Acta Cryst. (2006). E62, m2653-m2655  [ doi:10.1107/S1600536806037378 ]

Tetrakis(-naphthalene-1-acetato-²O:O')bis[(N,N-dimethylformamide-O)copper(II)] N,N-dimethylformamide disolvate

H.-T. Xia, Y.-F. Liu and S.-A. Li

Online 20 September 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.006 Å
• Disorder in solvent or counterion
• R factor = 0.037
• wR factor = 0.095
• Data-to-parameter ratio = 12.5

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.86 Ratio
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         N1     
PLAT243_ALERT_4_C High  'Solvent' Ueq as Compared to Neighbors for        C28     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for         N2     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for       C28'     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      44.00 Perc.
PLAT309_ALERT_2_C Single Bonded Oxygen (C-O .GT. 1.3 Ang) ........        O6'     

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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