2 0 2670.47 3858.16 352.30 o -1 2 0 33008.60 33096.75 925.70 o 0 2 0 1637.45 1087.65 231.25 o 2 2 0 2318.95 1667.80 158.91 o 3 2 0 127499.05 133030.31 1438.42 o 4 2 0 3274.44 1967.80 208.88 o 5 2 0 22084.32 23955.77 1663.59 o 6 2 0 21594.53 22306.70 1268.35 o 7 2 0 2510.13 3195.85 621.89 o 8 2 0 11645.72 9561.85 996.66 o 9 2 0 4916.89 4964.51 855.64 o 10 2 0 9036.25 5818.14 968.89 o 11 2 0 506.60 1080.20 566.70 o 12 2 0 21355.31 20056.28 1761.92 o 13 2 0 38455.18 42850.05 2763.31 o 14 2 0 4810.12 7289.88 1432.39 o 15 2 0 2188.16 2806.27 1098.68 o 16 2 0 2446.18 3049.45 1190.63 o 17 2 0 31.10 -671.59 671.59 o -15 3 0 56.02 -122.98 745.52 o -14 3 0 197.57 359.41 653.57 o -13 3 0 2023.49 1386.60 791.15 o -12 3 0 9.63 56.00 484.03 o -11 3 0 19576.49 18434.03 1539.72 o -10 3 0 46590.74 42892.20 2086.23 o -9 3 0 12766.62 13444.75 1123.93 o -8 3 0 4149.45 4083.58 292.86 o -7 3 0 11956.91 13842.79 582.70 o -6 3 0 18146.58 20129.00 664.40 o -5 3 0 31890.67 33604.02 1142.23 o -4 3 0 665.53 323.65 194.58 o -3 3 0 28494.23 37124.38 1212.90 o -2 3 0 14372.25 16094.26 799.49 o -1 3 0 28978.15 31509.70 1093.09 o 0 3 0 81724.52 88636.16 1302.12 o 1 3 0 93.19 77.72 56.44 o 2 3 0 39941.90 36810.22 2789.01 o 3 3 0 309.08 264.63 120.06 o 4 3 0 20072.28 18394.59 760.09 o 5 3 0 751.71 1795.40 208.23 o 6 3 0 15609.78 15022.35 807.91 o 7 3 0 175.93 154.09 277.40 o 8 3 0 23.21 579.61 386.67 o 9 3 0 4111.71 4527.75 918.19 o 10 3 0 4132.88 4331.97 934.83 o 11 3 0 499.66 563.50 515.12 o 12 3 0 32.47 -269.61 459.74 o 13 3 0 3942.15 2114.91 926.42 o 14 3 0 936.86 908.18 801.29 o 15 3 0 2397.25 2056.92 1003.61 o 16 3 0 3526.03 4231.52 1368.41 o 17 3 0 30.00 80.28 776.76 o -14 4 0 361.68 486.57 733.98 o -13 4 0 28.36 481.06 652.88 o -12 4 0 216.46 519.91 579.62 o -11 4 0 2402.04 3330.47 845.35 o -10 4 0 20346.90 21322.34 1557.91 o -9 4 0 16427.28 18116.61 1346.96 o -8 4 0 740.44 562.40 375.01 o -7 4 0 11298.02 10677.39 570.21 o -6 4 0 7848.49 7642.67 470.08 o -5 4 0 15245.11 18379.29 966.41 o -4 4 0 25665.44 26256.55 1160.01 o -3 4 0 16661.78 14480.94 865.44 o -2 4 0 3422.99 2953.00 446.75 o -1 4 0 19538.92 16626.71 917.76 o 0 4 0 20682.67 21996.60 558.35 o 1 4 0 39938.49 45056.27 827.08 o 2 4 0 355092.81 389588.09 11948.98 o 3 4 0 248675.22 265475.09 2521.18 o 4 4 0 1391.89 1143.54 226.87 o 5 4 0 