Acta Cryst. (2006). E62, m2442-m2444  [ doi:10.1107/S1600536806034751 ]

Acetato[-10,21-dibutyl-3,6,14,17-tetrazatricyclo[17.3.1.1^8,12]tetracosa-1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato(2-)-⁴N³,N⁶,O²³,O²⁴:⁴N¹⁴,N¹⁷,O²³,O²⁴]dinickel(II) perchlorate acetonitrile hemisolvate

H. Zhou, Z.-Q. Pan and Y.-J. Zhang

Online 6 September 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.005 Å
• R factor = 0.045
• wR factor = 0.101
• Data-to-parameter ratio = 15.5

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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