6205.37 6618.51 417.35 o 6 4 0 5729.42 4265.46 348.31 o 7 4 0 7805.07 9852.86 979.23 o 8 4 0 2989.03 4522.27 842.72 o 9 4 0 3481.36 2226.28 734.69 o 10 4 0 21174.58 18511.73 1624.85 o 11 4 0 777.60 505.40 501.63 o 12 4 0 8941.99 9685.11 1409.51 o 13 4 0 4009.98 5170.22 1201.47 o 14 4 0 0.99 42.41 625.96 o 15 4 0 90.92 394.40 750.56 o 16 4 0 1678.51 1515.31 991.96 o 17 4 0 22.35 -48.10 861.88 o -12 5 0 305.31 197.42 597.47 o -11 5 0 669.40 231.27 528.26 o -10 5 0 1.78 -354.17 354.17 o -9 5 0 1112.32 248.26 407.32 o -8 5 0 1780.13 1726.71 542.28 o -7 5 0 8446.93 8111.01 549.16 o -6 5 0 336.42 120.23 269.89 o -5 5 0 4795.17 3814.80 561.56 o -4 5 0 2347.93 4092.68 593.20 o -3 5 0 21527.55 24978.33 1262.00 o -2 5 0 15887.35 17330.99 1052.28 o -1 5 0 3820.76 3994.58 569.04 o 0 5 0 11836.35 12439.08 480.26 o 1 5 0 1032.36 1210.73 114.15 o 2 5 0 213539.88 228218.98 2258.01 o 3 5 0 357843.50 423355.25 6744.98 o 4 5 0 63285.99 65180.01 2164.71 o 5 5 0 7084.85 8745.75 526.77 o 6 5 0 38137.91 42042.66 1109.32 o 7 5 0 19478.87 19599.96 746.47 o 8 5 0 13101.24 15960.27 1399.72 o 9 5 0 10751.89 10374.41 1202.19 o 10 5 0 245.71 0.19 447.94 o 11 5 0 385.47 648.83 562.12 o 12 5 0 9869.05 9862.06 1433.28 o 13 5 0 7157.52 6594.49 1288.02 o 14 5 0 2013.59 1693.81 848.79 o 15 5 0 9630.89 10240.17 1689.99 o 16 5 0 1322.21 833.83 910.25 o 17 5 0 128.53 13.35 821.80 o -11 6 0 829.11 722.33 567.05 o -10 6 0 2163.54 1325.70 636.14 o -9 6 0 2.36 -23.99 389.68 o -8 6 0 27.59 -176.99 338.18 o -7 6 0 2965.35 3174.02 575.79 o -6 6 0 2812.15 3690.55 617.34 o -5 6 0 432.72 437.40 326.99 o -4 6 0 591.90 892.64 400.13 o -3 6 0 278.52 615.78 331.01 o -2 6 0 1175.10 863.83 369.76 o -1 6 0 24069.10 20743.17 1259.18 o 0 6 0 4288.80 3582.29 610.02 o 1 6 0 291.02 335.93 84.89 o 2 6 0 645.52 1905.30 262.64 o 3 6 0 70635.62 91409.45 1570.97 o 4 6 0 20258.02 22935.08 841.45 o 5 6 0 15271.05 15021.75 719.05 o 6 6 0 33497.14 32900.20 1075.56 o 7 6 0 159.97 201.18 163.67 o 8 6 0 40.17 70.83 166.07 o 9 6 0 7582.93 6575.74 517.82 o 10 6 0 15366.05 15290.30 1515.20 o 11 6 0 9044.96 6478.31 1159.05 o 12 6 0 7694.33 9143.11 1420.92 o 13 6 0 4050.42 4099.57 1123.54 o 14 6 0 5786.80 5042.06 1289.03 o 15 6 0 29284.69 31286.65 2614.05 o 16 6 0 14847.79 17498.49 2076.56 o 17 6 0 122.53 682.75 880.47 o -10 7 0 1044.48 498.29 552.90 o -9 7 0 1521.67 1137.48 603.33 o -8 7 0 11911.05 12522.43 1148.00 o -7 7 0 5088.81 5030.64 746.16 o -6 7 0 1395.00 1297.78 459.28 o -5 7 0 4931.55 3605.94 674.82 o -4 7 0 3680.01 3337.70 663.83 o -3 7 0 5181.37 5228.13 816.86 o -2 7 0 632.47 482.94 366.80 o -1 7 0 53436.15 47860.71 2051.73 o 0 7 0 62319.00 59580.99 2263.72 o 1 7 0 1264.55 1079.24 135.34 o 2 7 0 29816.36 31785.35 933.56 o 3 7 0 3392.23 3872.05 386.77 o 4 7 0 632.31 1200.19 285.97 o 5 7 0 7717.71 7828.31 573.05 o 6 7 0 31766.20 32405.92 1125.79 o 7 7 0 707.36 570.67 258.07 o 8 7 0 7738.99 9045.36 639.71 o 9 7 0 1882.56 2276.18 387.24 o 10 7 0 1540.71 1574.99 663.35 o 11 7 0 63.04 179.18 490.00 o 12 7 0 807.73 234.66 508.82 o 13 7 0 75.51 253.06 614.72 o 14 7 0 227.74 -0.70 625.21 o 15 7 0 7949.19 7659.60 1556.78 o 16 7 0 9355.16 9465.78 1758.81 o 17 7 0 145.57 -36.54 747.29 o -9 8 0 682.89 390.29 492.79 o -8 8 0 13622.09 13176.75 1222.80 o -7 8 0 18426.42 21025.66 1465.57 o -6 8 0 1106.33 1826.34 569.87 o -5 8 0 4791.48 3578.14 744.47 o -4 8 0 6404.18 6551.30 922.64 o -3 8 0 9702.30 10830.67 1082.47 o -2 8 0 12627.85 9737.10 1055.05 o -1 8 0 149.13 -73.38 295.21 o 0 8 0 11059.67 10154.18 520.65 o 1 8 0 2615.38 2491.16 203.22 o 2 8 0 13415.75 14276.64 688.34 o 3 8 0 5608.79 6621.04 696.58 o 4 8 0 14382.46 11437.38 682.05 o 5 8 0 29562.45 26913.14 2293.27 o 6 8 0 24.62 -97.96 169.04 o 7 8 0 3799.64 3664.92 672.70 o 8 8 0 577.66 576.26 278.11 o 9 8 0 130.65 194.10 242.39 o 10 8 0 8.16 46.11 335.55 o 11 8 0 2830.57 2301.49 816.90 o 12 8 0 15361.02 18244.81 1810.60 o 13 8 0 6171.96 5271.96 1226.67 o 14 8 0 194.53 -244.45 510.66 o 15 8 0 958.54 72.35 644.95 o 16 8 0 5.66 -360.08 667.00 o 17 8 0 125.72 -544.42 634.11 o -7 9 0 3960.36 4968.48 876.37 o -6 9 0 871.36 1708.34 606.53 o -5 9 0 1083.41 997.30 511.90 o -4 9 0 417.45 269.58 458.02 o -3 9 0 16.30 411.09 416.85 o -2 9 0 3860.26 2824.47 753.00 o -1 9 0 14036.77 12515.38 1227.74 o 0 9 0 7106.91 5859.62 958.70 o 1 9 0 4130.76 3731.55 438.00 o 2 9 0 9957.43 10075.79 641.54 o 3 9 0 2621.01 3031.15 427.50 o 4 9 0 40580.35 41314.85 1321.05 o 5 9 0 141897.30 141271.39 2520.01 o 6 9 0 53612.35 47935.01 7612.84 o 7 9 0 23.28 260.25 245.71 o 8 9 0 13114.13 12020.09 813.24 o 9 9 0 6894.33 7884.19 698.66 o 10 9 0 3022.85 3600.33 877.83 o 11 9 0 44.62 -70.00 458.47 o 12 9 0 4830.30 3674.33 1053.02 o 13 9 0 5261.88 4941.01 1223.36 o 14 9 0 361.07 -359.54 538.50 o 15 9 0 5867.45 5337.32 1372.87 o 16 9 0 1249.61 1221.56 948.57 o 17 9 0 75.97 -0.31 751.07 o -6 10 0 231.32 623.49 541.98 o -5 10 0 1967.51 1411.07 621.39 o -4 10 0 1411.49 2045.94 718.03 o -3 10 0 86.24 117.71 424.97 o -2 10 0 538.68 529.09 509.72 o -1 10 0 1200.23 466.45 461.73 o 0 10 0 2475.18 1779.45 666.27 o 1 10 0 95.45 -32.04 313.87 o 2 10 0 3.19 23.90 182.95 o 3 10 0 318.02 328.19 238.39 o 4 10 0 4901.58 4695.81 670.89 o 5 10 0 45360.50 52461.25 1609.33 o 6 10 0 48285.63 45800.06 2744.66 o 7 10 0 1947.32 2282.83 466.41 o 8 10 0 7546.03 5540.99 653.27 o 9 10 0 4962.22 4554.00 619.22 o 10 10 0 2361.55 2972.65 527.15 o 11 10 0 2400.38 1652.24 765.91 o 12 10 0 1569.31 1307.47 772.45 o 13 10 0 258.27 630.26 622.91 o 14 10 0 1453.02 2253.67 957.92 o 15 10 0 4815.38 5546.78 1357.59 o 16 10 0 382.36 -178.50 655.97 o 17 10 0 3604.71 2853.00 1187.91 o -7 11 0 142.56 -20.54 493.84 o -6 11 0 93.26 5.22 461.40 o -5 11 0 3.07 -72.48 441.97 o -4 11 0 1716.86 2059.31 780.14 o -3 11 0 2130.50 1657.95 741.90 o -2 11 0 112.83 -37.97 419.95 o -1 11 0 237.09 300.25 448.28 o 0 11 0 12.79 -125.86 369.76 o 1 11 0 7995.25 7578.49 1230.97 o 2 11 0 23697.10 20819.71 1570.06 o 3 11 0 8651.69 8033.09 704.31 o 4 11 0 35.26 105.88 236.82 o 5 11 0 563.36 534.43 309.41 o 6 11 0 110.86 307.99 275.32 o 7 11 0 2014.66 1817.46 534.48 o 8 11 0 8123.21 6880.29 747.08 o 9 11 0 1107.31 799.45 396.78 o 10 11 0 504.66 509.14 363.96 o 11 11 0 256.53 60.62 512.04 o 12 11 0 1513.44 2415.49 919.56 o 13 11 0 2237.59 2038.78 909.09 o 14 11 0 1171.99 1945.86 933.67 o 15 11 0 1299.68 800.42 749.32 o 16 11 0 80.45 -340.71 692.63 o -5 12 0 4756.08 5283.84 1149.14 o -4 12 0 856.52 621.85 593.34 o -3 12 0 910.78 805.44 613.14 o -2 12 0 2225.82 3059.47 941.05 o -1 12 0 2427.71 2585.34 892.63 o 0 12 0 1149.12 2004.19 824.71 o 1 12 0 956.37 831.17 620.11 o 2 12 0 15726.84 13025.05 1532.70 o 3 12 0 15055.54 14563.33 981.47 o 4 12 0 70.58 184.06 285.68 o 5 12 0 7894.86 8297.67 831.53 o 6 12 0 3441.47 3814.64 648.48 o 7 12 0 1026.69 1015.55 410.65 o 8 12 0 3181.51 3089.39 826.48 o 9 12 0 3205.70 2856.81 595.24 o 10 12 0 14.96 -4.82 325.96 o 11 12 0 675.44 248.81 542.24 o 12 12 0 13.70 39.23 545.56 o 13 12 0 44.45 -2.66 575.26 o 14 12 0 633.47 1030.82 834.86 o 15 12 0 1412.13 1288.65 926.67 o 16 12 0 170.91 66.81 671.60 o -4 13 0 3148.31 3658.03 1074.61 o -3 13 0 156.92 -138.19 489.51 o -2 13 0 348.31 619.40 720.24 o -1 13 0 659.21 473.63 690.15 o 0 13 0 1485.96 834.43 701.94 o 1 13 0 2373.15 2215.67 865.78 o 2 13 0 213.97 32.50 585.07 o 3 13 0 101.23 366.27 336.48 o 4 13 0 498.38 468.29 347.92 o 5 13 0 3480.61 3419.76 634.19 o 6 13 0 9.73 -80.91 305.79 o 7 13 0 6686.93 6358.75 1328.24 o 8 13 0 6435.73 6169.59 826.27 o 9 13 0 1.19 -3.63 332.99 o 10 13 0 1537.08 1546.59 514.05 o 11 13 0 1039.18 970.23 688.24 o 12 13 0 511.95 1112.23 727.13 o 13 13 0 1.13 369.98 731.74 o 14 13 0 1936.54 2793.12 1107.01 o 15 13 0 5644.18 5704.53 1393.67 o -2 14 0 154.57 103.10 701.79 o -1 14 0 28.11 -597.94 597.94 o 0 14 0 206.03 -450.78 651.31 o 1 14 0 381.19 836.09 729.84 o 2 14 0 2150.92 1766.09 925.84 o 3 14 0 1553.09 1452.21 871.63 o 4 14 0 1094.58 816.63 455.32 o 5 14 0 1425.78 1391.37 518.80 o 6 14 0 45.42 75.66 388.59 o 7 14 0 10491.43 11873.99 1706.26 o 8 14 0 20538.16 16927.31 1790.41 o 9 14 0 4448.89 5192.67 832.78 o 10 14 0 538.03 349.18 438.79 o 11 14 0 2569.45 3399.42 1116.96 o 12 14 0 1513.86 578.00 713.27 o 13 14 0 526.95 -121.72 677.98 o 14 14 0 2.44 -590.02 676.07 o 0 15 0 89.53 -473.89 655.01 o 1 15 0 69.17 42.83 693.28 o 2 15 0 32.76 -202.45 744.81 o 3 15 0 23.68 39.46 785.68 o 4 15 0 825.39 1041.86 530.47 o 5 15 0 552.75 868.31 485.06 o 6 15 0 19.49 231.66 434.34 o 7 15 0 550.52 64.40 418.00 o 8 15 0 3574.54 3765.08 774.80 o 9 15 0 1671.46 1123.33 818.03 o 10 15 0 147.14 122.66 451.05 o 11 15 0 785.12 567.66 689.70 o 12 15 0 56.44 -526.76 526.76 o 3 16 0 293.86 278.23 897.03 o 4 16 0 4215.96 4260.84 1382.82 o 5 16 0 6457.20 7946.25 1071.30 o 6 16 0 1531.29 988.01 592.41 o 7 16 0 143.61 -1.41 446.82 o 8 16 0 551.92 391.04 574.54 o 9 16 0 372.37 -214.64 465.77 o 10 16 0 945.47 43.78 519.73 o -7 -16 1 557.13 355.55 708.90 o -6 -16 1 89.88 -549.49 549.49 o -11 -15 1 1207.61 923.00 791.97 o -10 -15 1 964.05 987.75 848.20 o -9 -15 1 116.30 46.33 607.57 o -8 -15 1 655.07 135.35 482.05 o -7 -15 1 4.47 -328.38 389.90 o -6 -15 1 174.95 111.40 456.03 o -5 -15 1 4.36 -249.48 441.11 o -4 -15 1 30.38 -367.62 743.17 o -3 -15 1 0.19 -441.62 756.51 o 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